In the presented work, two multicomponent Cr ₂₅Z ₂₅Co ₂₀Mo ₁₅Si ₁₀Y ₅ and Cr ₂₅Co ₂₅Zr ₂₀Mo ₁₅Si ₁₀Y ₅ alloys were produced from bulk chemical elements using the vacuum arc melting technique. X-ray diffraction phase analysis was used to determine the phase composition of the obtained materials. Microstructure analysis included scanning electron microscopy and energy dispersive X-ray spectroscopy techniques. The studies revealed the presence of multi-phase structures in both alloys. Elemental distribution maps confirmed the presence of all six alloying elements in the microstructure. The segregation of chemical elements was also observed. Microhardness measurement revealed that both alloys exhibited microhardness from 832(27) to 933(22) HV1.