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Abstract

In this work, the effect of heat transfer during explosive welding (EXW) and post-processing annealing on the microstructural and chemical composition changes have been thoroughly analysed using scanning and transmission electron microscopies and X-ray synchrotron radiation. Several combination of explosively welded metal compositions were studied: Ti with Al, Cu with Al, Ta or stainless steel, stainless steel with Zr or Ta and Ti with carbon steel. It was found that the melted metals exhibit a strong tendency to form brittle crystalline, nano-grained or even amorphous phases during the solidification. For all analysed metal combinations most of the phases formed in the zones of solidified melt do not appear in the equilibrium phase diagrams. Concurrently, the interfacial layers undergo severe plastic deformation forming nano-grained structures. It has been established that these heavily deformed areas can undergo dynamic recovery and recrystallization already during clad processing. This leads to the formation of new stress-free grains near the interface. In the case of low temperature and short time post processing annealing only the melted zones and severely deformed layers undergo recovery and recrystallization. However, drastic changes in the microstructure occurs at higher temperature and for longer annealing times. Applying such conditions leads to diffusion dominant processes across the interface. As a consequence continuous layers of intermetallic phases of equilibrium composition are obtained.

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Authors and Affiliations

H. Paul
M.M. Miszczyk
A. Gałka
R. Chulist
Z. Szulc
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Abstract

In this paper, the microstructural and texture changes in polycrystalline CuZn30 alloy, copper, and AA1050 aluminium alloy have been studied to describe the crystal lattice rotation during shear bands formation. The hat-shaped specimens were deformed using a drop-hammer at the strain rate of 560 s –1. Microstructure evolution was investigated using optical microscopy, whereas texture changes were examined with the use of a scanning electron microscope equipped with the EBSD facility. The microstructural observations were correlated with nanohardness measurements to evaluate the mechanical properties of the sheared regions. The analyses demonstrate the gradual nature of the shear banding process, which can be described as a mechanism of the bands nucleation and then successive growth rather than as an abrupt instability. It was found that regardless of the initial orientation of the grains inside the sheared region, a well-defined tendency of the crystal lattice rotation is observed. This rotation mechanism leads to the formation of specific texture components of the sheared region, different from the one observed in a weakly or non-deformed matrix. During the process of rotation, one of the {111} planes in each grain of the sheared region ‘tends’ to overlap with the plane of maximum shear stresses and one of the <110> or <112> directions align with the shear direction. This allows slip propagation through the boundaries between adjacent grains without apparent change in the shear direction. Finally, in order to trace the rotation path, transforming the matrix texture components into shear band, rotation axis and angles were identified.
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Authors and Affiliations

I. Mania
1
ORCID: ORCID
H. Paul
1
ORCID: ORCID
R. Chulist
1
ORCID: ORCID
P. Petrzak
1
ORCID: ORCID
M. Miszczyk
1
ORCID: ORCID
M. Prażmowski
2
ORCID: ORCID

  1. Polish Academy of Sciences, Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Krakow, Poland
  2. Opole University of Technology, Faculty of Mechanics, 76 Prószkowska Str., 45-758 Opole, Poland

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