The study presents the results of research on the development of composite zones in castings based on the intermetallic phase of Ni3Al. Composite zones were obtained by placing packets with substrates for the reaction of titanium carbide in a foundry mould. To provide a variable carbides content in the composite zone, two compositions of the packets were prepared. The first packet contained only substrates for the reaction of TiC synthesis; the second one also contained a filler. The resulting composite zones in castings were examined for the filler effect on changes in the volume fraction, size and morphology of carbides in the zone. In addition, the effect of filler on the mechanical properties of the zone was verified, observing changes of Vickers hardness in this area. It was found that the presence of filler in the composition of the packet for synthesis reduced the content of carbides, as well as their size and morphology. Lower surface content of carbides reduced hardness of the zone, which enabled smooth control of the mechanical properties. At the same time, the use of the selected filler did not disturb the course of the TiC carbide synthesis.

In the aluminium alloy family, Al-Zn materials with non-standard chemical composition containing Mg and Cu are a new group

of alloys, mainly owing to their high strength properties. Proper choice of alloying elements, and of the method of molten metal treatment

and casting enable further shaping of the properties. One of the modern methods to produce materials with submicron structure is a method

of Rapid Solidification. The ribbon cast in a melt spinning device is an intermediate product for further plastic working. Using the

technique of Rapid Solidification it is not possible to directly produce a solid structural material of the required shape and length.

Therefore, the ribbon of an ultrafine grain or nanometric structure must be subjected to the operations of fragmentation, compaction,

consolidation and hot extrusion.

In this article the authors focussed their attention on the technological aspect of the above mentioned process and described successive

stages of the fabrication of an AlZn9Mg2.5Cu1.8 alloy of ultrafine grain structure designated for further plastic working, which enables

making extruded rods or elements shaped by the die forging technology. Studies described in the article were performed under variable

parameters determined experimentally in the course of the alloy manufacturing process, including casting by RS and subsequent

fragmentation.