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Number of results: 7
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Abstract

The paper presents the microstructure and selected properties of ausferritic nodular cast iron annealed at the temperature 520 and 550°C.

This choice was dictated by the temperatures used in the practice of nitriding. Nodular graphite in cast iron was obtained with use of

Inmold process. Cast iron containing molybdenum and copper ensuring obtaining an ausferrite in the cast iron matrix without the use of

heat treatment of castings was tested. The effect of annealing temperature on the microstructure and the kind of fracture of the ausferritic

nodular cast iron was presented. The effect of an annealing temperature on hardness, impact strength and the microhardness of ausferritic

nodular cast iron matrix was shown too. The lamellar structure of phases in the cast iron matrix after annealing has been ascertained. There

has been an increase in hardness of an annealed cast iron and microhardness of its matrix. The reduction in the impact strength of the cast

iron annealed at 520 and 550°C was approximately 10-30%. Both an increase in the hardness of cast iron as well as an decrease in its

impact strength is probably due to the separation of secondary carbides during the heat treatment.

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Authors and Affiliations

G. Gumienny
L. Klimek
B. Kurowska
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Abstract

The aim of these studies was to obtain single phase cubic modification of Li7La3Zr2O12 by mechanical milling and annealing of La(OH)3, Li2CO3 and ZrO2 powder mixture. Fritsch P5 planetary ball mill, Rigaku MiniFlex II X-ray diffractometer, Setaram TG-DSC 1500 analyser and FEI Titan 80-300 transmission electron microscope were used for sample preparation and investigations. The applied milling and annealing parameters allowed to obtain the significant contribution of c-Li7La3Zr2O12 in the sample structure, reaching 90%. Thermal measurements revealed more complex reactions requiring further studies.

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Authors and Affiliations

D. Oleszak
B. Kurowski
T. Pikula
M. Pawlyta
M. Senna
H. Suzuki
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Abstract

The paper presents the effect of tin on the crystallization process, microstructure and hardness of cast iron with compacted (vermicular) graphite. The compacted graphite was obtained with the use of magnesium treatment process (Inmold technology). The lack of significant effect of tin on the temperature of the eutectic transformation has been demonstrated. On the other hand, a significant decrease in the eutectoid transformation temperature with increasing tin concentration has been shown. It was demonstrated that tin narrows the temperature range of the austenite transformation. The effect of tin on the microstructure of cast iron with compacted graphite considering casting wall thickness has been investigated and described. The carbide-forming effect of tin in thin-walled (3 mm) castings has been demonstrated. The nomograms describing the microstructure of compacted graphite iron versus tin concentration have been developed. The effect of tin on the hardness of cast iron was given.

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Authors and Affiliations

Grzegorz Gumienny
ORCID: ORCID
B. Kurowska
ORCID: ORCID
P. Fabian
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Abstract

The paper presents the effect of manganese on the crystallization process, microstructure and selected properties: cast iron hardness as well as ferrite and pearlite microhardness. The compacted graphite was obtained by Inmold technology. The lack of significant effect on the temperature of the eutectic transformation was demonstrated. On the other hand, a significant reduction in the eutectoid transformation temperature with increasing manganese concentration has been shown. The effect of manganese on microstructure of cast iron with compacted graphite considering casting wall thickness was investigated and described. The nomograms describing the microstructure of compacted graphite iron versus manganese concentration were developed. The effect of manganese on the hardness of cast iron and microhardness of ferrite and pearlite were given.

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Authors and Affiliations

Grzegorz Gumienny
ORCID: ORCID
B. Kurowska
ORCID: ORCID
P. Just
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Abstract

We present Al2O3-ZnAl2O4-ZnO nanostructure, which could be a prominent candidate for optoelectronics, mechanical and sensing applications. While ZnO and ZnAl2O4 composites are mostly synthesized by sol-gel technique, we propose a solid-vapor growth mechanism. To produce Al2O3-ZnAl2O4-ZnO nanostructure, we conduct ZnO:C powder heating resulting in ZnO nanowires (NWs) growth on sapphire substrate and ZnAl2O4 spinel layer at the interface. The nanostructure was examined with Scanning Electron Microscopy (SEM) method. Focused Ion Beam (FIB) technique enabled us to prepare a lamella for Transmission Electron Microscopy (TEM) imaging. TEM examination revealed high crystallographic quality of both spinel and NW structure. Epitaxial relationships of Al2O3-ZnAl2O4 and ZnAl2O4-ZnO are given.
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Authors and Affiliations

W. Zajkowska-Pietrzak
1
ORCID: ORCID
J. Turczyński
1
ORCID: ORCID
B. Kurowska
1
ORCID: ORCID
H. Teisseyre
1
ORCID: ORCID
K. Fronc
1
ORCID: ORCID
J. Dąbrowski
1
ORCID: ORCID
S. Kret
1
ORCID: ORCID

  1. Institute of Physics Polish Academy of Sciences, 32/46 Lotników Av., 02-668 Warszawa, Poland

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