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Number of results: 87
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Abstract

Large elongation in one de?nite direction of a crystal of cubic symmetry is considered. The equations of second order elasticity theory are applied. In this approximation three constants of the second order and six constants of the third order characterize the crystal. The stress is a function of the elongation direction. The elongation directions for which the stress reaches an extreme value have been analyzed.

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Authors and Affiliations

Z. Wesołowski
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Abstract

There exists a problem with an in situ diagnostics of contamination of ethyl alcohol in a human being exhaled air. When ethyl alcohol in a mouth blowing (in a gaseous state) exists, the characteristic C–H stretch absorption bands in –CH3 and –CH2 – functional groups in ethanol (CH3–CH2–OH) appear at a wavelength of λ = 3.42 μm. To investigate the presence of ethyl alcohol in exhaled human air, the light beam of λ = 3.42 μm is passing through an air sample. If one alternately measures the intensity of the investigated beam and the reference, a percentage of ethanol in the air sample can be estimated using a sensitive nondispersive infrared (NDIR) system with a stable operating flow mass detector. To eliminate a mechanical chopper and noise generating stepper motors, a photonic chopper as a liquid crystal shutter for λ = 3.42 μm has been designed. For this purpose, an innovative infrared nematic liquid crystal mixture was intentionally prepared. The working mixture was obtained by a selective removal of CH bonds and its exchange by heavier polar substituents, what ensures a lack of absorption band of C–H bonds. The paper presents theory, concept and final experimental results of the infrared nematic liquid crystals mixture and the liquid crystal shutter for breathalyzer applications.

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Authors and Affiliations

W. Piecek
L. Jaroszewicz
E. Miszczyk
Z. Raszewski
M. Mrukiewicz
P. Kula
K. Jasek
P. Perkowski
E. Nowinowski-Kruszelnicki
J. Zieliński
J. Kędzierski
M. Olifierczuk
U. Chodorow
P. Morawiak
R. Mazur
K. Kowiorski
P. Harmata
J. Herman
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Abstract

The paper presents the properties of a strain sensor, which was made using the micro hole collapse method and operates in the configuration of a Mach-Zehnder modal interferometer with a PM-1550-01 polarization maintaining photonic crystal fibre. The sensor’s transfer curve was determined analytically. Its strain sensitivity, determined from measurements, decreases slightly with increasing wavelength and is in a range from −2.01 to −2.23 pm/µε in the wavelength range 1520–1580 nm. Based on the Fourier analysis of the wavelength spectrum of the constructed sensor, the difference of the group refractive indices of the core and the cladding of the photonic crystal fibre was determined, which are in a range from 7.45·10−3 to 1.01·10−2. The temperature sensitivity of the sensor, determined on the basis of measurements performed in a range from 23 to 60◦C, is positive and equals 5.9 pm/K.
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Authors and Affiliations

Cezary Kaczmarek
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Abstract

The aim of this work was to induce permanent birefringence both in typical liquid crystal cells and photonic crystal fibers (PCFs) by photo-polymerization. For this purpose three different liquid crystalline materials, namely E7, 5CB, and 6CHBT were combined with a mixture of RM257 monomer and a UV sensitive initiator with the percentage weight less than 10%. Due to the photo-polymerization process it was possible to achieve polymer-stabilized liquid crystal orientation inside LC cells and micro-sized cylindrical glass tubes. In particular, periodic change in spatial molecular orientation was achieved by selective photo-polymerization. Successful results obtained in these simple geometries allowed for the experimental procedure to be repeated in PCFs leading to locally-induced permanent birefringence in PCFs.

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Authors and Affiliations

M.S. Chychłowski
S. Ertman
K. Rutkowska
O. Strzeżysz
R. Dąbrowski
T.R. Woliński
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Abstract

In this work studies on propagation properties of a microstructured polymer optical fibre infiltrated with a nematic liquid crystal are presented. Specifically, the influence of an infiltration method on the LC molecular alignment inside fibre air-channels and, thus, on light guidance is discussed. Switching between propagation mechanisms, namely the transition from modified total internal reflection (mTIR) to the photonic bandgap effect obtained by varying external temperature is also demonstrated.

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Authors and Affiliations

K.A. Rutkowska
K. Milenko
O. Chojnowska
R. Dąbrowski
T.R. Woliński
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Abstract

Some eutectic stripes have been generated in a hexagonal (Zn) - single crystal. The stripes are situated periodically with the constant interstripes

spacing. The eutectic structure in the stripes consists of strengthening inter-metallic compound, Zn16Ti, and (Zn) – solid solution.

The rod-like irregular eutectic structure (with branches) appears at low growth rates. The regular lamellar eutectic structure is observed at

middle growth rates. The regular rod-like eutectic structure exists exclusively in the stripes at some elevated growth rates. A new

thermodynamic criterion is recommended. It suggests that this eutectic regular structure is the winner in a morphological competition for

which the minimum entropy production is lower. A competition between the regular rod-like and the regular lamellar eutectic growth is

described by means of the proposed criterion. The formation of branches within irregular eutectic structure is referred to the state of

marginal stability. A continuous transitions from the marginal stability to the stationary state are confirmed by the continuous

transformations of the irregular eutectic structure into the regular one.

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Authors and Affiliations

J. Szajnar
W. Wołczyński
S. Kjelstrup
D. Bedeaux
B. Billia
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Abstract

A liquid crystal display (LCD) recycling process is needed to increase its efficiency by recovering the resources in addition to metals and plastics. This study investigates the pre-treatment process for recycling LCD glass. Recycling pre-treatment includes dismantling the LCD from the waste product, crushing the glass, and separating the glass particles from the impurities. Scanning electron microscopy confirmed that the oscillation milling process is more effective in maintaining uniform powder shape and size as compared to the cut milling process. The glass particles crushed by the oscillating mill, optimized at 1500 rpm, had a uniformly distributed particle size of less than 10 µm. These small particles were separated from the organic impurities, achieving a 98% pure powder that can be used as recycled raw materials. The proposed pre-treatment process for recycling LCD glass will enhance the ability to use waste glass as a valuable resource in the manufacturing of future displays.

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Authors and Affiliations

Seyul Kim
Yubin Kang
Leeseung Kang
Hyun Seon Hong
Chan Gi Lee
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Abstract

The paper presents the application of liquid crystal thermography for temperature determination and visualisation of two phase flow images on the studied surface. Properties and applications of thermochromic liquid crystals are discussed. Liquid crystals were applied for two-dimensional detection of the temperature of the heating foil forming one of the surfaces of the minichannel along which the cooling liquid flowed. The heat flux supplied to the heating surface was altered in the investigation and it was accompanied by a change in the color distribution on the surface. The accuracy of temperature measurements on the surface with liquid crystal thermography is estimated. The method of visualisation of two-phase flow structures is described. The analysis of monochrome images of flow structures was employed to calculate the void fraction for some cross-sections. The flow structure photos were processed using Corel graphics software and binarized. The analysis of phase volumes employed Techsystem Globe software. The measurement error of void fraction is estimated.

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Authors and Affiliations

Magdalena Piasecka
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Abstract

Polarimetric optical fiber sensors based on highly birefringent (HB) polarization-maintaining fibers have focused great interest for last decades. The paper presents a novel modular fiber optic sensing system of potential industrial applications to measure temperature, hydrostatic pressure, and strain that is based on classical HB and photonic crystal fibers and can operate at visible and infrared wavelengths. The main idea of the system is a novel and replaceable fiber-optic head, which allows adjusting the measuring system both to the required range and type (strain, pressure or temperature) of the external measurand. We propose also a new configuration of the fiber optic strain gauge with a free cylinder and an all-fiber built-in analyzer based on the photonic crystal fiber filled with a liquid crystal. Additionally, strain sensitivities of various HB fibers operating at visible and infrared wavelengths range have been measured.

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Authors and Affiliations

T.R. Woliński
P. Lesiak
A.W. Domański
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Abstract

In article a two-dimensional photonic crystal (PhC) is considered and modelled as a new generation antireflection coating for optoelectronic devices. Traditional antireflective coatings (ARCs) reduce the reflection of the radiation only – the new generation of antireflective coatings should affect the distribution of the radiation also. Such functionality can be provided by the two-dimensional PhC which reduce the reflection and scatter transmitted light. Prior to the fabrication, the PhCs should be designed and analysed. Results of the analysis should provide quantitative means for choice of materials and design solutions. In work, we analyse the electromagnetic field distribution as Poynting vectors inside the materials of optoelectronic devices, in order to investigate the possibility of improving the construction of future optoelectronic devices. Furthermore, we calculate the reflection and transmission of that ARC. It’s a complex optic analysis of new generation of ARC. The numerical analysis has been performed with the FDTD method in Lumerical Software. In work, we consider the two-dimensional photonic crystal on the top surface of optoelectronic structures. We compared the results with the traditional ARC from these same parameters as PhC: thickness and material. As an example, we presented the application of modelled, photonic crystal, thin-film, GaAs solar cells with PhC on top. The efficiency of this solar cell, using the photonic crystal, was improved by 6.3% over the efficiency of this same solar cell without PhC. Thus, our research strongly suggests that the unique properties of the photonic crystal could be used as a new generation of ARC.

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Authors and Affiliations

D. Przybylski
S. Patela
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Abstract

A dual-wavelength optical polarimetric approach has been proposed as a means of elimination of the systematic errors and estimation of the optical anisotropy parameters for a single DKDP crystal. Our HAUP-related polarimeter uses two semiconductor lasers with the neighbouring wavelengths of 635 nm and 650 nm. Based on the temperature dependence analysis of small characteristic azimuths of light polarization with respect to the axis of the sample, we found the parameters of imperfections of polarization system. We acquired eigen waves ellipticities in a DKDP crystal and found perpendicular to the optic axis value of the optical rotatory power. Our results correlate positively with previously measured data for KDP crystals.

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Authors and Affiliations

Y. Shopa
M. Shopa
N. Ftomyn
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Abstract

The paper presents research of metallic glass based on a Mg72Zn24Ca4 alloy. Metallic glass was prepared using induction melting and further injection on a spinning copper wheel. The X-ray diffractometer and differential scanning calorimeter (DSC) were used to investigate the phase transformation of the amorphous ribbon. The heat released in the crystallization process, during isothermal annealing, based on the differential scanning calorimeter investigation, was determined to be 166.18 Jg-1. The effect of isothermal annealing temperature on the kinetics of the amorphous alloy crystallization process using differential scanning calorimeter was investigated. For this purpose, two isothermal annealing temperatures were selected. The incubation time decreases as the temperature of the isothermal annealing increases from 300 to 252 seconds. The same relationship is visible in the case of duration of the phase transformation, which also decreases as the temperature of the isothermal annealing increases from 360 to 228 seconds. The obtained results show a significant influence of isothermal annealing temperature on the degree of phase transformation.

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Authors and Affiliations

J. Lelito
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Abstract

The chemical composition of alloys plays an important role at their crystallization and influences the solid phase formation, and thus, microstructure and properties. The present paper studies the release of the heat of crystallization of alloyed wear-resistant cast irons in order to determine the quantitative patterns of the chemical composition influence to the kinetics of crystallization. The differential thermal analysis was applied to get the data of heat release, its rate at cast iron temperature decrease. The normalized dependence of the amount of crystallization heat over time was obtained. The main temperature parameters were analyzed and four stages at irons crystallization were established and characterized with their duration and released heat. The multiple correlation analysis allowed considering a numerous physical and chemical factors and distinguishing their role at crystallization of irons. As a result, the quantitative regularities are determined of influencing the content of alloying elements, impurities and carbides on a heat and time of crystallization at the different stages of solidification, which are of great importance in developing alloyed irons with required quality and properties.
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Authors and Affiliations

Y. Aftandiliants
1
ORCID: ORCID
S. Gnyloskurenko
1 2
ORCID: ORCID
H. Meniailo
3
ORCID: ORCID
V. Khrychikov
3
ORCID: ORCID
V. Lomakin
4
ORCID: ORCID

  1. National University of Life and Environmental Sciences of Ukraine, Ukraine
  2. Physical and Technological Institute of Metals and Alloys, National Academy of Sciences of Ukraine, Ukraine
  3. Ukrainian State University of Science and Technologies, Ukraine
  4. Central Ukrainian National Technical University, Ukraine
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Abstract

The paper presents the effect of manganese on the crystallization process, microstructure and selected properties: cast iron hardness as well as ferrite and pearlite microhardness. The compacted graphite was obtained by Inmold technology. The lack of significant effect on the temperature of the eutectic transformation was demonstrated. On the other hand, a significant reduction in the eutectoid transformation temperature with increasing manganese concentration has been shown. The effect of manganese on microstructure of cast iron with compacted graphite considering casting wall thickness was investigated and described. The nomograms describing the microstructure of compacted graphite iron versus manganese concentration were developed. The effect of manganese on the hardness of cast iron and microhardness of ferrite and pearlite were given.

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Authors and Affiliations

Grzegorz Gumienny
ORCID: ORCID
B. Kurowska
ORCID: ORCID
P. Just
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Abstract

A brief description of the innovative mathematical method for the prediction of CET – localization in solidifying copper and copper alloys’ ingots is presented. The method is to be preceded by the numerical simulation of both temperature field and thermal gradient filed. All typical structural zones were revealed within the copper and copper alloys’ massive ingots or rods manufactured by continuous casting. The role of thermal gradient direction for the single crystal core formation has been enlightened. The definition for the index describing proportion between volume fraction of the columnar structure and volume fraction of the equiaxed structure has been formulated by means of the interpretation of some features of the liquidus isotherm velocity course. An attempt has been undertaken to apply the developed mathematical method for the structural zones prediction in the rods solidifying under industrial conditions. An industrial application has been shown, that is, it was explained why the innovative rods should be assigned to the overhead conductors in the electric tractions.
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Authors and Affiliations

P. Kwapisiński
1
ORCID: ORCID
W. Wołczyński
2
ORCID: ORCID

  1. KGHM Polska Miedź S.A., M. Skłodowskiej-Curie 48, 59-301 Lubin, Poland
  2. Institute of Metallurgy and Materials Science, W. Reymonta 25, 30-059 Kraków, Poland
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Abstract

The article presents a study of a hybrid structure based on the combination of a tapered optical fibre and gold nanoparticles dispersed in a liquid crystal material. Sensitivity to changes of the refractive index of the environment in which the structure is located, as well as the possibility of changing the refractive index of liquid crystals by external factors, such as temperature and electric field, were investigated. Electro- and thermally-induced changes of the refractive index of a liquid crystal through the rotation of a molecule director, which cause changes in the light propagated in a tapered optical fibre, were described. The most important issue in the article is to determine the influence of doping a liquid crystal with gold nanoparticles the concentration of which varies between 0.1 and 0.3 wt.%. The paper presents transmission measurements in a wide optical range depending on voltage, temperature, and frequency changes. Additionally, time courses of the obtained signal were measured. The study shows that the appropriate selection of nanoparticle concentration has a huge impact on the optical wave propagation. The experimental results show that the optical changes obtained for the investigated hybrid structure prefer it for use as an electro-optical switcher, filter, or sensor.
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Authors and Affiliations

Joanna E. Moś
1
ORCID: ORCID
Karol A. Stasiewicz
1
ORCID: ORCID
Leszek R. Jaroszewicz
1
ORCID: ORCID

  1. Faculty of New Technologies and Chemistry, Military University of Technology, 2 Kaliskiego St., 00-908 Warsaw, Poland
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Abstract

Nowadays, the energy cost is very high and this problem is carried out to seek techniques for improvement of the aerothermal and thermal (heat flow) systems performances in different technical applications. The transient and steady-state techniques with liquid crystals for the surface temperature and heat transfer coefficient or Nusselt number distribution measurements have been developed. The flow pattern produced by transverse vortex generators (ribs) and other fluid obstacles (e.g. turbine blades) was visualized using liquid crystals (Liquid Crystal Thermography) in combination with the true-colour image processing as well as planar beam of double-impulse laser tailored by a cylindrical lens and oil particles (particle image velocimetry or laser anemometry). Experiments using both research tools were performed at Gdańsk University of Technology, Faculty of Mechanical Engineering. Present work provides selected results obtained during this research.

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Authors and Affiliations

Jan A. Stąsiek
Marcin Jewartowski
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Abstract

A sonic crystal consists of a finite-size periodic array of scatters embedded in a background material. One of the fascinating properties of sonic crystals is the focusing phenomenon. In this study, the near field focusing effect of a solid-air 2D sonic crystal lens with a square lattice configuration is investigated in the second frequency band. The band structure and equifrequency contour of the crystal are analyzed to reveal the dispersion of an acoustic wave on the crystal structure. The frequency dependence of the acoustic wave focalization by the sonic crystal flat lens is demonstrated via Finite Difference Time Domain simulation results and experimental measurements.

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Serkan Alagoz
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Abstract

PCFs (Photonic Crystal Fibers) with ‘T’ – shaped core have been proposed in this paper. ‘T’ –shaped core PCF structures have been analyzed using two different background materials: silica and lead silicate. A total of 3600 rotation at an interval of 900 has been introduced in the design of PCF structures. PCF structures A, B, C and D with rotation of 00, 900, 1800 and 2700 have silica as wafer. Similarly PCF structures E, F, G and H with similar rotation have lead silicate as background material. Numerical investigations shows structures ‘D’, ‘F’, ‘G’ and ‘H’ to have anomalous dispersion. PCF structures ‘F’, ‘G’, and ‘H’ have reported birefringence of the order of 10-2. Besides, other PCF structures report birefringence of the order of 10-3. Ultra low confinement loss has been observed in all the investigated PCF structures. Moreover, splice loss observed by the structure is very low. Large mode area has been shown by all the designed PCF structures.

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Authors and Affiliations

Pranaw Kumar
Amrit Tripathy
Jibendu Sekhar Roy
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Abstract

This paper outlines a measurement method of properties of microstructured optical fibers that are useful in sensing applications. Experimental studies of produced photonic-crystal fibers allow for a better understanding of the principles of energy coupling in photonic-crystal fibers. For that purpose, fibers with different filling factors and lattice constants were produced. The measurements demonstrated the influence of the fiber geometry on the coupling level of light between the cores. For a distance between the cores of 15 μm, a very low level (below 2%) of energy coupling was obtained. For a distance of 13 μm, the level of energy transfer to neighboring cores on the order of 2-4% was achieved for a filling factor of 0.29. The elimination of the energycoupling phenomenon between the cores was achieved by duplicating the filling factor of the fiber. The coupling level was as high as 22% in the case of fibers with a distance between the cores of 8.5 μm. Our results can be used for microstructured-fiber sensing applications and for transmission-channel switching in liquid-crystal multi-core photonic fibers.

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Jacek Klimek
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Abstract

The analysis of influence of mould withdrawal rate on the solidification process of CMSX-4 single crystal castings produced by Bridgman

method was presented in this paper. The predicted values of temperature gradient, solidification and cooling rate, were determined at the

longitudinal section of casting blade withdrawn at rate from 1 to 6mm/min using ProCAST software. It was found that the increase of

withdrawal rate of ceramic mould results in the decrease of temperature gradient and the growth of cooling rate, along blade height. Based

on results of solidification parameter G/R (temperature gradient/solidification rate), maximum withdrawal rate of ceramic mould

(3.5 mm/min), which ensures lower susceptibility to formation process of new grain defects in single crystal, was established. It was

proved that these defects can be formed in the bottom part of casting at withdrawal rate of 4 mm/min. The increase of withdrawal rate to 5

and 6 mm/min results in additional growth of susceptibility of defects formation along the whole height of airfoil.

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Authors and Affiliations

J. Sieniawski
D. Szeliga
K. Kubiak
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Abstract

Rare earth Nd-Fe-B, a widely used magnet composition, was synthesized in a shape of powders using gas atomization, a rapid solidification based process. The microstructure and properties were investigated in accordance with solidification rate and densification. Detailed microstructural characterization was performed by using scanning electron microscope (SEM) and the structural properties were measured by using X-ray diffraction. Iron in the form of α-Fe phase was observed in powder of about 30 μm. It was expected that fraction of Nd2Fe14B phase increased rapidly with decrease in powder size, on the other hand that of α-Fe phase was decreased. Nd-rich phase diffused from grain boundary to particle boundary after hot deformation due to capillary action. The coercivity of the alloy decreased with increase in powder size. After hot deformation, Nd2Fe14B phase tend to align to c-axis.

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Authors and Affiliations

Ju-Young Cho
Sardar Farhat Abbas
Yong-Ho Choa
Taek-Soo Kim
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Abstract

Specimens of Si single crystals with different crystal orientation [100] and [110] were studied by Electro-Ultrasonic Spectroscopy (EUS) and Resonant Ultrasonic Spectroscopy (RUS). A silicon single crystal is an anisotropic crystal, so its properties are different in different directions in the material relative to the crystal orientation. EUS is based on interaction of two signals: an electric AC signal and an ultrasonic signal, which are working on different frequencies. The ultrasonic wave affects the charge carriers' transport in the structures and the intermodulation electrical signal which is created due to the interaction between the ultrasonic wave and charge carriers, is proportional to the density of structural defects. RUS enables to measure natural frequencies of free elastic vibrations of a simply shaped specimen by scanning a selected frequency range including the appropriate resonances of the measured specimens.

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Authors and Affiliations

Petr Sedlak
Pavel Tofel
Vlasta Sedlakova
Jiri Majzner
Josef Sikula
Lech Hasse

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