Details

Title

Process Design for Size-Controlled Flame Spray Synthesis of Li4Ti5O12 and Electrochemical Performance

Journal title

Chemical and Process Engineering

Yearbook

2017

Numer

No 1

Publication authors

Divisions of PAS

Nauki Techniczne

Instructions for authors [EN]

<p>All manuscripts submitted for publication in Chemical and Process Engineering must comprise a description of original research that has neither been published nor submitted for publication elsewhere.</p> <p>The content, aim and scope of the proposals should comply with the main subject of the journal, i.e. they should deal with mathematical modelling and/or experimental investigations on momentum, heat and mass transfer, unit processes and operations, integrated processes, biochemical engineering, statics and kinetics of chemical reactions. The experiments and modelling may cover different scales and processes ranging from the molecular phenomena up to production systems. The journal language is grammatically correct British English.</p> <p>Chemical and Process Engineering publishes: i) full text research articles, ii) invited reviews, iii) letters to the editor and iv) short communications, aiming at important new results and/or applications. Each of the publication form is peer-reviewed by at least two independent referees. &nbsp;</p> <p><strong>Submission of materials for publication</strong></p> <p>The manuscripts are submitted for publication via Internet site <a href="http://www.chpe.pl">www.chpe.pl</a> and its subfolder Authors Pathway or e-mail address <a href="mailto:andrzej.bin@outlook.com">andrzej.bin@outlook.com</a>. When writing the manuscript, authors should preferably use the template for articles, which is available on the <a href="http://www.chpe.pl">www.chpe.pl</a> page in section Instructions for Authors.&nbsp; &nbsp;</p> <p>Proposals of a paper should be uploaded using the Internet site of the journal and should contain:</p> <ul> <li>a manuscript file in Word format (*.doc, *.docx),</li> <li>the manuscript mirror in PDF format,</li> <li>all graphical figuresin separate graphics files.</li> </ul> <ul> </ul> <p>In the following paragraphthe general guidelines for the manuscript preparation are presented.</p> <p><strong>Manuscript outline</strong></p> <ol> <ol> <ol> <ol> <li><strong>Header details</strong> <ol style="list-style-type: lower-alpha;"> <li>Title of paper</li> <li>Names (first name and further initials) and surnames of authors</li> <li>Institution(s) (affiliation)</li> <li>Address(es) of authors</li> <li>Information about the corresponding author; academic title, name and surname, email address, address for correspondence</li> </ol> </li> <li><strong>Abstract</strong> – should contain a short summary of the proposed paper. In the maximum of 200 words the authors should present the main assumptions, results and conclusions drawn from the presented study.</li> <li><strong>Keywords</strong>– Up to 5 characteristic keyword items should be provided.</li> <li><strong>Text</strong> <ol style="list-style-type: lower-alpha;"> <li>Introduction. In this part, description of motivation for the study and formulation of the scientific problem should be included and supported by a concise review of recent literature.</li> <li>Main text. It should contain all important elements of the scientific investigations, such as presentation of experimental rigs, mathematical models, results and their discussion. This part may be divided into subchapters.</li> <li>Conclusions. The major conclusions can be put forward in concise style in a separate chapter. Presentation of conclusions from the reported research work accompanied by a short commentary is also acceptable.</li> Figures: drawings, diagrams and photographs can be in colour and should be located in appropriate places in the manuscript text according to the template provided on the <a href="http://www.chpe.pl">www.chpe.pl</a> page. Their graphical form should be of vector or raster type with the minimum resolution of 900 dpi. In addition, separate files containing each of the drawings, graphs and photos should be uploaded onto the journal Web site in one of the following formats: bmp, gif, tiff, jpg, eps. Due to rigid editorial reasons, graphical elements created within MS Word and Excel are not acceptable. The final length of figures should be intended typically for 8 cm (single column) or 16 cm in special cases of rich-detail figures. The basic font size of letters in figures should be at least 10 pts after adjusting graphs to the final length. &nbsp; </ol> <p>Figures: drawings, diagrams and photographs should be in gray scale. In case of coloured graphs or photo an additional payment of 300 PLN (72 €) per 1 page containing coloured figures on both sides, or 150 PLN (36 €) per page containing coloured figures on one side will be required.</p> Tables should be made according to the format shown in the template.</li> <br> All figures and tables should be numbered and provided with appropriate title and legend, if necessary. They have to be properly referenced to and commented in the text of the manuscript.<br> <br> <li><strong>List of symbols </strong>should be accompanied by their units</li> <li><strong>Acknowledgements</strong> may be included before the list of literature references</li> <li><strong>Literature citations</strong></li> </ol> </ol> </ol> </ol> <p>&nbsp;</p> <p>The method of quoting literature source in the manuscript depends on the number of its authors:</p> <ul> <li>single author – their surname and year of publication should be given, e.g. Marquardt (1996) or (Marquardt, 1996),</li> <li>two authors – the two surnames separated by the conjunction “and” with the publication year should be given, e.g. Charpentier and McKenna (2004) or (Charpentier and McKenna, 2004),</li> <li>three and more authors – the surname of the first author followed by the abbreviation “et al.” and year of publication should be given, e.g. Bird et al. (1960) or (Bird et al., 1960).</li> </ul> <p>In the case of citing more sources in one bracket, they should be listed in alphabetical order using semicolon for separation, e.g. (Bird et al., 1960; Charpentier and McKenna, 2004; Marquardt, 1996). Should more citations of the same author(s) and year appear in the manuscript then letters “a, b, c, ...” should be successively applied after the publication year.</p> <p>Bibliographic data of the quoted literature should be arranged at the end of the manuscript text in alphabetic order of surnames of the first author. It is obligatory to indicate the DOI number of those literature items, which have the numbers already assigned. Journal titles should be specified by typingtheir right abbreviationsor, in case of doubts, according to the List of Title Word Abbreviations available at <a href="http://www.issn.org/2-22661-LTWA-online.php.">http://www.issn.org/2-22661-LTWA-online.php.</a></p> <p><strong>Examples of citation for:</strong></p> <p><strong>Articles</strong><br> Charpentier J. C., McKenna T. F., 2004.Managing complex systems: some trends for the future of chemical and process engineering. Chem. Eng. Sci., 59, 1617-1640. DOI: <a target="_blank" href="http://dx.doi.org/10.1016/j.ces.2004.01.044">10.1016/j.ces.2004.01.044</a>.</p> <p><strong>Information from books</strong> (we suggest adding the page numbers where the quoted information can be found)<br> Bird R. B., Stewart W.E., Lightfood E.N., 2002. Transport Phenomena. 2nd edition, Wiley, New York, 415-421.</p> <p><strong>Chapters in books</strong><br> Hanjalić K., Jakirlić S., 2002. Second-moment turbulence closure modelling, In: Launder B.E., Sandham N.D. (Eds.), Closure strategies for turbulent and transitional flows. Cambridge University Press, Cambridge, 47-101.</p> <p><strong>Conferences</strong><br> ten Cate A., Bermingham S.K., Derksen J.J., Kramer H.M.J., 2000. Compartmental modeling of an 1100L DTB crystallizer based on Large Eddy flow simulation. 10th European Conference on Mixing. Delft, the Netherlands, 2-5 July 2000, 255-264.</p> <p><strong>8. Payments </strong></p> <p>Starting from 2014 a principle of publishing articles against payment is introduced, assuming non-profit making editorial office. According to the principle authors or institutions employing them, will have to cover the expenses amounting to 40 PLN (or 10 €) per printed page. The above amount will be used to supplement the limited financial means received from the Polish Academy of Sciences for the editorial and publishing; and in particular to increase the capacity of the next CPE volumes and to proofread the linguistic correctness of the articles. The method of payment will be indicated in an invoice sent to the authors or institutions after acceptance of their manuscripts to be published. In justifiable cases presented in writing, the editorial staff may decide to relieve authors from basic payment, either partially or fully. All correspondence should be sent to Editor-in-Chief, Prof. Andrzej K. Biń, email address: <a href="mailto:andrzej.bin@outlook.com">andrzej.bin@outlook.com</a>.</p> <br> </body>

Publisher

Polish Academy of Sciences Committee of Chemical and Process Engineering

Date

2017

Identifier

ISSN 0208-6425

References

Wagemaker (2009), Li - ion diffusion in the equilibrium nanomorphology of spinel xTi, Phys Chem B, 4, 113, doi.org/10.1021/Jp8073706 ; Waser (2014), Air entrainment during flame aerosol synthesis of nanoparticles, Aerosol Sci Technol, 48, doi.org/10.1080/02786826.2014.969800 ; Pratsinis (1998), Flame aerosol synthesis of ceramic powders, Prog Energ Combust, 24, doi.org/10.1016/S0360-1285(97)00028-2 ; Naoi (2013), New generation nanohybrid supercapacitor ", Accounts Chem Res, 46, doi.org/10.1021/Ar200308h ; Kho (2011), Dopant - free , polymorphic design of TiO nanocrystals by flame aerosol synthesis, Chem Eng Sci, 66, doi.org/10.1016/J.Ces.2011.02.058 ; Gaberscek (2007), Is small particle size more important than carbon coating ? An example study on LiFePO cathodes, Electrochem Commun, 9, 4, doi.org/10.1016/J.Elecom.2007.09.020 ; Poullikkas (2013), A comparative overview of large - scale battery systems for electricity storage, Renew Sust Energ Rev, 27, doi.org/10.1016/J.Rser.2013.07.017 ; Athanassiou (2006), Large - scale production of carbon - coated copper nanoparticles for sensor applications, Nanotechnology, 17, doi.org/10.1088/0957-4484/17/6/022 ; Vlad (2014), Hybrid supercapacitor - battery materials for fast electrochemical charge storage, Sci Rep, 4, 1, doi.org/10.1038/Srep04315 ; Teleki (2006), Sensing of organic vapors by flame - made TiO nanoparticles, Chem, 119, doi.org/10.1016/j.snb.2006.01.027 ; Mueller (2004), Non - agglomerated dry silica nanoparticles, Powder Technol, 140, doi.org/10.1016/J.Powtec.2004.01.004\ ; Karhunen (2011), Transition metal - doped lithium titanium oxide nanoparticles made using flame spray pyrolysis, ISRN Nanotechnology, 2011, doi.org/10.5402/2011/180821 ; Hudak (2012), Size effects in the electrochemical alloying and cycling of electrodeposited aluminum with lithium, Electrochem Soc, 159, doi.org/10.1149/2.023206jes ; Deschanvres (1971), Synthesis and crystallographic study of new solid solution of spinelle xTi - xO less than or equal to x less than or equal to, Mater Res Bull, 1, 4, doi.org/10.1016/0025-5408(71)90103-6 ; Teoh (2010), Flame spray pyrolysis : An enabling technology for nanoparticles design and fabrication, Nanoscale, 2, 1324, doi.org/10.1039/C0nr00017e ; Ohzuku (1995), Zero - strain insertion material of Li ti for rechargeable lithium cells, Electrochem Soc, 1, 142, doi.org/10.1149/1.2048592 ; Jiang (2004), Comparison of the reactions between Ti or LiC and nonaqueous solvents or electrolytes using accelerating rate calorimetry, Electrochem Soc, 7, 151, doi.org/10.1149/1.1817698 ; Du Pasquier (2009), Nano Ti - LiMn batteries with high power capability and improved cycle - life, Power Sources, 4, 186, doi.org/10.1016/J.Jpowsour.2008.10.018 ; Wegner (2003), Scale - up of nanoparticle synthesis in diffusion flame reactors, Chem Eng Sci, 58, doi.org/10.1016/J.Ces.2003.07.010 ; Groehn (2012), Fluid - particle dynamics during combustion spray aerosol synthesis of ZrO, Chem Eng J, 191, doi.org/10.1016/J.Cej.2012.02.093 ; Johannessen (2000), Computational fluid - particle dynamics for the flame synthesis of alumina particles, Chem Eng ci, 55, doi.org/10.1016/S0009-2509(99)00183-9 ; Waser (2011), Continuous flame aerosol synthesis of carbon - coated nano - LiFePO for Li - ion batteries, Aerosol Sci, 4, 42, doi.org/10.1016/J.Jaerosci.2011.06.003 ; Ernst (2007), Electrochemically active flame - made nanosized spinels : LiMn Ti and LiFe, Mater Chem Phys, 4, 4, doi.org/10.1016/j.matchemphys.2006.06.014 ; Armand (2008), Building better batteries, Nature, 451, doi.org/10.1038/451652a ; Mueller (2003), Nanoparticle synthesis at high production rates by flame spray pyrolysis, Chem Eng Sci, 58, doi.org/10.1016/s0009-2509(03)00022-8 ; Sotiriou (2010), Non - toxic dry - coated nanosilver for plasmonic biosensors, Adv Funct Mater, 20, doi.org/10.1002/Adfm.201000985 ; Curtet (1958), Confined jets and recirculation phenomena with cold air, Combust Flame, 2, doi.org/10.1016/0010-2180(58)90032-4 ; Padhi (1997), Phospho - olivines as positive - electrode materials for rechargeable lithium batteries, Electrochem Soc, 144, doi.org/10.1149/1.1837571 ; Olfe (1961), Mean beam length calculations for radiation from non - transparent gases, Quant Spectrosc Ra, 1, doi.org/10.1016/0022-4073(61)90022-X ; Teleki (2008), In situ coating of flame - made TiO particles with nanothin SiO films, Langmuir, 24, doi.org/10.1021/La801630z ; Gamba (2012), Residence time distribution determination of a continuous stirred tank reactor using computational fluid dynamics and its application on the mathematical modeling of styrene polymerization, Int J Chem React Eng, 10, 1, doi.org/10.1515/1542-6580.3057 ; Magnussen (1977), On mathematical modeling of turbulent combustion with special emphasis on soot formation and combustion, Symp Int Combust, 16, 719, doi.org/10.1016/S0082-0784(77)80366-4 ; Madler (2002), Controlled synthesis of nanostructured particles by flame spray pyrolysis, Aerosol Sci, 33, doi.org/10.1016/S0021-8502(01)00159-8 ; Krumeich (null), Thermal annealing dynamics of carbon - coated LiFePO nanoparticles studied by in - situ analysis State, Solid Chem, 2016, doi.org/10.1016/j.jssc.2016.07.002 ; Hsiao (2008), Microstructure effect on the electrochemical property of Ti as an anode material for lithium - ion batteries, Electrochim Acta, 4, 53, doi.org/10.1016/J.Electacta.2008.05.002 ; Groehn (2014), Scale - up of nanoparticle synthesis by flame spray pyrolysis : The high - temperature particle residence time, Ind Eng Chem Res, 53, doi.org/10.1021/Ie501709s ; Birozzi (2015), von Passerini Scaling up Ti for high - power lithium - ion anodes using large flame spray pyrolysis, nano Electrochem Soc, 4, 162, doi.org/10.1149/2.0711512jes ; Rudin (2011), Uniform nanoparticles by flame - assisted spray pyrolysis FASP of low cost precursors, Nanopart Res, 13, doi.org/10.1007/s11051-010-0206-x ; Streltsov (1993), Multipole analysis of the electron - density in triphylite using ray - diffraction data, Acta Crystallogr B, 4, 49, doi.org/10.1107/S0108768192004701 ; Strobel (2007), Flame aerosol synthesis of smart nanostructured materials, Mater Chem, 17, 4743, doi.org/10.1039/b711652g ; Laruelle (2002), On the origin of the extra electrochemical capacity displayed by MO / Li cells at low potential, Electrochem Soc, 149, doi.org/10.1149/1.1467947 ; Bresser (2012), The importance of going nano for high power battery materials, Power Sources, 219, doi.org/10.1016/J.Jpowsour.2012.07.035 ; Morrison (1997), In situ Fourier transform infrared characterization of the effect of electrical fields on the flame synthesis of TiO particles, Chem Mater, 9, 2702, doi.org/10.1021/cm960508u ; Madler (2002), Flame - made ceria nanoparticles, Mater Res, 17, doi.org/10.1557/jmr.2002.0202 ; Kavan (2003), Li insertion into Ti - Charge capability vs particle size in thin - film electrodes, Electrochem Soc, 4, 150, doi.org/10.1149/1.1581262 ; Asbrink (1970), A refinement of crystal structure of copper ( oxide with a discussion of some exceptional s Acta Crystall, B Stru, 26, 8. ; Strobel (2009), Direct synthesis of maghemite , magnetite and wustite nanoparticles by flame spray pyrolysis, Adv Powder Technol, 20, doi.org/10.1016/j.apt.2008.08.002 ; Zheng (2012), A comprehensive understanding of electrode thickness effects on the electrochemical performances of Li - ion battery cathodes, Electrochim Acta, 71, doi.org/10.1016/J.Electacta.2012.03.161 ; Waser (2013), Size controlled CuO nanoparticles for Li - ion batteries, Power Sources, 241, doi.org/10.1016/J.Jpowsour.2013.04.147

DOI

10.1515/cpe-2017-0005

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