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Abstract

The paper presents the results of studies on the development of correlation of solidification parameters and chemical composition of nickel

superalloy IN-713C, which is used i.a. on aircraft engine turbine blades. Previous test results indicate significant differences in

solidification parameters of the alloy, especially the temperatures Tliq and Tsol for each batch of ingots supplied by the manufacturer.

Knowledge of such a relationship has important practical significance, because of the ability to asses and correct the temperatures

of casting and heat treatment of casts on the basis of chemical composition. Using the statistical analysis it was found that the temperature

of the solidification beginning Tliq is mostly influenced by the addition of carbon (similar to iron alloys). The additions of Al and Nb have

smaller but still significant impact. Other alloying components do not have significant effect on Tliq. The temperature Teut is mostly

affected by Ni, Ti and Nb. The temperature Tsol is not in any direct correlation with the chemical composition, which is consistent with

previous research. The temperature Tsol depends primarily on the presence of non-metallic inclusions present in feed materials and

introduced during the melting and casting processes.

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Authors and Affiliations

J. Szymszal
P. Gradoń
F. Binczyk
J. Cwajna
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Abstract

The paper presents the results of evaluation of the metallurgical quality of master heat ingots and of the identification of non-metallic inclusions (oxides of Al., Zr, Hf, Cr, etc.), which have been found in the shrinkage cavities formed in these ingots. The inclusions penetrate into the liquid alloy, and on pouring of mould are transferred to the casting, especially when the filtering system is not sufficiently effective. The specific nature of the melting process of nickel and cobalt alloys, carried out in vacuum induction furnaces, excludes the possibility of alloy refining and slag removal from the melt surface. Therefore, to improve the quality of castings (parts of aircraft engines), it is so important to evaluate the quality of ingots before charging them into the crucible of an induction furnace. It has been proved that one of the methods for rapid quality evaluation is an ATD analysis of the sample solidification process, where samples are taken from different areas of the master heat ingot. The evaluation is based on a set of parameters plotted on the graph of the dT/dt derivative curve during the last stage of the solidification process in a range from TEut to Tsol.
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Authors and Affiliations

P. Gradoń
F. Binczyk
J. Cwajna
S. Roskosz

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