In this article the structural and mechanical properties of grain refinement of Cu-Sn alloys with tin content of 10%, 15% and 20% using the KOBO method have been presented. The direct extrusion by KOBO (name from the combination of the first two letters of the names of its inventors – A. Korbel and W. Bochniak) method employs, during the course of the whole process, a phenomenon of permanent change of strain travel, realized by a periodical, two-sided, plastic metal torsion. Moreover the aim of this work was to study corrosion resistance. The microstructure investigations were performed using an optical microscope Olimpus GX71, a scanning electron microscope (SEM) and a scanning transmission electron microscope (STEM). The mechanical properties were determined with INSTRON 4505/5500 machine. Corrosion tests were performed using «Autolab» set – potentiostat/galvanostat from EcoChemie B.V. with GPES software ver. 4.9. The obtained results showed possibility of KOBO deformation of Cu-Sn casting alloys. KOBO processing contributed to the refinement of grains and improved mechanical properties of the alloys. The addition of tin significantly improved the hardness. Meanwhile, with the increase of tin content the tensile strength and yield strength of alloys decrease gradually. Ductility is controlled by eutectoid composition and especially δ phase, because they initiate nucleation of void at the particle/matrix interface. No significant differences in the corrosion resistance between cast and KOBO processed materials were found.
During excavation of the cremation cemetery of urnfield culture in Legnica at Spokojna Street (Lower Silesia, Poland), dated to 1100-700 BC, the largest - so far in Poland – a collection of casting moulds from the Bronze Age was discovered: three moulds for axes casting made out of stone and five moulds for casting sickles, razors, spearhead and chisels, made out of clay. This archaeological find constituted fittings of foundrymen’s graves. In order to perform the complete analysis of moulds in respect of their application in the Bronze Age casting technology analytical methods, as well as, computer aided methods of technological processes were used. Macroscopic investigations were performed and the X-ray fluorescence spectrometry method was used to analyse the chemical composition and metal elements content in mould cavities. Moulds were subjected to three-dimensional scanning and due to the reverse engineering the geometry of castings produced in these moulds were obtained. The gathered data was used to perform design and research works by means of the MAGMA5 software. Various variants of the pouring process and alloys solidification in these archaeological moulds were simulated. The obtained results were utilised in the interpretation of the Bronze Age casting production in stone and clay moulds, with regard to their quality and possibility of casting defects occurrence being the result of these moulds construction. The reverse engineering, modelling and computer simulation allowed the analysis of moulds and castings. Investigations of casting moulds together with their digitalisation and reconstruction of casting technology, confirm the high advancement degree of production processes in the Bronze Age.
The article presents the results of studies on the efficacy of water desalination (i.e. Elimination of NaCl ions from the solution) using graphene-polyamide composite membranes. The membrane used for filtration consists of a monolayer of polycrystalline graphene on a porous polyamide carrier support (nylon 66). The degree of desalination for an aqueous NaCl solution percolated through the membrane was 18%. In the future this type of membrane may replace the currently used reverse osmosis membranes.
The paper presents measurement results of standing wave ratio to be used as an efficiency indicator of microwave absorption by used moulding and core sands chosen for the microwave utilization process. The absorption measurements were made using a prototype stand of microwave slot line. Examined were five used moulding and core sands. It was demonstrated that the microwave absorption measurements can make grounds for actual microwave utilization of moulding and core sands.
The article takes into consideration the researches concerning inserting the Glassex additive to the microwaved-hardened and selfhardened moulding sands with water glass. In the research different types of ester hardeners to self-hardened moulding sands with water glass were used. The influence of Glassex additive on retained strength of moulding sands with different hardeners and prepared by different technologies of hardening were tested. The influence of different hardeners and the technology of hardening on retained strength of moulding sand with water glass and the Glassex additive were also estimated.