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Abstract

The β-phase Titanium (β-Ti) alloys have been under the spotlight in the recent past for their use as biomedical prosthetic materials owing to their excellent properties such as low elastic modulus, high corrosion resistance and tensile strength. Recently, Niobium (Nb) has gained a lot of attention as a β-phase stabilizing element in Ti alloys to replace Vanadium (V) due to its excellent solubility in Ti, low elastic modulus and biocompatibility. In this work, low cost Ti-20Nb binary alloy has been fabricated via powder metallurgy procedures. The blended powder mixtures of Ti and Nb were sintered at 900°C for 20 mins by the Spark Plasma Sintering (SPS) with an applied uniaxial pressure of 40 MPa. The heating rate was fixed at 50°C/min. The sintered alloy was subject to heat treatments at 1200°C in vacuum condition for various time durations. The characterizations of microstructure obtained during this process were done using FE-SEM, EDS and XRD. By increasing heat treatment time, as understood, the volume of residual Nb particles was decreased resulting in accelerated diffusion of Nb into Ti. Micro hardness of the alloy increased from 340 to 355 HV with the increase in β phase content from 30 to 45%. The resultant alloys had relatively high densities and homogenized microstructures of dispersed lamellar β grains in α matrix.

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Authors and Affiliations

M.A. Haq
S.F. Abbas
Nu Si A. Eom
T.S. Kim
B. Lee
K.-T. Park
B.S. Kim
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Abstract

Production of Ti-based alloys with non-toxic elements give the possibility to control the market of medical applications, using alloys with appropriate properties for human body, contributing to improving the health of the population. Determination of parameters of atomic and magnetic structure of functional biomaterials demonstrating interesting physical phenomena and being promising for medical applications in a wide range of thermodynamic parameters; exploration of the role of cluster aggregation in the formation of physical properties. Paper is about the obtaining of the new titanium system alloys, the determining their characteristics and structure, and obtaining information concerning phase transitions and some mechanical properties. Ti15Mo7ZrxTa (5 wt.%, 10 wt.% and 15 wt.%) alloys developed shows a predominant β phase highlighted by optical microstructure and XRD patterns. A very low young modulus of alloys was obtained (43-51 GPa) which recommends them as very good alloys for orthopedic applications.
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Authors and Affiliations

I. Baltatu
1
ORCID: ORCID
A.V. Sandu
1 2 3
ORCID: ORCID
M.S. Baltatu
1 2
ORCID: ORCID
M. Benchea
4
ORCID: ORCID
D.C. Achitei
1 2
ORCID: ORCID
F. Ciolacu
5
ORCID: ORCID
M.C. Perju
1 2
ORCID: ORCID
P. Vizureanu
1 2
ORCID: ORCID
L. Benea
6
ORCID: ORCID

  1. “Gheorghe Asachi” Technical University of Iasi, Faculty of Materials Science and Engineering, 41 “D. Mangeron” Street, 700050, Iasi, Romania
  2. University Malaysia Perlis, Centre of Excellence Geopolymer & Green Technology School of Materials Engineering, Kompleks Pengajian Jejawi 2,02600 Arau, Perlis
  3. Romanian Inventors Forum, Str. Sf. P. Movila 3, L11, 700089, Iasi, Romania
  4. “Gheorghe Asachi” Technical University of Iasi, Faculty of Mechanical Engineering, 61-63 “D. Mangeron” Street, 700050, Iasi, Romania
  5. “Gheorghe Asachi” Technical University of Iasi, Department of Natural and Synthetic Polymers, 73 Blvd. D. Mangeron, Iasi, 700050, Romania
  6. Dunărea de Jos University of Galati, Faculty of Engineering, 47 Domneasca St., 800008, Galati, Romania

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