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Abstract

The Centro de Desarrollo Tecnológico del Gas developed a static expansion system to enable the calibration of medium and high vacuum pressure gauges in Colombia. The system can generate pressures between 0.1 Pa and 100 kPa. The characterization tests included the evaluation of pressure stability and desorption rate, a trueness test, and the analysis of the uncertainty budget of the calibration result. The pressure stability test was successfully completed and showed the positive effect of baking on the final pressure in the system. The trueness test allowed concluding that the calibration results with the system are comparable with those obtained with a reference meter traceable to a national metrology institute. The uncertainty budget analysis indicated the dominance of the pressure of the unit under calibration and of the initial pressure in the small tank in different pressure ranges on the uncertainty of the result. A comparison with a Monte Carlo simulation led to the conclusion that in this situation, the GUM (Guide to the Expression of Uncertainty in Measurement) method is not ideal for estimating the uncertainty of the results.
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Bibliography

[1] Khan,W., Hong, H. H., Satar, T., Ahmed, M., Khan, Z. A.,& Khan, M. Z. (2016). The KRISS primary vacuum gauge calibration standards:Areview. Journal of the Vacuum Society of Japan, 59(8), 222–235.
[2] Astrua, M., Mari, D., & Pasqualin, S. (2019). Improvement of INRiM static expansion system as vacuum primary standard between 10(-4) Pa and 1000 Pa. 19th International Congress of Metrology, 27007. https://doi.org/10.1051/metrology/201927007
[3] Semwal, P., Khan, Z., Dhanani, K. R., Pathan, F. S., George, S., Raval, D. C., Thankey, P. L., Paravastu, Y., & Himabindu, M. (2012). Spinning rotor gauge based vacuum gauge calibration system at the Institute for Plasma Research. Journal of Physics: Conference Series, 390, 012027. https://doi.org/10.1088/1742-6596/390/1/012027
[4] Bergoglio, M., & Calcatelli, A. (2004). Uncertainty evaluation of the IMGC-CNR static expansion system. Metrologia, 41, 278–284. https://doi.org/10.1088/0026-1394/41/4/009
[5] Greenwood, J. C. (2006). Simulation of the operation and characteristics of static expansion pressure standards. Vacuum, 80, 548–553. https://doi.org/10.1016/j.vacuum.2005.09.003
[6] Soriano Cardona, B., Torres Guzmán, J., & Santander Romero, L. (2001). Sistema de referencia nacional para la medición de vacío. Simposio de Metrología CENAM 2001, México.
[7] Bergoglio, M., Calcatelli, A., Marzola, L., & Rumiano, G. (1988). Primary pressure measurements down to 10(-6) Pa. Vacuum, 38(8–10), 887–891. https://doi.org/10.1016/0042-207X(88)90486-1
[8] Fedchak, J. A., Abbott, P. J., & Hendricks, J. H. (2018). Review Article: Recommended practice for calibrating vacuum gauges of the ionization type. Journal of Vacuum Science & Technology A, 36, 030802. https://doi.org/10.1116/1.5025060
[9] Torres Guzmán, J. C., Santander, L. A., & Jousten, K. (2005). Realization of the medium and high vacuum primary standard inCENAM,Mexico.Metrologia, 42(6), S157–S160. https://doi.org/10.1088/0026-1394/42/6/S01
[10] Jousten, K., Röhl, P., & Aranda Contreras, V. (1999). Volume ratio determination in static expansion systems by means of a spinning rotor gauge. Vacuum, 52(4), 491–499. https://doi.org/10.1016/S0042-207X(98)00337-6
[11] Herranz, D., Ruiz, S., & Medina, N. (2009). Volume ratio determination in static expansion systems by means of two pressure balances. XIX IMEKO World Congress, Fundamental and Applied Metrology, Portugal. https://www.imeko2009.it.pt/Papers/FP_280.pdf
[12] Phanakulwijit, S.,&Pitakarnnop, J. (2019). Establishment of Thailand’s national primary vacuum standard by a static expansion method. Journal of Physics: Conference Series, 1380, 012003. https://doi.org/10.1088/1742-6596/1380/1/012003
[13] Jitschin, W. (2002). High-accuracy calibration in the vacuum range 0.3 Pa to 4000 Pa using the primary standard of static gas expansion. Metrologia, 39(3), 249–261. https://doi.org/10.1088/0026-1394/39/3/2
[14] Kangi, R., Ongun, B., & Elkatmis, A. (2004). The new UME primary standard for pressure generation in the range from 9 × 10 -4 Pa to 103 Pa. Metrologia, 41(4), 251–256. https://doi.org/10.1088/ 0026-1394/41/4/005
[15] International Organization for Standardization. (2011). Vacuum gauges – Calibration by direct comparison with a reference gauge ISO Standard No. 3567:2011. https://www.iso.org/standard/59372.html
[16] Antsukova, A. I., Gorobei, V. N., Liubomirov, A. B., Pimenova, A. A.,&Chernyshenko, A. A. (2019). Calibration of measuring instruments of low absolute pressures. IOP Conference Series: Journal of Physics: Conference Series, 1313, 012002. https://doi.org/10.1088/1742-6596/1313/1/012002
[17] Ruiz González, S. (2011). Desarrollo de un nuevo patrón nacional de presión. Desde la columna de mercurio a patrones primarios de vacío [Doctoral dissertation, Universidad de Valladolid]. UVaDOC Repositorio Documental de la Universidad de Valladolid. https://doi.org/10.35376/10324/830
[18] Joint Committee for Guides in Metrology. (2008). Evaluation of measurement data – Guide to the expression of uncertainty in measurement (JCGM 100:2008). http://www.bipm.org/utils/common/ documents/jcgm/JCGM_100_2008_E.pdf
[19] Joint Committee for Guides in Metrology. (2008). Evaluation of measurement data – Supplement 1 to the “Guide to the expression of uncertainty in measurement” – Propagation of distributions using a Monte Carlo method (JCGM 101:2008). https://www.bipm.org/documents/20126/2071204/ JCGM_101_2008_E.pdf

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Authors and Affiliations

Jonathan Javier Duarte Franco
1
Carlos Mauricio Villamizar Mora
2
Carlos Eduardo García Sánchez
1

  1. Corporación Centro de Desarrollo Tecnológico del Gas, Grupo de Investigación en Fluidos y Energía, Carrera 23# 106-08, ZIP 680004, Bucaramanga, Colombia
  2. Universidad Industrial de Santander, Escuela de Ingeniería Mecánica, Grupo de Investigación en Energía y MedioAmbiente, Carrera 27 calle 9, ZIP 680002, Bucaramanga, Colombia
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Abstract

Y and V codoped SrBi 2Nb 2O 9 ceramics, which have been characterized by XRD, FTIR and SEM techniques, were prepared through molten salt using NaCl-KCl medium. Through X-ray diffraction analysis, all prepared samples were matched by undoped SrBi 2Nb 2O 9. The lattice parameters do not depend on the amount of dopants. Under the optimized experimental conditions, the compounds are composed of small crystallites of varying size and orientation, resulting in many micros train defects. FTIR spectra revealed that the dopant promotes a slight decrease in the 612 cm –1 band. A plate-like morphology was revealed by scanning electron microscopy, while Nyquist plots indicate non-Debye relaxation for all compounds. V and Y were incorporated into SrBi 2Nb 2O 9 lattice in order to reduce dielectric loss tangent. Thus, the codoping increases the of SrB 1.9Y 0.1Nb 1.95V 0.05O 9 (Y0.1V0.05) ceramic whereas, they were significantly decreased in the case of SrBi 1.8Y 0.2Nb 2O 9 (Y0.2) ceramic. Y0.1V0.05 sample makes up the highest efficient charge transfer, followed by Y0.2 sample representing the lowest.
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Authors and Affiliations

Mohamed Afqir
1
ORCID: ORCID
Mohamed Elaatmani
1
ORCID: ORCID
Abdelouahad Zegzouti
1
ORCID: ORCID
Nabiha Tahiri
1
Mohamed Daoud
1
ORCID: ORCID

  1. Université Cadi Ayyad, Faculté des Sciences Semlalia, Laboratoire de Sciences des Matériaux et Optimisation des Procédés, Marrakech, Morocco
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Abstract

The safe environmental disposal of sulphide-rich copper/zine mine tailings is fast becoming a major economic factor in determining the profitability of mining operations. There have been new approaches and better technologies practised in the recent years which allow the mining industries to reduce and/or eliminate the environmental impacts of harmful mine tailings. One of these approaches is the use of high-density paste backfill (HDPB) which is consisting mainly of a mix of solid particles (with the cement) and water, containing between 70% and 85% by dry weight of solids. The increased use of HDPB has improved the reliability, and has reduced the cost of the preparation and transportation systems. This paper focuses on the potential environmental benefits of using the HDPB when tailings are acid generating, and also provides a case study conducted in an underground copper/zinc mine in northeast Turkey in order to illustrate these benefits.

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Authors and Affiliations

Erol Yilmaz
Tikou Belem
Mostafa Benzaazoua
Ayhan Kesimal
Bayram Ercikdi
Ferdi Cihangir
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Abstract

The whitefly, Bemisia tabaci, an insect of the order Hemiptera which attacks more than 600 species of plants, is one of the most important agricultural pests around the world. The insecticidal Cry proteins from Bacillus thuringiensis (Bt) are useful biological pesticides, and some are toxic to Hemipteran insects. In this study, Colombian native isolates of Bt were functionally characterized at molecular and biological levels. The strains contained between one and five different crystal shapes: round, triangular, amorphous, bipyramidal and squared. The strains presented between three to seven bands of proteins in their electrophoretic pattern that were organized into six groups according to their possible biological activity on insect pests. Cry1Aa, cry1Ab, cry1Ac, cry1B and cry1C genes were identified for PCR in the different Bt isolates. Bioassays were performed on tomato leaves whose surface was spread with 3 μg · ml−1 crude extract of Bt toxins. Second instar larvae of whitefly, which were placed on top of leaves and exposed to the toxins for 7 days, exhibited mortalities from 18 to 69%. The lethal concentration 50 (LC50) of ZBUJTL39, Bt kurstaki HD1 and ZCUJTL9 strains were 1.83, 1.85 and 2.16 μg · ml−1, respectively (p < 0.05). These results show that the native Bt strain ZBUJTL39, which contained the genes cry1Aa, cry1Ab, cryCa and cryBa could eventually be used for the development of an integrated management program together with other tools for the control of B. tabaci.

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Authors and Affiliations

Eneida Torres Cabra
Javier Adolfo Hernandez Fernandez
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Abstract

This paper presents a non-invasive measurement method for simultaneous characterization of diameter and refractive index of transparent fibres. The method is based on scattering of a polychromatic beam of light by a side-illuminated fibre under study. Both quantities of interest are inversely calculated from the scattering far-field region in the vicinity of the primary rainbow. The results of practical measurements are examined with the use of a novel optical system for laboratory-level tests. An analysis of prediction errors for 20– 120 μm thick fibres having various refractive indices helps to assess the outcome of the measurement data. The results show a clear route to improve the measurement process in on-line industrial process control.

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Authors and Affiliations

Grzegorz Świrniak
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Abstract

A new approach to passive electromagnetic modelling of coupled–cavity quantum cascade lasers is presented in this paper. One of challenges in the rigorous analysis of such eigenvalue problem is its large size as compared to wavelength and a high quality factor, which prompts for substantial computational efforts. For those reasons, it is proposed in this paper to consider such a coupled-cavity Fabry-Perot resonant structure with partially transparent mirrors as a two-port network, which can be considered as a deterministic problem. Thanks to such a novel approach, passive analysis of an electrically long laser can be split into a cascade of relatively short sections having low quality factor, thus, substantially speeding up rigorous electromagnetic analysis of the whole quantum cascade laser. The proposed method allows to determine unequivocally resonant frequencies of the structure and the corresponding spectrum of a threshold gain. Eventually, the proposed method is used to elaborate basic synthesis rules of coupled–cavity quantum cascade lasers.

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Authors and Affiliations

M. Krysicki
B. Salski
P. Kopyt
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Abstract

This study aims at the immobilization and characterization of thermoalkalophilic lipases produced recombinantly from Bacillus thermocatenulatus BTL2 and Bacillus pumilus MBB03. For this purpose, immobilization of the produced enzymes in calcium-alginate@gelatin (Ca–Alg@gelatin) hydrogel beads, immobilization optimization and characterization measurements of the immobilized-enzyme hydrogels were conducted. Optimum temperature and pH values were determined for B. thermocatenulatus and B. pumilus MBB03 immobilized-enzyme hydrogels (60–70 °C, 55 °C and pH 9.5, pH 8.5). Thermal stability was determined between 65 °C and 60 °C of B. thermocatenulatus and B. pumilus MBB03 immobilized enzymes, respectively. The pH stability was determined between pH 7.0–11.0 at +4°C and pH 8.0–10.0 at +4 °C, respectively.
In conclusion, the entrapment technique provided controlled production of small diameter hydrogel beads (~ 0:19 and ~ 0:29) with negligible loss of enzyme. These beads retained high lipase activity at high pH and temperature. The activity of Ca–Alg@gelatin-immobilized lipase remained relatively stable for up to three cycles and then markedly decreased. With this enzyme immobilization, it may have a potential for use in esterification and transesterification reactions carried out in organic solvent environments. We can conclude that it is one of the most promising techniques for highly efficient and economically competent biotechnological processes in the field of biotransformation, diagnostics, pharmaceutical, food and detergent industries.
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Authors and Affiliations

Kezban Yildiz Dalginli
1
ORCID: ORCID
Onur Atakisi
2
ORCID: ORCID

  1. Department of Chemistry and Chemical Processing Technologies, Kars Vocational High School Kafkas University, Kars, Turkey
  2. Department of Chemistry, Faculty Science and Letter, Kafkas University, Kars, Turkey
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Abstract

In pursuit of increased efficiency and longer operating times of photovoltaic systems, one may encounter numerous difficulties in the form of defects that occur in both individual solar cells and whole modules. The causes of the occurrence range from structural defects to damage during assembly or, finally, wear and tear of the material due to operation. This article provides an overview of modern imaging methods used to detect various types of defects found in photovoltaic cells and panels. The first part reviews typical defects. The second part of the paper reviews imaging methods with examples of the authors’ own test results. The article concludes with recommendations and tables that provide a kind of comprehensive guide to the methods described, depending on the type of defects detected, the range of applicability, etc. The authors also shared their speculations on current trends and the possible path for further development and research in the field of solar cell defect analysis using imaging.
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Authors and Affiliations

Maurycy Maziuk
1
Laura Jasińska
1
Jarosław Domaradzki
1
Paweł Chodasewicz
1

  1. Wrocław University of Science and Technology, Faculty of Electronic, Photonics and Microsystems, Department ofElectronic and Photonic Metrology, Division of Thin Film Technologies, Wybrzeze Wyspianskiego 27, 50-370 Wrocław,Poland
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Abstract

Active thermography is an efficient tool for defect detection and characterization as it does not change the properties of tested materials. The detection and characterization process involves heating a sample and then analysing the thermal response. In this paper, a long heating pulse was used on samples with a low thermal diffusivity and artificially created holes of various depths. As a result of the experiments, heating and cooling curves were obtained. These curves, which describe local characteristics of the material, are recognized using a classification tree and divided into categories depending on the material thickness (hole depths). Two advantages of the proposed use of classification trees are: an in-built mechanism for feature selection and a strong reduction in the dimensions of the pattern. Based on the experimental study, it can be concluded that classification trees are a useful tool for the thinning detection of homogeneous material.
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Authors and Affiliations

Sebastian Dudzik
1
Grzegorz Dudek
1

  1. Czestochowa University of Technology, Faculty of Electrical Engineering, Al. Armii Krajowej 17, 42-200 Częstochowa, Poland
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Abstract

Members of Enterobacteriaceae are known to produce extended-spectrum beta-lactamases (ESBL) which hydrolyze the beta-lactam group of antibiotics. The existence of ESBL-producing Salmonella enterica ( S. enterica) and Escherichia coli ( E. coli) harbored by urban avifauna was investigated in this study. Dropping samples (n= 180) were collected from six different bird species in the district Jhang, Punjab province, Pakistan. Isolation and identification of ESBL isolates were made by using cefotaxime- (4 mg/L) supplemented MacConkey agar and double disc synergy test (DDST). Polymerase chain reaction (PCR) was performed for the detection of four different ESBL genes including bla CTX-M, bla TEM, bla SHV and bla OXA. A total of 42.69% isolates were confirmed as ESBL via DDST including 30.64% S. enterica and 49.54% E. coli. The incidence of ESBL S. enterica and ESBL E. coli was found highest in egret ( Ardea alba) and pigeon ( Columba livia) as 64.28% and 78.95%, respectively. The bla CTX-M gene was detected in 57.89% and 64.81% of isolates of S. enterica and E. coli, respectively. Among other genes in S. enterica and E. coli, bla TEM (21.05%, 20.4%); bla SHV (15.78%, 9.26%), and bla OXA (5.26%, 5.56%) were detected, respectively. All of the tested isolates were found resistant to at least one of the thirteen antimicrobial agents except meropenem. To the best of our knowledge, this is the first study reporting the incidence and genetic diversity of ESBL bacteria associated with urban avifauna in Pakistan. The urban avifauna can serve as a potential subject of bio-surveillance to monitor the emergence of antimicrobial-resistant bacteria.
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Authors and Affiliations

M.A. Saeed
1
U. Waheed
1
S. Ehtisham-ul-Haque
1
A.U. Khan
1
M. Kashif
2
M.F. Qamar
1
A. Ghafoor
3
M. Saqlain
1
J. Asghar
1

  1. Department of Pathobiology, University of Veterinary and Animal Sciences, Lahore, CVAS Campus, 12-Km Chiniot Road, Jhang, 35200, Pakistan
  2. Department of Clinical Sciences, University of Veterinary and Animal Sciences, Lahore, CVAS Campus, 12-Km Chiniot Road, Jhang, 35200, Pakistan
  3. Institute of Microbiology, University of Veterinary and Animal Sciences, Outfall Road, Lahore, 54000, Pakistan
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Abstract

Staphylococcus aureus (S. aureus) has been recognized as one of the important zoonotic pathogens. However, it was limited about the epidemiology and genetic characteristics of S. aureus isolated from pigs in Hunan province, china. The aim of this study was to determine the characteristics of 163 S. aureus isolated from 590 pigs in Hunan Province, China. All isolates were characterized by agr typing, detection of virulence genes and antibiotic resistance genes, lethal test of mice and antibiotic susceptibility tests. The results showed that 30 strains of the 163 isolates were divided into agrI (18.40%), agrII (36/163, 22.09%), agrIII (20/163, 12.27%,), agrIV (20/163,12.27%) and the remaining 57 isolates were amplified negative by agr primers. In the 163 isolates, the detection rate of the virulence genes hlb, hld, hla, icaA, seb, fnbA, eta, etb, sea, tst and pvl ranged from 2.45% to 100%. The 43 isolates that were lethal to the mice, had β-hemolytic activity, the number of virulence genes of which was 7.8% higher than that of the remaining 120 non-fatal strains. The resistance rates of the 163 isolates to the 15 antibiotics were 0% (0/163) - 100% (163/163). All isolates were susceptible to Vancomycin and only 7 isolates were methicillin - resistant S. aureus (MRSA). The detection rates of the 11 resistance genes was 0% (0/163) - 100% (163/163). This study first to describes the epidemiology and characteristics of S. aureus from pigs in Hunan Province, which will help in tracking the evolution of epidemic strains and preventing pig-human transmission events.

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Authors and Affiliations

X. Zhang
G. Wang
C. Yin
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Abstract

Characterization of sound absorbing materials is essential to predict its acoustic behaviour. The most commonly used models to do so consider the flow resistivity, porosity, and average fibre diameter as parameters to determine the acoustic impedance and sound absorbing coefficient. Besides direct experimental techniques, numerical approaches appear to be an alternative to estimate the material's parameters. In this work an inverse numerical method to obtain some parameters of a fibrous material is presented. Using measurements of the normal incidence sound absorption coefficient and then using the model proposed by Voronina, subsequent application of basic minimization techniques allows one to obtain the porosity, average fibre diameter and density of a sound absorbing material. The numerical results agree fairly well with the experimental data.

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Authors and Affiliations

Jesus Alba
Romina del Rey
Jaime Ramis
Jorge Arenas
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Abstract

It is well known that sound absorption and sound transmission properties of open porous materials are highly dependent on their airflow resistance values. Low values of airflow resistance indicate little resistance for air streaming through the porous material and high values are a sign that most of the pores inside the material are closed. The laboratory procedures for measuring airflow resistance have been stan- dardized by several organizations, including ISO and ASTM for both alternate flow and continuous flow. However, practical implementation of these standardized methods could be both complex and expensive. In this work, two indirect alternative measurement procedures were compared against the alternate flow standardized technique. The techniques were tested using three families of eco-friendly sound absorbent materials: recycled polyurethane foams, coconut natural fibres, and recycled polyester fibres. It is found that the values of airflow resistance measured using both alternative methods are very similar. There is also a good correlation between the values obtained through alternative and standardized methods.
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Authors and Affiliations

Romina del Rey
Jesus Alba
Jorge P. Arenas
Jaime Ramis
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Abstract

This work was carried out during two successive seasons (2016 and 2017) on cucumber fruits from a plastic greenhouse and from open field cultivation in El Gharbeia and El Giza Governorates, Egypt. Isolation trials from spoilage fruit samples of plastic greenhouse cultivation recorded high frequency of Alternaria tenusinium, Fusarium spp. and Pleospora alli. The most common fungi of rotten cucumber fruits from an open field were Galactomyces spp. and Fusarium spp. Pathogenicity tests proved that, Fusarium solani from El-Gharbeia followed by A. tenusinium from El-Giza were the most frequent isolates responsible for rot of cucumber fruits from plastic greenhouse cultivation. Moreover, the most frequent isolates causing postharvest disease of cucumber fruits of the open field were Galactomyces candidium from El-Giza followed by Geotrichum sp. and F. fujikuroi from El-Gharbeia Governorates, respectively. This is the first report of several fungi causing postharvest fruit rot disease of cucumber i.e., G. candidium, Geotrichum sp., A. tenusinium, P. alli and Fusarium spp. (F. fujikuroi, F. verticiolides, F. solani, F. geraminearium and Fusarium incarnatum). Fungal isolates were identified according to cultural, morphological and molecular characterization based on sequencing of internal transcribed spacer1 (ITS1). All the ITS nucleotide sequences of fungi were applied and conserved in GenBank.

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Authors and Affiliations

El Sayed Hussein Ziedan
Abd El-Nasser Abd El-Hafez Khattab
Ahmed Farahat Sahab
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Abstract

The proposed paper discusses the design and characterization of a soft miniature Magneto-Rheological (MR) shock absorber. In particular, the final application considered for the insertion of the designed devices is a controllable variable stiffness sole for patients with foot neuropathy. Such application imposes particularly challenging constraints in terms of miniaturization (cross-sectional area ≤ 1.5 cm2, height ≤ 25 mm) and high sustainable loads (normal loads up to 60 N and shear stresses at the foot/device interface up to 80 kPa) while ensuring moderate to low level of power consumption. Initial design considerations are done to introduce and justify the chosen novel configuration of soft shock absorber embedding a MR valve as the core control element. Successively, the dimensioning of two different MR valves typologies is discussed. In particular, for each configuration two design scenarios are evaluated and consequently two sets of valves satisfying different specifications are manufactured. The obtained prototypes result in miniature modules (external diam. ≤ 15 mm, overall height ≤ 30 mm) with low power consumption (from a minimum of 63 mW to a max. of 110 mW) and able to sustain a load up to 65 N. Finally, experimental sessions are performed to test the behaviour of the realized shock absorbers and results are presented.

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Authors and Affiliations

Daniel Grivon
Yoan Civet
Zoltan Pataky
Yves Perriard
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Abstract

AISI 52100 bearing steels are commonly used in applications requiring high hardness and abrasion resistance. The bearing steels are

working under dynamic loads in service conditions and their toughness properties become important. In order to provide the desired

mechanical properties, various heat treatments (austenizing, quenching and tempering) are usually applied. In this study, AISI 52100

bearing steel samples were austenized at 900°C for ½ h and water quenched to room temperature. Then tempering was carried out at

795°C, 400°C and 200°C for ½ h. In order to investigate the effect of heat treatment conditions on wear behavior, dry friction tests were

performed according to ASTM G99-05 Standard with a ‘ball-on-disk’ type tribometer. The samples were tested against steel and ceramic

counterparts using the parameters of 100 m distance and 30 N load and 0.063 m/s rotational speed. After wear test, the surface

characterization was carried out using microscopy. Wear loss values were calculated using a novel optical method on both flat and

counterpart specimens.

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Authors and Affiliations

E. Türedi
M. Yilmaz
V. Senol
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Abstract

In the present investigation, the morphology of Ti inclusions in high strength tire cord steel was investigated and their precipitation behavior was discussed using a precipitation and growth model. The results show that Ti inclusions mainly exist in the form of TiN. The two-dimensional characterization of Ti inclusions is square-like with sharp edges and corners, while its three-dimensional shape exhibits a cubic or rectangular-prism morphology. The Ti inclusions do not precipitate when the solid fraction of tire cord during solidification is less than 0.987, and their final radius is closely related to the cooling rate and initial concentration product. The higher the cooling speed, the smaller the final radius, when the cooling speed is constant, the final radius of Ti inclusions is mainly determined by the initial concentration product, w[N]0×w[Ti]0. In order to retard the precipitation and growth of Ti inclusions in tire cord steel, the cooling rate and initial concentration product can be taken into consideration.

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Authors and Affiliations

Jialiu Lei
Dongnan Zhao
Yongjun Fu
Xianfeng Xu
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Abstract

In this paper, the authors investigated the size distribution of titanium oxide (TiO2), titanium nitride (TiN) and titanium carbide (TiC) inclusions in a titanium deoxidized 4130 steel and compared it with the 4130 base alloy composition inclusions. TiN and TiC inclusions are of particular interest due to their role as heterogeneous nuclei for various phase reactions in steels. Two types of samples were prepared, a polished sample and a filtered sample. Electrolytic dissolution was employed to make the filter paper samples. The size range of titanium inclusions was found to be more than that of the non-metallic inclusions from 4130 base alloy heat. Titanium inclusions from the filter and polished samples were round in shape. TiC and TiN inclusions were not found in the electrolytic extraction samples. Inclusions and their chemistries were analyzed using scanning electron microscope and energy dispersive spectrometer. The inclusion size range was larger for the titanium deoxidized samples than the base alloy. However, in both steels the majority of inclusions had a size smaller than 10 μm.

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Authors and Affiliations

R.B. Tuttle
S. Kottala
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Abstract

The proper interaction of bone tissue - the natural porous biomaterial - with a porous coated intra-osseous implant is conditioned, among others, by the implant porous coating poroaccessibility for bone tissue adaptive ingrowth. The poroaccessibility is the ability of implant porous coating outer layer to accommodate the ingrowing bone tissue filling in its pore space and effective new formed bone mineralizing in the pores to form a biomechanically functional bone-implant fixation. The functional features of the microtopography of intra-osseous implant porous surfaces together with the porosity of pore space of the outer layer of the porous coating are called by bioengineers the porostructural-osteoconductive properties of the porous coated implant. The properties are crucial for successful adaptive bone tissue ingrowth and further long-term (secondary) biomechanical stability of the boneimplant interface. The poroaccessibility of intra-osseous implants porous coating outer layers is characterized by - the introduced in our previous papers - set of stereometric parameters of poroaccessibility: the effective volumetric porosity fVef, the index of the porous coating space capacity VPM, the representative surface porosity fSrep, the representative pore size pSrep, the representative angle of the poroaccessibility Wrep and the bone-implant interface adhesive surface enlargement index y. Presented in this paper, an original method of evaluation of the porostructural-osteoconductive properties of intra-osseous implant porous coatings outer layer by means of the parameters of poroaccessibility was preliminary verified during experimental tests performed on the representative examples of porous coated femoral stems and acetabular cups of various hip endoprostheses. The computer-aided stereometric evaluation of the microstructure of implant porous coatings outer layer can be now realized by the authoring application software PoroAccess_1.0 elaborated in our research team in Java programming language

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Authors and Affiliations

Ryszard Uklejewski
Mariusz Winiecki
Piotr Rogala
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Abstract

In the paper a method using active thermography and a neural algorithm for material defect characterization is presented. Experimental investigations are conducted with the stepped heating method, so-called time-resolved infrared radiometry, for the test specimen made of a material with low thermal diffusivity. The results of the experimental investigations were used in simulations of artificial neural networks. Simulations are performed for three datasets representing three stages of the heating process occurring in the investigated sample. In this work, the simulation research aimed to determine the accuracy of defect depth estimation with the use of the mentioned algorithm is descibed

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Authors and Affiliations

Sebastian Dudzik
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Abstract

This work reports the results of a study of Mo thin films synthesis by DC Pulsed Magnetron Sputtering method (PMS), operating at pulse main frequency of 100 kHz and modulated by the additional modulation frequency, driving in the range of 5-1000 Hz (modulated Pulse Magnetron Sputtering – mPMS). We have studied the influence of mPMS on plasma chemical reactions and mechanisms of layer growth using optical emission spectroscopy technique. Our experiment showed strong influence of mPMS method, on the morphology (scanning electron microscopy), phase composition (X-ray diffractometry) and electric properties (4-point probes method) of nanocrystalline and amorphous Mo films. From the utilitarian point of view, low value of resistivity – 43,2 μΩcm of synthesized Mo films predestines them as back contacts for thin solar cells CIGS. Our results revealed that additional modulation frequency should be considered as an important factor for optimization of films synthesis by means of PMS-based methods.

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Authors and Affiliations

B. Wicher
R. Chodun
K. Nowakowska-Langier
S. Okrasa
K. Król
R. Minikayev
G. Strzelecki
K. Zdunek
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Abstract

Photonic devices often use light delivered by a single-mode telecommunication fibre. However, as the diameter of the core of the optical fibre is of 10 microns, and the transverse dimensions of the photonic waveguides are usually micrometer or less, there is an issue of incompatibility. The problem may be solved by application of tapered optical fibres. For efficient light coupling, the taper should be prepared so as to create a beam of long focal length and small spot diameter in the focus. The article describes the design, fabrication and characterization of tapered optical fibres prepared with a fibre-optic fusion splicer. We modelled the tapers with FDTD method, for estimation of the influence of the tapered length and angle on the spot diameter and the focal length of an outgoing beam. We fabricated tapers from a standard single mode fibre by the Ericsson 995 PMfi- bre-optic fusion splicer. We planned the splicing technology so as to get the needed features of the beam. We planned a multistep fusion process, with optimized fusion current and fusion time. The experimental measurements of best tapered optical fibres were carried out by the knife-edge method.

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Authors and Affiliations

A. Zakrzewski
A. Pięta
S. Patela
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Abstract

We describe a new method to separate ballistic from the scattered photons for optical tissue characterization. It is based on the hypothesis that the scattered photons acquire a phase delay. The photons passing through the sample without scattering or absorption preserve their coherence so they may participate in interference. We implement a Mach−Zehnder experimental setup where the ballistic photons pass through the sample with the delay caused uniquely by the sample indices of refraction. We incorporate a movable mirror on the piezoelectric actuator in the sample arm to detect the amplitude of the modulation term. We present the theory that predicts the path−integrated (or total) concentration of the scattering and absorption centres. The proposed technique may characterize samples with transmission attenuation of ballistic photons by a factor of 10-14.

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Authors and Affiliations

F. Corral
M. Strojnik
G. Paez

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