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The work presents the results of the experimental research concerning the impact of a heat treatment (toughening) of aluminum bronze CuAl10Fe4Ni4 on its mechanical properties. The conditions of the experiments and selected results are described. A detailed description of the effects of individual heat treatment conditions namely low and high temperature aging is also presented in the work.
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Improvement of Al-Si alloys properties in scope of classic method is connected with change of Si precipitations morphology through: using modification of the alloy, maintaining suitable temperature of overheating and pouring process, as well as perfection of heat treatment methods. Growing requirements of the market make it necessary to search after such procedures, which would quickly deliver positive results with simultaneous consideration of economic aspects. Presented in the paper shortened heat treatment with soaking of the alloy at temperature near temperature of solidus could be assumed as the method in the above mentioned understanding of the problem. Such treatment consists in soaking of the alloy to temperature of solutioning, keeping in such temperature, and next, quick quenching in water (20 0 C) followed by artificial ageing. Temperature ranges of solutioning and ageing treatments implemented in the adopted testing plan were based on analysis of recorded curves from the ATD method. Obtained results relate to dependencies and spatial diagrams describing effect of parameters of the solutioning and ageing treatments on HB hardness of the investigated alloy and change of its microstructure. Performed shortened heat treatment results in precipitation hardening of the investigated 320.0 alloy, what according to expectations produces increased hardness of the material.
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Mechanical and technological properties of castings made from 3xx.x alloys depend mainly on properly performed process of melting and casting, structure of a casting and mould, as well as possible heat treatment. Precipitation processes occurring during the heat treatment of the silumins containing additives of Cu and/or Mg have effect on improvement of mechanical properties of the material, while choice of parameters of solutioning and ageing treatments belongs to objectives of research work performed by a number of authors. Shortened heat treatment, which is presented in the paper assures suitable mechanical properties (Rm), and simultaneously doesn’t cause any increase of production costs of a given component due to long lasting operations of the solutioning and ageing. Results of the research concern effects of the solutioning and ageing parameters on the Rm tensile strength presented in form of the second degree polynomial and illustrated in spatial diagrams. Performed shortened heat treatment results in considerable increase of the Rm tensile strength of the 320.0 alloy as early as after 1 hour of the solutioning and 2 hours of the ageing performed in suitable.
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Secondary or multiple remelted alloys are common materials used in foundries. For secondary (recycled) Al-Si-Cu alloys, the major problem is the increased iron presence. Iron is the most common impurity and with presence of other elements in alloy creates the intermetallic compounds, which may negatively affect the structure. The paper deals with effect of multiple remelting on the microstructure of the AlS9iCu3 alloy with increased iron content to about 1.4 wt. %. The evaluation of the microstructure is focused on the morphology of iron-base intermetallic phases in caste state, after the heat treatment (T5) and after natural aging. The occurrence of the sludge phases was also observed. From the obtained results can be concluded that the multiple remelting leads to change of chemical composition, changes in the final microstructure and also increases sludge phases formation. The use of heat treatment T5 led to a positive change of microstructure, while the effect of natural aging is beneficial only to the 3rd remelting.
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Neodymium-Iron-Boron (Nd-Fe-B) magnets are considered to have the highest energy density, and their applications include electric motors, generators, hard disc drives, and MRI. It is well known that a fiber structure with a high aspect ratio and the large specific surface area has the potential to overcome the limitations, such as inhomogeneous structures and the difficulty in alignment of easy axis, associated with such magnets obtained by conventional methods. In this work, a suitable heat-treatment procedure based on single-step and multistep treatments to synthesize sound electrospun Nd-Fe-B-O nanofibers of Φ572 nm was investigated. The single-step heat-treated (directly heat-treated at 800°C for 2 h in air) samples disintegrated along with the residual organic compounds, whereas the multistep heat-treated (sequential three-step heat-treated including three steps;: dehydration (250°C for 30 min in an inert atmosphere), debinding (650°C for 30 min in air), and calcination (800°C for 1 h in air)) fibers maintained sound fibrous morphology without any organic impurities. They could maintain such fibrous morphologies during the dehydration and debinding steps because of the relatively low internal pressures of water vapor and polymer, respectively. In addition, the NdFeO3 alloying phase was dominant in the multistep heat-treated fibers due to the removal of barriers to mass transfer in the interparticles.
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The aim of this paper was to determine the effect of heat treatment for the corrosion resistance of the ZnAl40Ti2Cu alloy under “acid rain” conditions. ZnAl40TiCu alloy after supersaturation and after supersaturation and aging was studied. Potentiodynamic studies, potentiostatic studies and studies on structure of the alloy top layer of samples after corrosion tests were carried out. These investigations indicated a significant influence of heat treatment on corrosion resistance of the ZnAl40Ti2Cu alloy. The highest increase in corrosion resistance comparing to the alloy in the as-cast condition may be obtained by supersaturation. A significant influence of the aging temperature and time on corrosion resistance was proved.
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Heat treatment of a casting elements poured from silumins belongs to technological processes aimed mainly at change of their mechanical properties in solid state, inducing predetermined structural changes, which are based on precipitation processes (structural strengthening of the material), being a derivative of temperature and duration of solutioning and ageing operations. The subject-matter of this paper is the issue concerning implementation of a heat treatment process, basing on selection of dispersion hardening parameters to assure improvement of technological quality in terms of mechanical properties of a clamping element of energy network suspension, poured from hypoeutectic silumin of the LM25 brand; performed on the basis of experimental research program with use of the ATD method, serving to determination of temperature range of solutioning and ageing treatments. The heat treatment performed in laboratory conditions on a component of energy network suspension has enabled increase of the tensile strength Rm and the hardness HB with about 60-70% comparing to the casting without the heat treatment, when the casting was solutioned at temperature 520 o C for 1 hour and aged at temperature 165 o C during 3 hours.
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Very well-known advantages of aluminum alloys, such as low mass, good mechanical properties, corrosion resistance, machining-ability, high recycling potential and low cost are considered as a driving force for their development, i.e. implementation in new applications as early as in stage of structural design, as well as in development of new technological solutions. Mechanical and technological properties of the castings made from the 3xx.x group of alloys depend mainly on correctly performed processes of melting and casting, design of a mould and cast element, and a possible heat treatment. The subject-matter of this paper is elaboration of a diagrams and dependencies between parameters of dispersion hardening (temperatures and times of solutioning and ageing treatments) and mechanical properties obtained after heat treatment of the 356.0 (EN AC AlSi7Mg) alloy, enabling full control of dispersion hardening process to programming and obtaining a certain technological quality of the alloy in terms of its mechanical properties after performed heat treatments. Obtained results of the investigations have enabled obtainment of a dependencies depicting effect of parameters of the solutioning and ageing treatments on the mechanical properties (Rm, A5 and KC impact strength) of the investigated alloy. Spatial diagrams elaborated on the basis of these dependencies enable us to determine tendencies of changes of the mechanical properties of the 356.0 alloy in complete analyzed range of temperature and duration of the solutioning and ageing operations.
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Automation of machining operations, being result of mass volume production of components, imposes more restrictive requirements concerning mechanical properties of starting materials, inclusive of machinability mainly. In stage of preparation of material, the machinability is influenced by such factors as chemical composition, structure, mechanical properties, plastic working and heat treatment, as well as a factors present during machining operations, as machining type, cutting parameters, material and geometry of cutting tools, stiffness of the system: workpiece – machine tool – fixture and cutting tool. In the paper are presented investigations concerning machinability of the EN AC-AlSi9Cu3(Fe) silumin put to refining, modification and heat treatment. As the parameter to describe starting condition of the alloy was used its tensile strength Rm. Measurement of the machining properties of the investigated alloy was performed using a reboring method with measurement of cutting force, cutting torque and cutting power. It has been determined an effect of the starting condition of the alloy on its machining properties in terms of the cutting power, being indication of machinability of the investigated alloy. The best machining properties (minimal cutting power - Pc=48,3W) were obtained for the refined alloy, without heat treatment, for which the tensile strength Rm=250 MPa. The worst machinability (maximal cutting power Pc=89,0W) was obtained for the alloy after refining, solutioning at temperature 510 o C for 1,5 hour and aged for 5 hours at temperature 175 o C. A further investigations should be connected with selection of optimal parameters of solutioning and ageing treatments, and with their effect on the starting condition of the alloy in terms of improvement of both mechanical properties of the alloy and its machining properties, taking into consideration obtained surface roughness.
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This article presents the results of investigations of the effect of heat treatment temperature on the content of the carbide phase of HS3-1-2 and HS6-5-2 low-alloy high-speed steel. Analysis of the phase composition of carbides is carried out using the diffraction method. It is determined that with increasing austenitising temperature, the intensification of dissolution of M6C carbide increases. As a result, an increase in the grain size of the austenite and the amount of retained austenite causes a significant reduction in the hardness of hardened steel HS3-1-2 to be observed. The results of diffraction investigations showed that M7C3 carbides containing mainly Cr and Fe carbides and M6C carbides containing mainly Mo and W carbides are dissolved during austenitisation. During austenitisation of HS3-1-2 steel, the silicon is transferred from the matrix to carbides, thus replacing carbide-forming elements. An increase in a degree of tempering leads to intensification of carbide separation and this process reduce the grindability of tested steels.
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Within the presented research, effect of annealing on nature of corrosion damages of medium-nickel austenitic nodular cast iron castings, containing 5.5% to 10.3% Ni, was determined. Concentration of nickel, lower than in the Ni-Resist cast iron, was compensated with additions of other austenite-stabilising elements (manganese and copper). In consequence, raw castings with austenitic matrix structure and gravimetrically measured corrosion resistance increasing along with nickel equivalent value EquNi were obtained. Annealing of raw castings, aimed at obtaining nearly equilibrium structures, led to partial austenite-to-martensite transformation in the alloys with EquNi value of ca. 16%. However, corrosion resistance of the annealed alloys did not decrease in comparison to raw castings. Annealing of castings with EquNi value above 18% did not cause any structural changes, but resulted in higher corrosion resistance demonstrated by smaller depth of corrosion pits.
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The paper presents research on the effects of soft annealing parameters on a change of the impact strength KC and Brinell hardness (HB) of the EN AC-AlSi11 alloy. The research has been performed according to the trivalent testing plan for two input parameters – temperature in the range between 280°C and 370°C and time in the range between 2 and 8 hours. The application of such heat treatment improves the plasticity of the investigated alloy. The improvement of the impact strength KC by 71% and the decrease of the hardness HB by 20% was achieved for the soft annealing treatment conducted at a temperature 370°C for 8 hours, compared to the alloy without the heat treatment. A change of the form of eutectic silicon precipitations which underwent refinement, coagulation and partial rounding, had a direct effect on the hardness HB and impact strength KC. The results obtained were used to prepare space plots enabling the temperature and time for soft annealing treatment to be selected with reference to the obtained impact strength KC and hardness HB of the alloy with the heat treatment.
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Al- and Al/Zn-enriched layers containing intermetallic phases were deposited on the Mg substrate by heating the Mg specimens in contact with the powdered materials in a vacuum furnace. The Al-enriched surface layers were produced using Al powder, whereas the Al/Znenriched layers were obtained from an 80 wt.% Al + 20 wt.% Zn powder mixture. The microstructure and composition of the layers were analyzed by optical microscopy, scanning electron microscopy and X-ray diffraction. The results showed that the Al-enriched layer comprised an Mg17Al12 intermetallic phase and a solid solution of Al in Mg. The layer obtained from the Al+Zn powder mixture was composed of Mg-Al-Zn intermetalic phases and a solid solution of Al and Zn in Mg. Adding 20% of Zn into the Al powder resulted in the formation of a considerably thicker layer. Moreover, the hardness of the surface layers was much higher than that of the Mg substrate.
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The experimental material consisted of semi-finished products of high-grade, medium-carbon constructional steel with: manganese, chromium, nickel, molybdenum and boron. The experimental material consisted of steel products obtained in three metallurgical processes: electric and desulfurized (E), electric and desulfurized with argon-refined (EA) and oxygen converter with vacuum degassed of steel (KP). The production process involved two melting technologies: in a 140-ton basic arc furnace with desulphurisation and argon refining variants, and in a 100-ton oxygen converter. Billet samples were collected to analyze: relative volume of impurities, microstructure and fatigue tests. The samples were quenched and austenitized at a temperature of 880o C for 30 minutes. They were then cooled in water and tempered by holding the sections at a temperature of 200, 300, 400, 500 and 600o C for 120 minutes and air-cooled. Fatigue tests were performed with the use of a rotary bending machine at a frequency of 6000 cpm. The results were statistical processed and presented in graphic form. This paper discusses the results of microstructural analyses, the distribution of the relative volume of impurities in different size ranges, the fatigue strength characteristics of different production processes, the average number of sampledamaging cycles and the average values of the fatigue strength coefficient for various heat processing options.
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This article discusses the influence of Tungsten Inert Gas (TIG) surfacing of duplex cast steel on its hardness and structure. The samples of 24Cr-5Ni-2.5Mo ferritic-austenitic cast steel were subjected to single-overlay processes with the use of solid wire having the chemical composition similar to that of the duplex cast steel. As a result of the surfacing, the welds were obtained that had no welding imperfections with a smooth transition to the base material. In the test without the heat treatment, directly below the fusion line, we observe a ferrite band with a width of approximately 200 m without visible austenite areas. Some of the samples were then solution treated (1060°C). Both variants, without and after solution heat treatment, were subjected to testing. Significant changes in the microstructure of the joint were observed after the heat treatment process (heat affected zone and weld microstructure changes). In both areas, an increase in the austenite volume fraction after solution heat treatment was observed. Changes in the microhardness of the ferrite in the HAZ area directly below the fusion line were also observed.
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The most important parameters which predetermine mechanical properties of a material in aspects of suitability for castings to machinery components are: tensile strength (Rm), elongation (A5, hardness (HB) and impact strength (KCV). Heat treatment of aluminum alloys is performed to increase mechanical properties of the alloys mainly. The paper comprises a testing work concerning effect of heat treatment process consisting of solution heat treatment and natural ageing on mechanical properties and structure of AlZn10Si7MgCu alloy moulded in metal moulds. Investigated alloy was melted in an electric resistance furnace. Run of crystallization was presented with use of thermal-derivative method (ATD). This method was also implemented to determination of heat treatment temperature ranges of the alloy. Performed investigations have enabled determination of heat treatment parameters’ range, which conditions suitable mechanical properties of the investigated alloy. Further investigations will be connected with determination of optimal parameters of T6 heat treatment of the investigated alloy and their effect on change of structure and mechanical/technological properties of the investigated alloy.
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Dispersion hardening, as the main heat treatment of silumins having additions of copper and magnesium, results in considerable increase of tensile strength and hardness, with simultaneous decrease of ductility of the alloy. In the paper is presented an attempt of introduction of heat treatment operation consisting in homogenizing treatment prior operation of the dispersion hardening, to minimize negative effects of the T6 heat treatment on plastic properties of hypereutectoidal AlSi17CuNiMg alloy. Tests of the mechanical properties were performed on a test pieces poured in standardized metal moulds. Parameters of different variants of the heat treatment, i.e. temperature and time of soaking for individual operations were selected basing on the ATD (Thermal Derivation Analysis) diagram and analysis of literature. The homogenizing treatment significantly improves ductility of the alloy, resulting in a threefold increase of the elongation and more than fourfold increase of the impact strength in comparison with initial state of the alloy. Moreover, the hardness and the tensile strength (Rm) of the alloy decrease considerably. On the other hand, combination of the homogenizing and dispersion hardening enables increase of elongation with about 40%, and increase of the impact strength with about 25%, comparing with these values after the T6 treatment, maintaining high hardness and slight increase of the tensile strength, comparing with the alloy after the dispersion hardening
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Mg-0.5Si-xSn (x=0.95, 2.9, 5.02wt.%) alloys were cast and extruded at 593K (320 ºC) with an extrusion ratio of 25. The microstructure and mechanical properties of as-cast and extruded test alloys were investigated by OM, SEM, XRD and tensile tests. The experimental results indicate that the microstructure of the Mg-0.5Si-xSn alloys consists of primary α-Mg dendrites and an interdendritic eutectic containing α-Mg, Mg2Si and Mg2Sn. There is no coarse primary Mg2Si phase in the test alloys due to low Si content. With the increase in the Sn content, the Mg2Si phase was refined. The shape of Mg2Si phase was changed from branch to short bar, and the size of them were reduced. The ultimate tensile strength and yield strength of Mg-0.52Si-2.9Sn alloy at the temperature of 473K (200 ºC) reach 133MPa and 112MPa respectively. Refined eutectic Mg2Si phase and dispersed Mg2Sn phase with good elevated temperature stability are beneficial to improve the elevated temperature performance of the alloys. However, with the excess addition of Sn, large block-like Mg2Sn appears around the grain boundary leading to lower mechanical properties.
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The work presents experiment results from the area of copper casting technology and chosen examples of alloyed copper. At present, copper casting technology is applied in many branches of industrial manufacturing, especially in the sector of construction, communications, arms and power engineering. Alloyed copper, containing slight additions of different elements and having special physio-chemical properties, is used in a special range of applications. Copper technology and alloyed copper analyses have been presented, these materials being used for cast manufacturing for power engineering. The quality of casts has been assessed, based on their microstructure analysis, chemical content and the cast properties. During the research, special deoxidizing and modifying agents were applied for copper and chosen examples of alloyed copper; also exemplary samples were tested with the help of metallographic analysis, electrical conductivity and gaseous impurities research.
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The paper attempts to analyze distortions of cast iron and cast steel rings, after heat treatment cycles. The factors influencing distortion are: chemical composition of material, sample geometry, manufacturing process, hardenability, temperature and heat treatment method. Standard distortion tests are performed on C-ring samples. We selected a ring-model, which approximate the actual part, so that findings apply to gear rings. Because distortion depends on so many variables, this study followed strictly defined procedures. The research was started by specifying the appropriate geometry of the samples. Then, the heat treatment was conducted and samples were measured again. The obtained results allow to determine the value of the resulting distortion and their admissibility. The research will be used to evaluate the possibility of using the material to produce parts of equipment operated under extreme load conditions.
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One type of spheroidal cast iron, with additions of 0.51% Cu and 0.72% Ni, was subjected to precipitation hardening. Assuming that the greatest increase in hardness after the shortest time of ageing is facilitated by chemical homogenisation and fragmentation of cast iron grain matrix, precipitation hardening after pre-normalisation was executed. Hardness (HB), microhardness (HV), qualitative and quantitative metalographic (LM, SEM) and X-ray structural (XRD) tests were performed. The acquired result of 13.2% increase in hardness after ca. 5-hour ageing of pre-normalised cast iron confirmed the assumption.
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The paper deals with influence of multiple remelting on AlSi9Cu3 alloy with higher iron content on chosen mechanical properties. Multiple remelting may in various ways influence mechanical, foundry properties, gas saturation, shrinkage cavity, fluidity etc. of alloy. Higher presence of iron in Al-Si cast alloys is common problem mainly in secondary (recycled) aluminium alloys. In Al-Si alloy the iron is the most common impurity and with presence of other elements in alloy creates the intermetallic compounds, which decreases mechanical properties. Iron in the used alloy was increased to about 1.4 wt. %, so that the influence of increased iron content can be investigated. In the paper, the effect of multiple remelting is evaluated with respect to the resulting mechanical properties in cast state, after the heat treatment (T5) and after natural aging. From the obtained results it can be concluded that the multiple remelting leads to change of chemical composition and affect the mechanical properties.
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Grey cast iron belongs to materials for casting production, which have wide application for different industry branches. Wide spectrum of properties of these materials is given by the structure of base metal matrix, which can be influenced with heat treatment. Processes of annealing can be applied for grey cast iron without problems. During heat treatment processes, where higher cooling rates are used, the thermal and structural strains become important. Usage and conditions of such heat treatment for grey cast iron castings of common production are the subject of evaluation of this article.
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AZ91 alloy was cast in a steel mould pre-exposed to three different temperatures: -196 ºC, 20 ºC and 650 ºC. The aim of the study was to determine the difference in the microstructure and mechanical properties between the castings formed in a cold mould and those solidifying under near-equilibrium conditions in a mould pre-heated to 650 ºC. Solidification at a low temperature led to dispersion of the structure elements as well as supersaturation of the solid solution of aluminium in magnesium. The heat treatment results indicate that the alloy solidified in the mould pre-exposed to 20 ºC can be successfully aged (heat treated to the T5 temper). It was found that the effect of the ageing process (T5 temper) was greater than the effect of the microstructure fragmentation, which was due to rapid solidification. The ageing results were assessed by comparing the microstructure and mechanical properties of AZ91 brought to the T5 condition with those obtained for the material in the T6 condition.
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The article shows a new model of Continuous Cooling Transformation (CCT) diagrams of structural steels and engineering steels. The modelling used artificial neural networks and a set of experimental data prepared based on 550 CCT diagrams published in the literature. The model of CCT diagrams forms 17 artificial neural networks which solve classification and regression tasks. Neural model is implemented in a computer software that enables calculation of a CCT diagram based on chemical composition of steel and its austenitizing temperature.
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