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Number of results: 3
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Abstract

The effect of additions of silver or titanium (0.5 or 3 vol.%) microparticles on the microstructure, as well as some physical properties of Al2O3-based composites, were studied. The processing method for the manufacturing of alumina-based composites was a combination of RBAO and SPS processes. After the SPS process, bodies with almost full density were obtained. Observations by optical microscopy show a very fine and homogenous microstructure in all samples. Concerning mechanical properties, the addition of metals on alumina increases its fracture toughness significantly (112% for the sample with additions of silver, while the composite with additions of titanium fracture toughness increases by 72%). In terms of optical properties, both silver and titanium improve the absorbance in the visible range.
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Authors and Affiliations

Enrique Rocha-Rangel
1
ORCID: ORCID
Carlos A. Calles-Arriaga
1
ORCID: ORCID
Juan López-Hernández
1
ORCID: ORCID
José A. Rodríguez-García
1
ORCID: ORCID

  1. Universidad Politécnica de Victoria, Ciudad Victoria, México
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Abstract

Through the powder metallurgy technique, alloys of the eutectic composition of the Zn-Al system were manufactured (22.3 wt.%Al), reinforced with Ag additions (0.5, 1, 2.5, 5 wt.%), with subsequent annealing heat treatment at three different temperatures; 100, 150 and 200°C for 1 hr. X-ray diffraction, optical microscopy and mechanical tests were performed on the resulting samples. The addition of Ag favors the formation of alpha and beta compounds with Al and Zn respectively, which improves the compressive strength of the alloy. However, with the presence of Ag the hardness is decreased. On the other hand, the application of an annealing heat treatment, shows no significant effect on the evaluated properties of the alloy. The microstructure of the alloys resulted in the presence of very small grains smaller than 1 mm and with rounded morphology.
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Authors and Affiliations

Miguel Angel Rubio-Padrón
1
ORCID: ORCID
Olga Alondra Echartea-Reyes
1
Carlos A. Calles-Arriaga
1
ORCID: ORCID
Enrique Rocha-Rangel
1
ORCID: ORCID

  1. Universidad Politécnica de Victoria, Ciudad Victoria, México
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Abstract

A SrTiO3 electroceramic with perovskite structure was produced by the calcination of a mixture of SrCO3 and TiO2 intensively grounded by high energy milling. For this purpose, raw materials were mixed in stoichiometric amounts in a planetary type mill; the obtained powder mixture was calcined for 2 h at temperatures between 800 and 1300°C. Samples resulting from the calcination were characterized by XRD, FTIR, SEM analysis and electrical measurements. From XRD, it was determined that the SrTiO3 formed presents the cubic structure of perovskite. The complete reaction for SrTiO3 compound formation occurs at 1200°C. Micrograph observations indicate the presence of a homogeneous microstructure with tiny grain size. The measured values of electrical resistivity were within the typical range of insulating materials.

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Authors and Affiliations

Enrique Rocha-Rangel
ORCID: ORCID
Wilian J. Pech-Rodríguez
Juan López-Hernández
ORCID: ORCID
Carlos A. Calles-Arriaga
ORCID: ORCID
Eddie N. Armendáriz-Mireles
José A. Castillo-Robles
José A. Rodríguez-García
ORCID: ORCID

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