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Abstract

Sodium silicate is one of the most successful inorganic binder. Along with the broad application of sodium silicate for domestic and industrial purposes, the composition analysis, include modulus (m), ratio of SiO2:Na2O, Na2O%, SiO2%, and solid-containing content, is important for the products strength and service life. However, it is perplexing to operate, inefficient and low precision for traditional standard testing method of these parameters. In this study, an automatic measurement system of sodium silicate composition analysis, with the potential electrode for potentiometer titration, micro-controller, PCB, heater, stirrer, printer and micro peristaltic pump, was developed according to the determine method principle. The end-points of pH value in the two titrating steps, first was 4.3 and second was 6.0, were set in the micro-controller to control the reaction in the processing of the sodium silicate composition analysis. And all the potential signals of the pH electrode were transited in the special PCB for the micro-controller.
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Bibliography

[1] Rabbii, A. (2001). Sodium silicate glass as an inorganic binder in foundry industry. Iranian Polymer Journal. 10(4), 229-235.
[2] Stachowicz, M., Pałyga, Ł.& Kȩpowicz, D. (2020). Influence of automatic core shooting parameters in hot-box technology on the strength of sodium silicate olivine moulding sands. Archives of Foundry Engineering. 20(1), 67-72.
[3] Huafang, W., Wenbang, G. & Jijun, L. (2014). Improve the humidity resistance of sodium silicate sands by estermicrowave composite hardening. Metalurgija. 53(4), 455-458.
[4] Nowak, D. (2017). The impact of microwave penetration depth on the process of heating the moulding sand with sodium silicate. Archives of Foundry Engineering. 17(4), 115-118.
[5] M. Stachowicz, K. Granat, & D. Nowak. (2011). Application of microwaves for innovative hardening of environment-friendly water-glass moulding sands used in manufacture of cast-steel castings. Archives of Civil and Mechanical Engineering. XI(1), 209-219.
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[7] Masuda Yuki, Tsubota Keiji, Ishii Kenichi, Imakoma Hironobu, Ohmura Naoto. (2009) Drying rate and surface temperature in solidification of glass particle layer with inorganic binder by microwave drying. Kagaku Kogaku Ronbunshu. 35(2). 229-231.
[8] Standardization Administration of the P.R.C. (2008). GB/T4209-2008, Sodium silicate for industry use[S]. Beijing, China Standard Press.
[9] Bourikas K., Kordulis C. & Lycourghiotis A. (2005). Differential potentiometric titration: Development of a methodology for determining the point of zero charge of metal (Hydr)oxides by one titration curve. Environmental Science & Technology. 39(11), 4100-4108.
[10] Fan ZT, Liu M, Wang HF, Long W, Hu XT. (2010). Chinese Patent No. 201010558029.3. Beijing, China National Intellectual Property Administration.
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Authors and Affiliations

Huafang Wang
1
ORCID: ORCID
Quanrun Wang
1
Wu Zhang
1
Xiang Gao
1
Jijun Lu
1
ORCID: ORCID

  1. School of Mechanical Engineering and Automation, Wuhan Textile University, Wuhan 430073, China

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