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Number of results: 7
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Abstract

Noise diagnostics has been performed on the cold field-emission cathode in high-vacuum. The tested cold field-emission cathode, based on tungsten wire with ultra-sharp tip coated by epoxy was designed to meet the requirements of transmission electron microscopy, which uses a small and stable source of electrons. Current fluctuations are reduced by improving the structure and fabrication technology. Noise was measured both in time and frequency domains, which gives information about current fluctuations and also about charge transport. Mutual correlation between the noise spectral density, extractor voltage and beam brightness was analyzed.

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Authors and Affiliations

Alexandr Knápek
Lubomír Grmela
Josef Šikula
Ondřej Šik
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Abstract

The paper deals with the preparation and measurement of an experimental polymer graphite cathode that

seems to be a promising and cheap source of electrons utilizing cold field-emission in high- and ultra-high

vacuum. Polymer graphite seems to be a proper material as it contains a large amount of hybridized carbon

with a low degree of surface oxidation and silicon monoxide (SiO). Within the frame of this work, a special

experimental method of tip preparation has been designed and tuned. This method is based on ion milling

inside a dual-beam electron microscope enabling to obtain ultra-sharp tips of a diameter smaller than 100 nm

with a predefined opening angle. The charge transport within experimental samples is evaluated based on

results provided by the noise spectroscopy of the total emission current in the time and frequency domains.

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Authors and Affiliations

Alexandr Knápek
Miroslav Horáček
Jana Chlumská
Tomáš Kuparowitz
Dinara Sobola
Josef Šikula
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Abstract

Samples of CdTe single crystals which are used as radiation detectors were periodically measured during a long time interval with different values of an applied voltage. The samples were also periodically exposed during long time periods to high temperatures of 390 K and to rapid changes of temperature from 300 K to 390 K. After 1.5 years of measurements we observed ageing of the samples which resulted in deterioration of their transport characteristics. The resistance of the samples increased significantly and current-voltage characteristics were unstable in time. Noise spectroscopy showed that low frequency noise can be used for detection of CdTe sample ageing as its spectral density increases significantly comparing to the 1/f noise of a high quality sample

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Authors and Affiliations

Lubomír Grmela
Ondřej Šik
Alexey Andreev
Josef Sikula
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Abstract

Specimens of Si single crystals with different crystal orientation [100] and [110] were studied by Electro-Ultrasonic Spectroscopy (EUS) and Resonant Ultrasonic Spectroscopy (RUS). A silicon single crystal is an anisotropic crystal, so its properties are different in different directions in the material relative to the crystal orientation. EUS is based on interaction of two signals: an electric AC signal and an ultrasonic signal, which are working on different frequencies. The ultrasonic wave affects the charge carriers' transport in the structures and the intermodulation electrical signal which is created due to the interaction between the ultrasonic wave and charge carriers, is proportional to the density of structural defects. RUS enables to measure natural frequencies of free elastic vibrations of a simply shaped specimen by scanning a selected frequency range including the appropriate resonances of the measured specimens.

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Authors and Affiliations

Petr Sedlak
Pavel Tofel
Vlasta Sedlakova
Jiri Majzner
Josef Sikula
Lech Hasse
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Abstract

Electrochemical amperometric gas sensors represent a well-established and versatile type of devices with unique features: good sensitivity and stability, short response/recovery times, and low power consumption. These sensors operate at room temperature, and therefore have been applied in monitoring air pollutants and detection of toxic and hazardous gases in a number of areas. Some drawbacks of classical electrochemical sensors are overcome by the solid polymer electrolyte (SPE) based on ionic liquids. This work presents evaluation of an SPE-based amperometric sensor from the point of view of current fluctuations. The sensor is based on a novel three-electrode sensor platform with solid polymer electrolytes containing ionic liquid for detection of nitrogen dioxide − a highly toxic gas that is harmful to the environment and presenting a possible threat to human health even at low concentrations. The paper focuses on using noise measurement (electric current fluctuation measurement) for evaluation of electrochemical sensors which were constructed by different fabrication processes: (i) lift-off and drop-casting technology, (ii) screen printing technology on a ceramic substrate and (iii) screen printing on a flexible substrate.

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Authors and Affiliations

Petr Sedlak
Petr Kubersky
Pavel Skarvada
Ales Hamacek
Vlasta Sedlakova
Jiri Majzner
Stanislav Nespurek
Josef Sikula
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Abstract

Electronic Double-Layer Capacitors (EDLC), called Supercapacitors (SC), are electronic devices that are capable to store a relatively high amount of energy in a small volume comparing to other types of capacitors. They are composed of an activated carbon layer and electrolyte solution. The charge is stored on electrodes, forming the Helmholtz layer, and in electrolyte. The capacitance of supercapacitor is voltage- dependent. We propose an experimental method, based on monitoring of charging and discharging a supercapacitor, which enables to evaluate the charge in an SC structure as well as the Capacitance-Voltage (C-V) dependence. The measurement setup, method and experimental results of charging/discharging commercially available supercapacitors in various voltage and current conditions are presented. The total charge stored in an SC structure is proportional to the square of voltage at SC electrodes while the charge on electrodes increases linearly with the voltage on SC electrodes. The Helmholtz capacitance increases linearly with the voltage bias while a sublinear increase of total capacitance was found. The voltage on SC increases after the discharge of electrodes due to diffusion of charges from the electrolyte to the electrodes. We have found that the recovery voltage value is linearly proportional to the initial bias voltage value.

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Authors and Affiliations

Arkadiusz Szewczyk
Josef Sikula
Vlasta Sedlakova
Jiri Majzner
Petr Sedlak
Tomas Kuparowitz
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Abstract

Noise spectroscopy and I-V characteristic non-linearity measurement were applied as diagnostic tools in order to characterize the volume and contact quality of positive temperature coefficient (PTC) chip sensors and to predict possible contact failure. Correctly made and stable contacts are crucial for proper sensing. I-V characteristics and time dependences of resistance were measured for studied sensors and, besides the samples with stable resistance value, spike type resistance fluctuation was observed for some samples. These spikes often disappear after about 24 hours of voltage application. Linear I-V characteristics were measured for the samples with stable resistance. The resistance fluctuation of burst noise type was observed for some samples showing the I-V characteristic dependent on the electric field orientation. We have found that the thermistors with high quality contacts had a linear I-V characteristic, the noise spectral density is of 1/f type and the third harmonic index is lower than 60 dB. The samples with poor quality contacts show non-linear I-V characteristics and excess noise is given by superposition of g-r and 1/fn type noises, and the third harmonic index is higher than 60 dB.

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Authors and Affiliations

Lubomír Grmela
Zdenek Sita
Vlasta Sedlakova
Jiri Majzner
Petr Sedlak
Josef Sikula

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