Ceramic injection moulding and gas pressure infiltration were employed for the manufacturing of alumina/AlSi10Mg composites. Porous ceramic preforms were prepared by mixing alumina powder with a multi-binder system and injection moulding of the powder polymer slurry. Then, the organic part was removed through a combination of solvent and thermal debinding, and the materials were finally sintered at different temperatures. The ceramic preforms manufactured in this way were infiltrated by an AlSi10Mg alloy. The microstructure and properties of the manufactured materials were examined using scanning electron microscopy, mercury porosimetry and bending strength testing. The results of transmission electron microscopy and scanning electron microscopy observations show that the fabricated composite materials are characterised by the percolation type of the microstructure and a lack of unfilled pores with good cohesion at the metal-ceramic interfaces. This is surprising considering that over 30% of the pores are smaller than 1 μm. The results show that the bending strength of the obtained composites decreased with increasing sintering temperature of the porous preforms.
In this study, a pilot-scale subsurface wastewater infiltration system (SWIS) was deployed to study landscape water treatment. The goal of the study was to investigate the effects of hydraulic loading on pollutant removal and the spatial distribution of biofilm properties in SWIS. Results showed that the efficiencies of chemical oxygen demand (COD), total nitrogen (TN) and total phosphorus (TP) removal degraded as hydraulic loading increased. Furthermore, quantities of the biofilm properties parameter s increased with the hydraulic loading. Polysaccharide and protein levels ranged from 560 to 1110 μg/g filler and 60 to 190 μg/g filler, respectively, at a hydraulic loading of 0.2 m/d. At a hydraulic loading of 0.4 m/d, the quantities of polysaccharide and protein ranged from 1200 to 3300 μg/g filler and 80 to 290 μg/g filler, respectively. Biofilm intensity and biofilm activity per unit weight decreased with the increase in hydraulic loading.
The paper presents a detailed description of one of the newest methods of vacuum saturation of reinforcing preforms in gypsum molds. As an appropriate selection of the infiltration time is a crucial problem during realization of this process, aim of the analysis shown in the paper is to present methods of selection of subatmospheric pressure application time, a sequence of lowering and increasing pressure, as well as examining influence of structure of reinforcing preforms on efficiency of this process. To realize the aim, studies on infiltration of reinforcing preforms made of a corundum sinter of various granulation of sintered particles with a model alloy were conducted. The infiltration process analysis was carried out in two stages. The first stage consisted in investigation of influence of lengthening of sucking off air from the reinforcing preforms on efficiency of this process. In the second stage, an analysis of influence of a two-staged infiltration process on saturation of the studied materials was conducted. Because the studied preforms were of similar porosity, the obtained differences of the saturation level of particular preforms have shown, that the saturation process is influenced mostly by size of pores present in the reinforcement. Because of these differences, each reinforcement type requires individual selection of time and sequence of the saturation process. For reinforcements of higher pore diameter, it is sufficient to simply increase air sucking off time to improve the saturation, while for reinforcement of smaller pore diameter, it is a better solution to apply the two-staged process of sucking off air. Application of the proposed analysis method allows not only obtaining composite castings of higher quality, but also economical optimization of the whole process.