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Abstract

We present the results of investigations of Pb(Fe1/2Nb1/2)O3 (PFN) ceramic samples obtained using two-step synthesis (i.e. columbite method). For obtained samples complex investigations of microstructure, magnetic and electrophysical properties have been performed at low and at high temperatures. Microstructure is characterized by small grains with high homogeneity and high density (low porosity). Impedance of samples and the phase shift angle have been measured using LCR Meter. Next the AC electric conductivity, dielectric permittivity and loss tangent have been calculated. AC conductivity at frequency 3 Hz was measured in similar way using Quantum Design PPMS System in magnetic fields 1000 Oe and 10000 Oe. At temperature range 240K-260K the anomalies of conductivity are observed. These anomalies depend on measuring cycle (heating, cooling) and magnetic field.

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Authors and Affiliations

D. Bochenek
R. Skulski
P. Niemiec
D. Brzezińska
K. Rogacki
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Abstract

The Fe-based alloy with manganese led to the appearance of new austenitic alloys, with the antiferromagnetic property pursued, resulting in compatibility with the magnetic field as that of magnetic resonance imaging. The corrosion resistance behavior of the biodegradable Fe-Mn-Si alloy was analyzed in a thermostatic chamber at 37±1°C for 24, 48 and 72 hours by immersing in Ringer solution. Also, the cast and laminated samples were subjected to electro-corrosion tests using a potentiostat equipment. Linear and cyclic potentiometry is presented for characterize the corrosion behavior of the experimental samples in electrolyte. Due to the interaction between the alloy and the liquid medium a change in the solution pH was observed. Structure analysis and chemical composition details of the surfaces were obtained using electron scanning microscopy (SEM) and X-ray energy dispersive spectroscopy (EDS).
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Authors and Affiliations

A.-M. Roman
1
ORCID: ORCID
R. Chelariu
1
ORCID: ORCID
R. Cimpoesu
1
ORCID: ORCID
I. Stirbu
1
ORCID: ORCID
I. Ionita
1
ORCID: ORCID
M.M. Cazacu
2
ORCID: ORCID
B.A. Prisecariu
3
ORCID: ORCID
N. Cimpoesu
3
ORCID: ORCID
P. Pietrusiewicz
4
ORCID: ORCID
A. Sodor
3
ORCID: ORCID

  1. Faculty of Materials Science and Engineering, “Gheorghe Asachi” Technical University of Iasi, Prof.dr.doc. D. Mangeron no. 41 Street, 700050 Iasi, Romania
  2. “Gheorghe Asachi” Technical University of Iasi, Department of Physics, 700050 Iasi, Romania
  3. “Grigore T. Popa” University of Medicine and Pharmacy of Iasi, 16 Univ. Street, 700115 Iasi, Romania
  4. Częstochowa University of Technology, Department of Physics , 42-200 Częstochowa, Poland

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