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Abstract

In this study, stainless steel 316L and Inconel 625 alloy powders were additively manufactured by using directed energy deposition process. And heat treatment effect on hardness and microstructures of the bonded stainless steel 316L/Inconel 625 sample was investigated. The microstructures shows there are no secondary phases and big inclusions near interfacial region between stainless steel 316L and Inconel 625 except several small cracks. The results of TEM and Vickers Hardness show the interfacial area have a few tens of micrometers in thickness. Interestingly, as the heat treatment temperature increases, the cracks in the stainless steel region does not change in morphology while both hardness values of stainless steel 316L and Inconel 625 decrease. These results can be used for designing pipes and valves with surface treatment of Inconel material based on stainless steel 316L material using the directed energy deposition.
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Bibliography

[1] G .H. Shin, J.P. Choi, K.T. Kim, B.K. Kimm, J.H. Yu, J. Korean Powder Metall. Inst. 24, 210 (2017).
[2] A. Ambrosi, M. Pumera, Chem. Soc. Rev. 45, 2740 (2016).
[3] G .S. Lee, Y.S. Eom, K.T. Kim, B.K. Kim, J. H. Yu, J. Korean Powder Metall. Inst. 26, 138 (2019).
[4] Y.S. Eom, D.W. Kim, K.T. Kim, S.S. Yang, J. Choe, I. Son, J.H. Yu, J. Korean Powder Metall. Inst. 27, 103 (2020).
[5] J. Hwang, S. Shin, J. Lee, S. Kim, H. Kim, Journal of Welding and Joining 35, 28 (2017).
[6] I . Gibson, D. Rosen, B. Stucker, Additive Manufacturing Technologies, Springer New York, 245 (2015).
[7] A. Saboori, D. Gallo, S. Biamino, P. Fino, M. Lombardi, Appl. Sci. 7, 883 (2017).
[8] J.S. Park, M.-G. Lee, Y.-J. Cho, J. H. Sung, M.-S. Jeong, S.-K. Lee, Y.-J. Choi, D.H. Kim, Met. Mater. Int. 22, 143 (2016).
[9] R . Koike, I. Unotoro, Y. Kakinuma, Y. Oda, Int. J. Autom. Techno. 13, 3 (2019).
[10] D.R. Feenstra, A. Molotnikov, N. Birbilis, J. Mater. Sci. 55, 13314- 13328 (2020).
[11] B.E. Carroll, R.A. Otis, J.P. Borgonia, J. Suh, R.P. Dillon, A.A. Shapiro, D.C. Hofmann, Z.-K. Liu, A. M. Beese, Acta Mater. 108, 46 (2016).
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[15] Y.S. Eom, K.T. Kim, S. Jung, J.H. Yu, D.Y. Yang, J. Choe, C.Y. Sim, S.J. An, J. Korean Powder Metall. Inst. 27, 219 (2020).
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Authors and Affiliations

Yeong Seong Eom
1 2
Kyung Tae Kim
1
Dong Won Kim
1
Ji Hun Yu
1
Chul Yong Sim
3
Seung Jun An
3
Yong-Ha Park
4
Injoon Son
2
ORCID: ORCID

  1. Korea Institute of Materials Science, 797 Changwon-daero, Changwon, Republic of Korea
  2. Kyungpook National University, 80 Daehakro, Bukgu, Daegu 41566, Republic of Korea
  3. Insstek, Daejeon, Republic of Korea
  4. Samsung Heavy Industries, Geoje-si, Republic of Korea
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Abstract

Direct energy deposition (DED) is a three-dimensional (3D) deposition technique that uses metallic powder; it is a multi-bead, multi-layered deposition technique. This study investigates the dependence of the defects of the 3D deposition and the process parameters of the DED technique as well as deposition characteristics and the hardness properties of the deposited material. In this study, high-thermal-conductivity steel (HTCS-150) was deposited onto a JIS SKD61 substrate. In single bead deposition experiments, the height and width of the single bead became bigger with increasing the laser power. The powder feeding rate affected only the height, which increased as the powder feeding rate rose. The scanning speed inversely affected the height, unlike the powder feeding rate. The multi-layered deposition was characterized by pores, a lack of fusion, pores formed by evaporated gas, and pores formed by non-molten metal inside the deposited material. The porosity was quantitatively measured in cross-sections of the depositions, revealing that the lack of fusion tended to increase as the laser power decreased; however, the powder feeding rate and overlap width increased. The pores formed by evaporated gas and non-molten metal tended to increase with rising the laser power and powder feeding rate; however, the overlap width decreased. Finally, measurement of the hardness of the deposited material at 25℃, 300℃, and 600℃ revealed that it had a higher hardness than the conventional annealed SKD61.

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Authors and Affiliations

Jong-Youn Son
Gwang-Yong Shin
Ki-Yong Lee
Hi-Seak Yoon
Do-Sik Shim
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Abstract

This study investigated the effect of heat treatment on the microstructure and impact toughness property of AISI D2 manufactured with direct energy deposition (DED) and compared the results with conventional wrought material. The fracture crack propagation behavior was examined in connection with microstructures through fracture surface analysis. AISI D2 manufactured with DED had a eutectic structure that turned into a net-type carbide after heat treatment, and Cr-rich needle-type secondary carbide was observed. Impact toughness of DED AISI D2 measured 2.0 J/cm2 in the as-built sample and 1.1 J/cm2 in the heat-treated sample. Compared to a wrought heat-treated AISI D2, DED AISI D2 had relatively low impact toughness. DED AISI D2 and wrought material had different crack propagation mechanisms. In DED AISI D2, the eutectic structure and net-type carbide boundary were identified as the major microstructural factor decreasing impact toughness.
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Authors and Affiliations

Jung-Hyun Park
1
ORCID: ORCID
Kyu-Sik Kim
1
ORCID: ORCID
Yong-Mo Koo
2
ORCID: ORCID
Jin-Young Kim
3
ORCID: ORCID
Min-Chul Kim
4
Kee-Ahn Lee
1
ORCID: ORCID

  1. Inha University, Department of Materials Science and Engineering, Incheon 22212, Korea
  2. Changsung Corp., Incheon, 21628, Korea
  3. Maxrotech Corp., Daegu, 42703, Korea
  4. Korea Atomic Energy Research Institute (KAERI), Daejeon 34057, Korea
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Abstract

Molybdenum (Mo) is used to form a barrier layer for metal wiring in displays or semiconductor devices. Recently, researches have been continuously attempted to fabricate Mo sputtering targets through additive manufacturing. In this study, spherical Mo powders with an average particle size of about 37 um were manufactured by electrode induction melting gas atomization. Subsequently, Mo layer with a thickness of 0.25 mm was formed by direct energy deposition in which the scan speed was set as a variable. According to the change of the scan speed, pores or cracks were found in the Mo deposition layer. Mo layer deposited with scan speed of 600 mm/min has the hardness value of 324 Hv with a porosity of approximately 2%. We demonstrated that Mo layers with higher relative density and hardness can be formed with less effort through direct energy deposition compared to the conventional powder metallurgy.
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Bibliography

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[8] X. Gao, L. Li, J. Liu, X. Wang, H. Yu, Int. J. Refract. Met. Hard Mater. 88, 105186 (2020).
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[15] D.R. Feenstra, A. Molotnikov, N. Birbilis, Mater. Des. 198, 109342 (2021).
[16] R. Ohser-Wiedemann, U. Martin, H. J. Seifert, A, Müller, Int. J. Refract. Met. Hard Mater. 28 (4), 550-557 (2010)
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Authors and Affiliations

Goo-Won Roh
1 2
ORCID: ORCID
Eun-Soo Park
2
ORCID: ORCID
Jaeyun Moon
3
ORCID: ORCID
Hojun Lee
4
ORCID: ORCID
Jongmin Byun
4
ORCID: ORCID

  1. University, Department of Materials Science and Engineering, Seoul 04763, Republic of Korea
  2. Research and Development Center, Eloi Materials Lab (EML) Co. Ltd., Suwon 16229, Republic of Korea
  3. University of Nevada, Department of Mechanical Engineering, Las Vegas, 4505 S. Maryland PKWY Las Vegas, NV 89154, United States
  4. Seoul National University of Science and Technology, Department of Materials Science and Engineering Seoul 01811, Republic of Korea

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