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Abstract

The growing interest in one-dimensional tin oxide-based nanomaterials boosts research on both high-quality nanomaterials as well as production methods. This is due to the fact that they present unique electrical and optical properties that enable their application in various (opto)electronic devices. Thus, the aim of the paper was to produce ceramic SnO₂ nanowires using electrospinning with the calcination method, and to investigate the influence of the calcination temperature on the morphology, structure and optical properties of the obtained material. A scanning electron microscope (SEM) and Fourier-transform infrared spectroscopy (FTIR) were used to examine the morphology and chemical structure of obtained nanomaterials. The optical properties of manufactured one-dimensional nanostructures were investigated using UV-Vis spectroscopy. Moreover, based on the UV-Vis spectra, the energy band gap of the prepared nanowires was determined. The analysis of the morphology of the obtained nanowires showed that both the concentration of the precursor in the spinning solution and the calcination temperature have a significant impact on the diameter of the nanowires and, consequently, on their optical properties.
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Authors and Affiliations

Tomasz Tański
1
ORCID: ORCID
Weronika Smok
1
ORCID: ORCID
Wiktor Matysiak
1

  1. Department of Engineering Material and Biomaterials, Silesian University of Technology, ul. Konarskiego 18A, 44-100 Gliwice, Poland
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Abstract

Textile industry emits daily huge amounts of sewage rich in non-biodegradable organic compounds, especially in textile dyes. Such contaminants are highly soluble in water, which makes their removal difficult. Other studies suggest their carcinogenicity, toxicity and mutagenicity. A promising chemical treatment of textile wastewater is the photodegradation of dye molecules in the process of photocatalysis in the presence of a photocatalyst. One-dimensional nanostructures exhibit a high surface-to-volume ratio and a quantum confinement effect, making them ideal candidates for nanophotocatalyst material. Nb2O5 is, among other metal oxides with a wide band gap, gaining popularity in optical applications, and electrospun niobium oxide nanostructures, despite their ease and low cost, can increase the chemical removal of textile dyes from wastewater. Facile synthesis of electrospun one-dimensional niobium oxide nanofibers is presented. The nanophotocatalysts morphology, structure, chemical bonds and optical properties were examined. Based on photodegradation of aqueous solutions (ph=6) of methylene blue and rhodamine B, the photocatalytic activity was established. The photocatalytic efficiency after 180 minutes of ultraviolet irradiation in the presence of Nb2O5 nanofibers was as follows: 84.9% and 31.8% for methylene blue and rhodamine B decolorization, respectively.
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Authors and Affiliations

Marta Zaborowska
1
ORCID: ORCID
Weronika Smok
1
ORCID: ORCID
Tomasz Tański
1
ORCID: ORCID

  1. Department of Engineering Materials and Biomaterials, Silesian University of Technology, Konarskiego 18A, 44-100 Gliwice, Poland
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Abstract

Magnesium alloys have recently become increasingly popular in many sectors of the industry due to their unique properties, such as low density, high specific strength, vibration damping ability along with their recyclability and excellent machinability. Nowadays, thin films have been attracting more attention in applications that improve mechanical and corrosion properties. The following alloys were used for the coated Mg-Al-RE and the ultra-light magnesium-lithium alloy of the Mg-Li-Al-RE type. A single layer of TiO2 was deposited using the atomic layer deposition ALD method. Multiple layers of the Ti/TiO₂ and Ti/TiO₂/Ti/TiO₂ type were obtained by the MS-PVD magnetron sputtering technique. Samples were investigated by scanning and a transmission electron microscope (SEM, TEM) and their morphology was studied by an atomic forces microscope (AFM). Further examinations, including electrochemical corrosion, roughness and tribology, were also carried out. As a result of the research, it was found that the best electrochemical properties are exhibited by single TiO2 layers obtained by the ALD method. Moreover, it was found that the Ti/TiO₂/Ti/TiO₂ double film has better properties than the Ti/TiO₂ film.
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Authors and Affiliations

Marcin Staszuk
1
ORCID: ORCID
Łukasz Reimann
1
Aleksandra Ściślak
1
Justyna Jaworska
1
Mirosława Pawlyta
1
Tomasz Mikuszewski
2
Dariusz Kuc
2
Tomasz Tański
1
ORCID: ORCID
Antonín Kříž
3

  1. Silesian University of Technology, Faculty of Mechanical Engineering, ul. Konarskiego 18a, 44-100 Gliwice, Poland
  2. Silesian University of Technology, Faculty of Materials Engineering and Metallurgy, ul. Krasińskiego 8, Katowice, Poland
  3. University of West Bohemia, Faculty of Mechanical Engineering, Univerzitni 22 St., 30614 Plzen, Czech Republic
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Abstract

In this paper, thermal oxidation resistance of silicide-coated niobium substrates was tested in a temperature range of 1300–1450°C using an HVOF burner. Pure niobium specimens were coated using the pack cementation CVD method. Three different silicide thickness coatings were deposited. Thermal oxidation resistance of the coated niobium substrates was tested in a temperature range of 1300–1450°C using an HVOF burner. All samples that passed the test showed their ability to stabilize the temperature over a time of 30 s during the thermal test. The rise time of substrate temperature takes about 10 s, following which it keeps constant values. In order to assess the quality of the Nb-Si coatings before and after the thermal test, light microscopy, scanning electron microscopy (SEM) along with chemical analysis (EDS), X-ray diffraction XRD and Vickers hardness test investigation were performed. Results confirmed the presence of substrate Nb compounds as well as Si addition. The oxygen compounds are a result of high temperature intense oxidizing environment that causes the generation of SiO phase in the form of quartz and cristobalite during thermal testing. Except for one specimen, all substrate surfaces pass the high temperature oxidation test with no damages.
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Authors and Affiliations

Radosław Szklarek
1 2 3
Tomasz Tański
1
ORCID: ORCID
Bogusław Mendala
1
Marcin Staszuk
1
ORCID: ORCID
Łukasz Krzemiński
1
Paweł Nuckowski
1
Kamil Sobczak
3

  1. Silesian University of Technology, ul. Akademicka 2A, 44-100 Gliwice, Poland
  2. Spinex Spinkiewicz Company, Klimontowska 19, 04-672 Warsaw, Poland
  3. Łukasiewicz Research Network – Institute of Aviation, al. Krakowska 110/114, 02-256 Warsaw, Poland
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Abstract

The purpose of the paper was to design geometric models of the movable connection made of brass for three different attachment options and three different loads. The numerical analysis of the mechanical properties, stresses, strains and displacements using the finite element method was carried out in SolidWorks 2020 and their comparative analysis was performed. The computer simulations performed will allow the boundary conditions that directly affect the mechanical properties of the engineering materials to be optimised.
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Authors and Affiliations

Amadeusz Dziwis
1
ORCID: ORCID
Tomasz Tański
1
ORCID: ORCID
Marek Sroka
1
ORCID: ORCID
Agata Śliwa
1
ORCID: ORCID
Rafał Dziwis
1
ORCID: ORCID

  1. Silesian University of Technology, Department of Engineering Materials and Biomaterials, 18A S. Konarskiego Str., 44-100 Gliwice, Poland
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Authors and Affiliations

Bogusław Major
1
ORCID: ORCID
Andrei Victor Sandu
2
ORCID: ORCID
Mohd Mustafa Al Bakri Abdullah
3
Marcin Nabiałek
4
ORCID: ORCID
Tomasz Tański
5
ORCID: ORCID
Adam Zieliński
6
ORCID: ORCID

  1. Institute of Metallurgy and Materials Science Polish Academy of Science, ul. Reymonta 25, 30-059 Kraków, Poland
  2. Faculty of Materials Science and Engineering, Gheorghe Asachi Technical University of Iasi, 71 D. Mangeron Blvd., 700050 Iasi, Romania
  3. Faculty of Chemical Engineering Technology, Universiti Malaysia Perlis (UniMAP), 01000 Perlis, Malaysia
  4. Institute of Physics, Czestochowa University of Technology, ul. Dabrowskiego 69, 42-201 Czestochowa, Poland
  5. Department of Engineering Materials and Biomaterials, Silesian University of Technology, ul. Konarskiego 18A, 44-100, Gliwice, Poland
  6. Sieć Badawcza Łukasiewicz – Instytut Metalurgii Żelaza im. Stanisława Staszica, (Łukasiewicz Research Network – Institute for Ferrous Metallurgy), ul. K. Miarki 12-14, 44-100 Gliwice, Poland

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