In recent years, more and more attention has been paid to the quality of produced coal size categories for energy purposes. This is important from the perspective of promoting clean coal technologies which aim at changing the perception of coal as a fuel friendly for the environment. This is specifically because hard coal resources in Poland allow the national energy security to be guaranteed on the basis of energy production based on hard coal. Fine coals upgraded at coal processing facilities in the separation process in fine coal jigs are mainly used in energy production from coal. In the article, an analysis of hard coal upgrading in a jig regarding the optimum recovery of a useful fraction in the concentrate (combustible and volatile matter) and non-useful fraction in tailings (ash and sulfur) was conducted. Based on the industrial testing of a fine coal jig, the granulometric and densimetric analysis of the taken samples of concentrate, middlings and tailings of coal was conducted in laboratory conditions. Yields of products were calculated in separated size-fractions of separation products, and ash content and total sulfur content were determined in them. Based on the results of granulometric, densimetric and chemical analyses of the obtained size-fractions, the balance of separation products and appropriate calculations, Fuerstenau upgrading curves which allowed the process to be evaluated and a comparison of the results of hard coal upgrading regarding the optimum recovery of the organic phase in the concentrate and mineral components in tailings to be drawn. The obtained results were evaluated on the basis of different criteria for changing the device’s hydrodynamic operational conditions. The ash content and total sulfur content were analyzed as non-useful substances.