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Abstract

Blast furnace and cupola furnace are furnace aggregates used for pig iron and cast iron production. Both furnace aggregates work on very similar principles: they use coke as the fuel, charge goes from the top to down, the gases flow against it, etc. Their construction is very similar (cupola furnace is usually much smaller) and the structures of pig iron and cast iron are very similar too. Small differences between cast iron and pig iron are only in carbon and silicon content. The slags from blast furnace and cupola furnace are very similar in chemical composition, but blast furnace slag has a very widespread use in civil engineering, primarily in road construction, concrete and cement production, and in other industries, but the cupola furnace slag utilization is minimal. The contribution analyzes identical and different properties of both kinds of slags, and attempts to explain the differences in their uses. They are compared by the contribution of the blast furnace slag cooled in water and on air, and cupola furnace slag cooled on air and granulated in water. Their chemical composition, basicity, hydraulicity, melting temperature and surface were compared to explain the differences in their utilization.

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Authors and Affiliations

A. Pribulová
P. Futáš
J. Petrík
M. Pokusová
M. Brzeziński
J. Jakubski
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Abstract

The rolls for the hot rolling finishing stands are cast centrifugally as two or three-layer rolls. The working layer is called a shell. The material of the shell is selected according to the position of the respective roll in the final finishing stand of the rolling mill. Typically, a combination of rolls made of a high-chromium cast iron + indefinite cast iron or high-speed steel + indefinite cast iron is commonly used. Great attention has been paid to indefinite cast iron in recent years and this material received a number of modifications that led to the increase of material properties up to 20% in comparison to the ordinary indefinite cast iron. But the goals of the new generation of material for hot rollers were chosen higher: increasing of production about 30% and more. This material has specific physical properties, heat treatment requirements as well as rolling mill requirements as is stated in the paper. It is expected that introduction of this material will reduce the difference between wear of the front and finishing stands, which can extend rolling campaigns and have a positive effect on the reduction rolls exchanges, the grinding of the rolls and the reduction of downtime.

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Authors and Affiliations

T. Válek
Z. Kuboň
J. Kosňovská
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Abstract

The paper deals with the influence of manganese in AlSi7Mg0.3 alloy with higher iron content. Main aim is to eliminate harmful effect of intermetallic – iron based phases. Manganese in an alloy having an iron content of about 0.7 wt. % was graded at levels from 0.3 to 1.4 wt. %. In the paper, the effect of manganese is evaluated with respect to the resulting mechanical properties, also after the heat treatment (T6). Morphology of the excluded intermetallic phases and the character of the crystallisation of the alloy was also evaluated. From the obtained results it can be concluded that the increasing level of manganese in the alloy leads to an increase in the temperature of the β-Al5FeSi phase formation and therefore its elimination. Reducing the amount of β-Al5FeSi phase in the structure results in an improvement of the mechanical properties (observed at levels of 0.3 to 0.8 wt. % Mn). The highest addition of Mn (1.4 wt.%) leads to a decrease in the temperature corresponding to the formation of eutectic silicon, which has a positive influence on the structure, but at the same time the negative sludge particles were also present

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Authors and Affiliations

D. Bolibruchová
R. Podprocká
R. Pastirčák
K. Major-Gabryś
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Abstract

The work deals with possibilities of using this specific material. It is focused on cast metal foams with a regular arrangement of internal cells and it refers to already used casting technologies – the production of metal foamswith the aid of sand cores. Metal foamsare used in many industries, such as: automotive, aerospace, construction, power engineering. They have unique propertiesand due to lower weight with sufficient strength and greater contact surface can be used, for example, for the conduction of heat. This article deals with the useof the metal foam as a heat exchanger. The efficiency of the heat exchanger depends on its shape and size and therefore the study is focused first on the optimization of the shape before the proper manufacture.

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Authors and Affiliations

F. Radkovský
M. Gebauer
V. Merta
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Abstract

The results of mechanical reclamation of waste moulding sands with furfuryl resin and activators of new generation are presented.

The aim of the research described in this study was to determine what effect the addition of reclaim obtained in the process of dry mechanical reclamation could have on the properties of furan sands.

The sand supplied by one of the domestic foundries was after the initial reclamation subjected to a two-step proper reclamation

process. The following tests were carried out on the obtained reclaim: pH, S and N content, loss on ignition and comprehensive

sieve analysis. The obtained reclaim was next used as a component of moulding sands with furfuryl resin, wherein it formed 50%

and 80% of the base moulding material, respectively. The strength properties of the ready sand mixtures (bending strength Rg u and tensile strength Rm u ) were determined after the hardening time of 0.5, 1, 2, 4 and 24 hours.

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Authors and Affiliations

J. Kamińska
E. Basińska
M. Angrecki
A. Palma
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Abstract

Main aim of submitted work is evaluation and experimental verification of inoculation effect on Al alloys hot-tear sensitivity. Submitted work consists of two parts. The first part introduces the reader to the hot tearing in general and provides theoretical analysis of hot tearing phenomenon. The second part describes strontium effect on hot tearing susceptibility, and gives the results on hot tearing for various aluminium alloys. During the test, the effect of alloy chemical composition on hot tearing susceptibility was also analyzed. Two different Al-based alloys were examined. Conclusions deals with effect of strontium on hot tearing susceptibility and confirms that main objective was achieved.

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Authors and Affiliations

D. Bolibruchová
M. Bruna
R. Pastirčák
K. Major-Gabryś
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Abstract

Currently is the biggest problem of metallurgical companies the increase of fossil fuel prices and strict environmental regulations. As a result of this, companies must look for alternatives that would reduce the amount of fossil fuels and reduce emissions. Wood sawdust has huge energy potential, which can be used in the process of agglomerate production. This type of energy is locally available, has some similar properties as fossil fuels and is economically advantageous. For these reasons, experimental study using laboratory agglomeration pan was realized to study the possibility of agglomerate production with a mixed fuel. Experimental results show the viability of mixed fuel use in the agglomeration process, but also show significant possibility for improvement. The maximum acceptable substitution ratio, which corresponds to qualitatively suitable agglomerate is 20% of pine sawdust. Based on the realized experiments and the obtained results we have acceded to the intensification of the agglomeration process with an objective to increase the amount of added substitution fuel while maintaining the required quality of agglomerate.

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Authors and Affiliations

Z. Semanová
J. Legemza
M. Hrubovčáková
R. Findorák
M. Fröhlichová
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Abstract

Internal structure of metal foams is one of the most important factors that determine its mechanical properties. There exists a number of methods for studying the nature of the inner porous structure. Unfortunately most of these processes is destructive and therefore it is not possible to reuse the sample. From this point of view, as a suitable method seems to be the ability of using the so-called X-ray microtomography (also micro-CT). This is a non-destructive methodology used in a number of fields (industry, science, archaeology, medicine) for a description of the material distribution in the space (e.g. pores, fillers, defects, etc.). In principle, this technology works on different absorption of X-ray radiation by materials with changing proton number. The contribution was worked out in collaboration with experts from the Faculty of Electrical Engineering and Computer Science of the VŠB-Technical University of Ostrava and it is focused on the analysis of internal structure of the metal foam casting with irregular arrangement of internal pores by using micro-CT. The obtained data were evaluated in the commercial software VGStudio MAX 2.2 and in the FOTOMNG system. For the evaluation of these data a new specialized module was introduced in this system. Several methods of pre-processing the image was prepared for the measurement. This preliminary processing consists, for example, from a binary image thresholding for better diversity between the internal porosity and the material itself or functions for colour inversion.

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Authors and Affiliations

I. Kroupová
P. Lichý
L. Ličev
J. Hendrych
K. Souček
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Abstract

The post-processing slags containing about 0.8 wt.% of copper were subjected to the treatment of a complex reagent. The chemical composition of the complex reagent has been elaborated and patented in frame of the Grant No. PBS3/A5/45/2015. The slags had an industrial origin and were delivered by the Smelter and Refinery Plant, Głogów, as a product of the direct-to-blister technology performed in the flash furnace assisted by the arc furnace. An agglomeration of copper droplets suspended in the liquid slag, their coagulation, and deposition on the bottom of furnace were observed after the treatment this post-processing slag by the mentioned reagent. The treatment of the post-processing slags by the complex reagent was performed in the arc furnace equipped with some additional electrodes situated at the furnace bottom (additional, in comparison with the arc furnace usually applied in the Smelter and Refinery Plant, Głogów). The behaviour of the copper droplets in the liquid slag within the competition between buoyancy force and gravity was studied from the viewpoint of the required deposition of coagulated copper droplets. The applied complex reagent improves sufficiently the surface free energy of the copper droplets. In the result, the mechanical equilibrium between coagulated copper droplets and surrounding liquid slag is properly modified. Eventually, sufficiently large copper droplets are subjected to a settlement on the furnace bottom according to the requirements. The agglomeration and coagulation of the copper droplets were significantly improved by an optimized tilting of the upper electrodes and even by their rotation. Moreover, the settlement was substantially facilitated and improved by the employment of both upper and lower system of electrodes with the simultaneous substitution of the variable current by the direct current.

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Authors and Affiliations

W. Wołczyński
A.W. Bydałek
P. Migas
A. Tarasek
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Abstract

Experimental observations of the steel morphology as well as measurements of the solutes concentration in the macro-scale were made on the basis of the vertical cut at the mid-depth of the 15-tons steel forging ingot serially produced in one of the steel plant in Poland. Experimental observations of the morphology accompanied by the measurements of the Peclet Number were also made on the cross-section of the continuously cast brass ingots serially produced in the copper / brass industry in Poland. The performed measurements allowed to work out some maps of the alloying elements segregation for the longitudinal section of the steel static ingot and a Growth Law for the columnar grains formation in the brass ingots. The marginal stability criterion has been applied to the last mentioned development / description. Some suggestions for the micro-segregation measurement mode in the columnar structure are derived.

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Authors and Affiliations

W. Wołczyński
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Abstract

The behaviour of porous sinters, during compression and compression with reverse cyclic torsion tests is investigated in the article based on the combination of experimental and numerical techniques. The sinters manufactured from the Distaloy AB powder are examined. First, series of simple uniaxial compression tests were performed on samples with three different porosity volume fractions: 15, 20 and 25%. Obtained data were then used during identification procedure of the Gurson-Tvergaard-Needleman finite element based model, which can capture influence of porosity evolution on plasticity. Finally, the identified Gurson-Tvergaard- Needleman model was validated under complex compression with reverse cyclic torsion conditions and proved its good predictive capabilities. Details on both experimental and numerical investigations are presented within the paper.

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Authors and Affiliations

L. Madej
K. Perzyński
M. Składzień
M. Tkocz
M. Rosiak
F. Grosman
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Abstract

The paper analyzes the effect of ageing on the variations in the mechanical and technological properties of steel wire. The process of drawing 5.5 mm-diameter wire rod into 1.70 mm wire was carried out in 12 draws on a Koch KGT multi-stage drawing machine in the drawing velocity range of 5-25 m/s. Finished 1.7 mm-diameter wires after, respectively, 1, 24, 720 and 8760 hours of the completion of the drawing process were subjected to testing to determine their mechanical and technological properties. The yield strength, YS; tensile strength, UTS; uniform elongation, Ar; total elongation, Ac; reduction of area, Z; number of twists, Nt; and the number of bends, Nb, have been determined. It has been demonstrated that variations in mechanical properties occur after the multi-stage drawing process due to ageing, with their degree and mode being dependent on the drawing speed.

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Authors and Affiliations

M. Suliga
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Abstract

Detailed studies of the movement of liquid steel (hydrodynamics) on a real object are practically impossible. The solution to this problem are physical modelling carried out on water models and numerical modelling using appropriate programs. The method of numerical modelling thanks to the considerable computing power of modern computers gives the possibility of solving very complex problems.

The paper presents the results of model tests of liquid flow through tundish. The examined object was model of the twonozzle tundish model. The ANSYS Fluent program was used to describe the behavior of liquid in the working area of the tundish model. Numerical simulations were carried out using two numerical methods of turbulence description: RANS (Reynolds-Averaged Navier-Stokes) – model k-ε and LES (Large Eddy Simulation). The results obtained from CFD calculations were compared with the results obtained using the water model.

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Authors and Affiliations

T. Merder
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Abstract

The paper deals with squeeze casting technology. For this research a direct squeeze casting method has been chosen. The influence of process parameters variation (casting temperature, mold temperature, pressure) on mechanical properties and structure will be observed. The thicknesses of the individual walls were selected based on the use of preferred numbers and series of preferred numbers (STN ISO 17) with the sequence of 3.15, 4.00, 5.00, 6.00 and 8.00 mm. The width of each wall was 22 mm with a length of 100 mm. As an experimental material was chosen the AlSi12 and AlSi7Mg0.3 alloys. The mechanical properties (UTS, E) for individual casting parameters and their individual areas of different thicknesses were evaluated. In the structure the influence of pressure on the change of the eutectic morphology, the change of the volume of eutectic and the primary alpha phase, the effect of the pressure on the more fine-grain and the regularization of the structure were evaluated.

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Authors and Affiliations

R. Pastirčák
J. Ščury
M. Brůna
D. Bolibruchová
J. Jakubski
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Abstract

It is really hard to determine the phenomena occurring during aluminum refining process using argon blowing through the liquid metal in industrial conditions. The solution of such problem is physical modelling. This kind of modelling gives possibility to determine the level of dispersion of the refining gas in liquid metal. Especially in steel metallurgy RTD (Residence Time Distribution) analysis and visualization process with some colour tracer, which can give extra information about time of mixing are very popularly used. Because the modelling research (especially visualization) is pictorial, the research was conducted to check if it is possible to estimate quantitatively impeller working effectiveness basing on determination of the RTD curves. The examined object was model of URO-200 batch refining reactor. The RTD curves was registered and discussed for three different impellers and four different variants of processing parameters (rotary impeller speed: 300-500 rpm, and gas flow rate: 15-20 l·min–1). Additionally, the process of mixing of the inert gas with water as a modelling agent was enabled to be observed due to introduction of colour tracer (KMnO4). Results obtained from both measuring methods were graphically presented, compared and shortly discussed.

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Authors and Affiliations

M. Saternus
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Abstract

The subject of the study are alumina foams produced by gelcasting method. The results of micro-computed tomography of the foam samples are used to create the numerical model reconstructing the real structure of the foam skeleton as well as the simplified periodic open-cell structure models. The aim of the paper is to present a new idea of the energy-based assessment of failure strength under uniaxial compression of real alumina foams of various porosity with use of the periodic structure model of the same porosity. Considering two kinds of cellular structures: the periodic one, for instance of fcc type, and the random structure of real alumina foam it is possible to justify the hypothesis, computationally and experimentally, that the same elastic energy density cumulated in the both structures of the same porosity allows to determine the close values of fracture strength under compression. Application of finite element computations for the analysis of deformation and failure processes in real ceramic foams is time consuming. Therefore, the use of simplified periodic cell structure models for the assessment of elastic moduli and failure strength appears very attractive from the point of view of practical applications.

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Authors and Affiliations

M. Nowak
Z. Nowak
R.B. Pęcherski
M. Potoczek
R.E. Śliwa
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Abstract

In this paper, explain the preparation of CaTiO3 ceramics synthesized by the solid-state reaction method. Calcium carbonate and titanium dioxide were high energy mixed in stoichiometric amounts, and the obtained mixture was calcined at different temperatures (800, 900, 1000 and 1300ºC) for 2 h. The obtained samples were characterized by measurement of particle size, Energy Dispersive X-Ray (EDX) Analysis; differential thermal analysis, X-ray diffraction and SEM images. XRD patterns indicated that CaTiO3 ceramics with the structure of perovskite is obtained from calcined powders at 1,300°C for 2 h. SEM images show the formation of a very fine and homogeneous morphology. The measured values of electrical resistivity were within the typical range of insulating materials and approach values corresponding to insulating ceramics.

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Authors and Affiliations

E. Rocha-Rangel
J. López-Hernández
J.A. Castillo-Martínez
J.J. Osorio-Ramos
C.A. Calles-Arriaga
I. Estrada-Guel
R. Martínez-Sánchez
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Abstract

The aim of the performed experiments was to determine the influence of deformation and of austenitization temperature on the kinetics of phase transformations during cooling of high-carbon steel (0.728 wt. % C). The CCT and DCCT diagrams for austenitization temperature 940°C and DCCT diagram for austenitization temperature 1000°C were constructed with the use of dilatometric tests. On the basis of obtained results, a featureless effect of austenitization temperature and deformation on the kinetics of phase transformations during cooling of investigated steel was observed. Critical cooling rates for the transformation of martensite in microstructure fluctuated from 5 to 7°C · s–1 (depending on the parameters of austenitization and deformation), but only at cooling rates higher than 8°C · s–1 a dominant share of martensite was observed in the investigated steel, which resulted in the significant increase of hardness.

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Authors and Affiliations

P. Kawulok
P. Podolinský
P. Kajzar
I. Schindler
R. Kawulok
V. Ševčák
P. Opěla
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Abstract

In view of their advantageous properties (high hardness, good frictional wear resistance, chemical and thermal stability at elevated temperatures), cubic boron nitride (cBN) and tungsten carbide (WC) are commonly used for the fabrication of cutting tools. The composites were consolidated at a temperature of 1100°C under a load of 100 MPa for 10 min. The density of the thus produced material was close to the theoretical value (about 99.6%), and the hardness HV30 was about 1950. The phases identified in the composite were WC, Co, and cBN. Microstructural examinations revealed that numerous trans-crystalline fractures through the cBN particles occurred in the material.

The present study is concerned with the wear of the WCCo and WCCo/cBN composites. Comparative tribological examinations were performed in a tribological tester using the ball-on-disc arrangement under the conditions of dry friction. The counterspecimens were steel and Al2O3 balls. The tests were conducted under a unit load of 10 N. After the tests, the surface of the samples was examined to describe the wear mechanisms active in various composite materials.

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Authors and Affiliations

J. Wachowicz
T. Truszkowski
M. Rosiński
M. Ossowski
G. Skrabalak
M. Cyrankowski
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Abstract

The welding of nuclear grade P91 and P92 steel plate of thickness 5.2 mm were performed using the autogenous tungsten

inert gas (TIG) welding process. The welded joint of P91 and P92 steel plate were subjected to the varying post weld heat-treatment

(PWHT) including the post weld heat treatment (PWHT) and re-austenitizing based tempering (PWNT). A comparative study was

performed related to the microstructure evolution in fusion zone (FZ) of both the welded joint using the scanning electron microscope

and optical microscope in a different condition of heat treatment. The hardness test of the FZ for both joints was also conducted in

a different condition of heat treatment. P92 steel welded joint have observed the higher tendency of the δ ferrite formation that led

to the great variation in hardness of the P92 FZ. The homogeneous microstructure (absence of δ ferrite) and acceptable hardness

was observed after the PWNT treatment for both the welded joint.

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Authors and Affiliations

C. Pandey
M. Mohan Mahapatra
P. Kumar
P. Prakesh Kumar
J.G. Thakare
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Abstract

In this study, two different compositions of submicron-structured titanium (760 nm) and micron-structured chromium (4.66 μm) powders were mixed to fabricate Cr-31.2 mass% Ti alloys by vacuum hot-press sintering. The research imposed various hot-press sintering pressures (20, 35 and 50 MPa), while the sintering temperature maintained at 1250°C for 1 h. The experimental results showed that the optimum parameters of the hot-press sintered Cr-31.2 mass% Ti alloys were 1250°C at 50 MPa for 1 h. Also, the relative density reached 99.94%, the closed porosity decreased to 0.04% and the hardness and transverse rupture strength (TRS) values increased to 81.90 HRA and 448.53 MPa, respectively. Moreover, the electrical conductivity is enhanced to 1.58 × 104 S·cm–1. However, the grain growth generated during the high-temperature and high-pressure of the hot-press sintering process resulted in the grain coarsening phenomenon of the Cr-31.2 mass% Ti alloys after 1250°C hot-press sintering at 50 MPa for 1 h. In addition, the Cr-31.2 mass% Ti alloys were fabricated with the submicron-structured titanium (760 nm) and chromium (588 nm) powders showed more effective compaction than the micron-structured titanium (760 nm) and chromium (4.66 μm) powders did. The closed porosity decreases to 0.02% and the hardness values increase to 83.23 HRA. However, the agglomeration phenomenon of the Cr phase and brittleness of the TiCr2 Laves phases easily led to a slight decrease in TRS (400.54 MPa).

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Authors and Affiliations

Shih-Hsien Chang
Chien-Lun Li
Kuo-Tsung Huang
Tzu-Hsien Yang
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Abstract

Single point incremental forming process is a most economical Die-less forming process. The major constraint of it is that it is a time consuming process. In this work, a new attempt was made in incremental forming process using Multipoint tool for SS430 sheets to increase the formability and to reduce forming time. Fractography analysis was made to study the size of voids that were formed during fracture. The forming limit diagrams were drawn and compared for single point incremental forming and the multipoint incremental forming of SS430 sheet. It was proved that the formability of SS430 sheet in the multipoint forming was better than the formability of that in single point forming and the time consumed was reduced. The strain distribution in both processes had also been studied along with surface roughness.

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Authors and Affiliations

K. Ramkumar
G. Paulraj
K. Elangovan
C. Sathiya Narayanan
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Abstract

The work deal with an assembling and comparing of transformation diagrams of two low-alloy steels, specifically 16MnCrS5 and 20MnCrS5. In this work, diagrams of the type of CCT and DCCT of both steels were assembled. Transformation diagrams were assembled on the basis of dilatometric tests realized on the plastometer Gleeble 3800, of metallographic analyses and of hardness measurements. In addition, for comparison, the transformation diagrams were assembled even with use of the QTSteel 3.2 software. Uniform austenitization temperature of 850°C was chosen in case of both steels and even both types of diagrams. In case of both steels, an influence of deformation led to expected acceleration of phase transformations controlled by diffusion and also of bainite transformation. In both cases, the kinetics of martensitic transformation was not significantly affected by deformation.

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Authors and Affiliations

R. Kawulok
P. Kawulok
I. Schindler
P. Opěla
S. Rusz
V. Ševčák
Z. Solowski
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Abstract

In the present work, studies have been carried out on the variations in the microstructure and hardness of P91 base-metal and welded joint. This variations result from the grit blasting and thermal cycle experienced during the thermal spraying process. The microstructural effects have been analyzed in terms of the depth of the deformation zone. Scanning Electron Microscopy and Xray diffraction were used as characterization techniques. The grit blasting carried out prior to thermal spraying has resulted in the highest change in sub-surface hardness of the heat affected zone (HAZ). However, flame treatment further reduced the subsurface hardness of the heat affected zone. The depth of deformation zone was highest for inter-critical heat affected zone (IC-HAZ). The overall coating process resulted in an increase in subsurface hardness of various regions of HAZ and fusion zone (FZ). The base metal showed a 7% increase in subsurface hardness due to the overall coating process. The IC-HAZ showed maximum variation with 36% increase in subsurface hardness. The coarse grained heat affected zone (CG-HAZ) and FZ did not show any change in subsurface hardness. As a whole, the hardness and microstructure of the welded joint was observed to be more sensitive to the thermal spray coating process as compared to the base metal.

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Authors and Affiliations

J.G. Thakare
C. Pandey
R.S. Mulik
M.M. Mahapatra
H.K. Narang

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