In this study, modification of the AZ91 magnesium alloy surface layer with a CO2 continuous wave operation laser has been taken on. The

extent and character of structural changes generated in the surface layer of the material was being assessed on the basis of both macro- and

microscopy investigations, and the EDX analysis. Considerable changes in the structure of the AZ91 alloy surface layer and the

morphology of phases have been found. The remelting processing was accompanied by a strong refinement of the structure and a more

uniform distribution of individual phases. The conducted investigations showed that the remelting zone dimensions are a result of the

process parameters, and that they can be controlled by an appropriate combination of basic remelting parameters, i.e. the laser power, the

distance from the sample surface, and the scanning rate. The investigations and the obtained results revealed the possibility of an effective

modification of the AZ91 magnesium alloy surface layer in the process of remelting carried out with a CO2 laser beam.

This work presents an influence of cooling rate on crystallization process, structure and mechanical properties of MCMgAl12Zn1 cast magnesium alloy. The experiments were performed using the novel Universal Metallurgical Simulator and Analyzer Platform. The apparatus enabled recording the temperature during refrigerate magnesium alloy with three different cooling rates, i.e. 0.6, 1.2 and 2.4°C/s and calculate a first derivative. Based on first derivative results, nucleation temperature, beginning of nucleation of eutectic and solidus temperature were described. It was fund that the formation temperatures of various thermal parameters, mechanical properties (hardness and ultimate compressive strength) and grain size are shifting with an increasing cooling rate.

The paper presents low-cycle fatigue (LCF) characteristics of selected magnesium alloys used, among others, in the automotive and aviation industries. The material for the research were bars of magnesium alloys AZ31 and WE43 after hot plastic working. Due to their application(s), these alloys should have good/suitable fatigue properties, first of all fatigue durability in a small number of cycles.

Low-cycle fatigue tests were carried out on the MTS-810 machine at room temperature. Low-cycle fatigue trials were conducted for three total strain ranges Δεt of 0.8%, 1.0% and 1.2% with the cycle asymmetry factor R = –1. Based on the results obtained, fatigue life characteristics of materials, cyclic deformation characteristics σa = f(N) and cyclic deformation characteristics of the tested alloys were developed. The tests have shown different behaviors of the tested alloys in the range of low number of cycles. The AZ31 magnesium alloy was characterized by greater fatigue life Nf compared to the WE43 alloy.

The results of some mechanical properties of four Mg-5Al-xRE-0.4Mn (x = 1 – 5) alloys are presented. The microstructure of

experimental alloys consisted of an α-Mg phase and an α+γ semi-divorced eutectic, Al11RE3 phase and an Al10RE2Mn7 intermetallic

compound. For gravity casting in metal mould alloys, Brinell hardness, impact strength, tensile and compression properties at ambient

temperature were determined. The performed mechanical tests allowed the author to determine the proportional influence of the mass

fraction of rare earth elements in the alloys on their tensile strength, yield strength, compression strength and Brinell hardness. The

impact strength of the alloys slightly decreases with a rise in the rare earth elements mass fraction.

Magnesium alloy with 5 wt% Al, 0.35 wt% Mn and 5 wt% rare earth elements (RE) was prepared and gravity cast into a sand mould.

Microstructure investigations were conducted. Analyses of the Mg-Al-RE alloy microstructure were carried out by light microscopy,

scanning electron microscopy and the XRD technique. In the as-cast condition, the alloy was composed of α-Mg, Al11RE3 and

Al10RE2Mn7 intermetallic phases. Additionally, due to non-equilibrium solidification conditions, an Al2RE intermetallic phase was

revealed.

Investigation of the tensile and fatigue properties of cast magnesium alloys, created by the heated mold continuous casting process (HMC),

was conducted. The mechanical properties of the Mg-HMC alloys were overall higher than those for the Mg alloys, made by the

conventional gravity casting process (GC), and especially excellent mechanical properties were obtained for the Mg97Y2Zn1

-HMC alloy.

This was because of the fine-grained structure composed of the -Mg phases with the interdendritic LPSO phase. Such mechanical

properties were similar levels to those for conventional cast aluminum alloy (Al84.7Si10.5Cu2.5Fe1.3Zn1 alloys: ADC12), made by the GC

process. Moreover, the tensile properties (UTS and f

) and fatigue properties of the Mg97Y2Zn1

-HMC alloy were about 1.5 times higher

than that for the commercial Mg90Al9Zn1

-GC alloy (AZ91). The high correlation rate between tensile properties and fatigue strength

(endurance limit: l

) was obtained. With newly proposed etching technique, the residual stress in the Mg97Y2Zn1 alloy could be revealed,

and it appeared that the high internal stress was severely accumulated in and around the long-period stacking-order phases (LPSO). This

was made during the solidification process due to the different shrinkage rate between α-Mg and LPSO. In this etching technique, microcracks

were observed on the sample surface, and amount of micro-cracks (density) could be a parameter to determine the severity of the

internal stress, i.e., a large amount to micro-cracks is caused by the high internal stress.

The paper presents the susceptibility of AE44 magnesium alloy to electrochemical corrosion and stress corrosion cracking (SCC). The evaluation of the intensity of the interaction of the corrosive environment was carried out using the corrosion tests and the Slow Strain Rate Test (SSRT). Corrosion tests performed in 0.1 M Na2SO4 solution (immersion in solution and under cathodic polarization conditions) revealed that the layer of corrosion products was much thicker after immersion test. The results of SSRT showed that the AE44 alloy deformed in the solution was characterized by higher plasticity compared to the alloy deformed in the air after immersion in solution. Moreover, the fractures were characterized by different morphology. In the case of an alloy deformed in the solution under cathodic polarization many microcracks on the fracture were observed, which were not observed in the case of the alloy deformed in the air.

The thermochemical treatment applied to improve the surface properties of AZ91 consisted in heating the material in contact with AlSi10Mg powder at 445 oC for 30 min. During heat treatment process the powder was held under pressure to facilitate the diffusion of the alloying elements to the substrate and, accordingly, the formation of a modified layer. Two pressures, 1 MPa and 5 MPa, were tested. The resultant layers, containing hard Mg2Si and Mg17Al12 phases, were examined using an optical microscope and a scanning electron microscope equipped with an energy-dispersive X-ray spectrometer (EDS). The experimental data show that the layer microstructure was dependent on the pressure applied. A thicker, three-zone layer (about 200 μm) was obtained at 1 MPa. At the top, there were Mg2Si phase particles distributed over the Mg17Al12 intermetallic phase matrix. The next zone was a eutectic (Mg17Al12 and a solid solution of Al in Mg) with Mg2Si phase particles embedded in it. Finally, the area closest to the AZ91 substrate was a eutectic not including the Mg2Si phase particles. By contrast, the layer produced at a pressure of 5 MPa had lower thickness of approx. 150 μm and a two-zone structure. Mg2Si phase particles were present in both zones. In the upper zone, Mg2Si phase particles were regularly distributed over the Mg17Al12 intermetallic phase matrix. The lower zone, adjacent to the AZ91, was characterized by a higher volume fraction of Mg2Si phase particles distributed over the matrix composed mainly of Mg17Al12. The alloyed layers enriched with Al and Si had much higher hardness than the AZ91 substrate.

In this paper is discussed the effect of the inoculant mischmetal addition on the microstructure of the magnesium alloy AZ91. The concentration of the inoculant was increased in the samples within the range from 0.1% up to 0.6%. The thermal process was performed with the use of Derivative and Thermal Analysis (DTA). A particular attention was paid to finding the optimal amount of the inoculant, which causes fragmentation of the microstructure. The concentration of each element was verified with use of a spark spectrometer. In addition, the microstructures of every samples were examined with the use of an optical microscope and also was performed an image analysis with a statistical analysis using the NIS–Elements program. The point of those analyses was to examine the differences in the grain diameters of phase αMg and eutectic αMg+γ(Mg17Al12) in the prepared samples as well as the average size of each type of grain by way of measuring their perimeters. This paper is the second part of the introduction into a bigger research on grain refinement of magnesium alloys, especially AZ91. Another purpose of this research is to achieve better microstructure fragmentation of magnesium alloys without the relevant changes of the chemical composition, which should improve the mechanical properties.

Ultrasonic assisted active-passive filling friction stir repairing (A-PFFSR) was proposed to repair volume defects in the metallic parts. Sound joints without interfacial defects could be achieved. Firstly, the ultrasonic was beneficial to improving material flow and atom diffusion, and then eliminated kissing bond defects compared to conventional A-PFFSR joints. Secondly, the equiaxed grains were refined by ultrasonic vibration. Lastly, the repairing passes were reduced due to the ultrasonic, which decreased softening degree of the repaired joints. The maximum tensile strength of 150 MPa was achieved. Therefore, this strategy to repair the volume defects is feasibility and potential in the remanufacturing fields of aerospace and transportation.

The paper presents the results of tests concerning the effect of the extrusion process in the complex strain state on the microstructure and properties of one of magnesium alloy with aluminium, zinc and manganese, designated AZ61. Due to its specific gravity, it is increasingly being used in the automotive and aerospace industries to reduce the weight of structural elements. As a result of plastic deformation processes, rods with a diameter of 8, 6 and 4 mm were obtained from AZ61 magnesium alloy. The microstructure analysis was performed using light and electron microscopy (STEM) techniques in the initial state and after plastic deformation. Microstructure studies were supplemented with a quantitative analysis using the Metilo program. A number of stereological parameters were determined: average diameter of grain, shape factor. A static tensile test was carried out at 250ºC and 300ºC, at deformation rates of 0.01, 0.001 and 0.0001 m·s–1. Better plastic properties after deformation using KoBo method were obtained than with conventional extrusion.

Mg-0.5Si-xSn (x=0.95, 2.9, 5.02wt.%) alloys were cast and extruded at 593K (320 o C) with an extrusion ratio of 25. The microstructure and mechanical properties of as-cast and extruded test alloys were investigated by OM, SEM, XRD and tensile tests. The experimental results indicate that the microstructure of the Mg-0.5Si-xSn alloys consists of primary α-Mg dendrites and an interdendritic eutectic containing α-Mg, Mg2Si and Mg2Sn. There is no coarse primary Mg2Si phase in the test alloys due to low Si content. With the increase in the Sn content, the Mg2Si phase was refined. The shape of Mg2Si phase was changed from branch to short bar, and the size of them were reduced. The ultimate tensile strength and yield strength of Mg-0.52Si-2.9Sn alloy at the temperature of 473K (200 o C) reach 133MPa and 112MPa respectively. Refined eutectic Mg2Si phase and dispersed Mg2Sn phase with good elevated temperature stability are beneficial to improve the elevated temperature performance of the alloys. However, with the excess addition of Sn, large block-like Mg2Sn appears around the grain boundary leading to lower mechanical properties.