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Abstract

Applying new technologies basing on coal utilization demands precise identification of coal-bed composition. It is suggested, that such possibility is enabled by coal-bed logging with use of - adjusted to this aim - microlithotype analysis. Modification of this research method relies on ten-fold augmentation of 20 point grid size dimensions - up to 500 x 500 [...]. Maceral associations - as identified duringmicroscope observations - are placed in computer database according to their localization in logging. This allows for later graphic interpretation - microlithotype profile drawing. 13 associations has been educed in description, in majority being consistent with commonly used microlithotypes. However, a few changes has been introduced: in description of vitrite, telovitrite, macroscopically recognized in logging as vitrine layers, has been distinguished, as well as detro-gelo-vitrite, macroscopically recognized in logging as durain, while within bimaceralic microlithotypes there has been distinguished: vitrinertite (W), vitrinertite (I), clarite (W), clarite (I), durite (L), durite (I), all on the basis of dominant ingredient named in parenthesis. Accepted research methodology enables precise characteristics of petrographic variation within coal-bed logging. This allows especially to describe variation within dull coal (durain). Basing on research results, it is suggested that the biggest share in seam composition belongs to duroclarite - 23.8%, then vitrite - 18.7% and clarodurite - 17.6%, lower share of few percent belongs to: vitrinertite (I), vitrinertite (W), inertite, clarite (W), vitrinertoliptite, durite (I), durite (L), while both liptite and clarite (L) are less than one percent . Sequence of following microlithotypes also illustrate facies variation, what allows interpretation of environments of peat deposition in paleo-peat bog 116/2. Dominating percentage in log belongs to Forest Moor facies - 33.5%, while the lowest is Forest Terrestial Moor - 12.5%.

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Authors and Affiliations

Jacek Misiak
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Abstract

Alkali-aggregate reactivity (AAR) is one of the major causes of damage in concrete. Potential susceptibility of aggregates to this reaction can be determined using several methods. This study compares gravel alkali reactivity results obtained from different tests conducted on coarse aggregates with complex petrography. The potential for the reactivity in the aggregates was revealed in the chemical test using treatment with sodium hydroxide. Optical microscopy, scanning electron microscopy and X-ray diffraction were used to identify the reactive constituents. The expansion measured in the mortar bars test confirmed that the aggregate was potentially capable of alkali silica reactivity with consequent deleterious effect on concrete.

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Authors and Affiliations

Z. Owsiak
P. Czapik
J. Zapała-Sławeta
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Abstract

Proper values of physical and mechanical properties and their homogeneity are one of major requirements deciding about technological suitability of the rocks quarried to manufacturing aggregates. These properties depend on the natural features of a rock, its mineral composition, texture and structure. The characteristic of aggregates and the technical requirements they must meet are normalized in adequate standards that describe the procedures of conducting particular determinations and the methods of interpreting their results. In the basaltoids (usually called basalts) of selected deposits of Lower Silesia that represent different intrusive forms, five textural varieties have been distinguished: aphanitic, aphanitic-porphyritic, porphyritic-aphanitic, porphyritic-nodular and nodular-porphyritic. The petrography and essential physical and mechanical properties of these varieties have been described in Tables 1 and 2, respectively. The highest technical parameters have the aphanitic and aphanitic-porphyritic rock varieties. They result mainly from the textures of these rocks and their insignificant weathering, and to a lesser degree from their mineral composition. The resistance to wear (micro-Deval) and the resistance to fragmentation (Los Angeles) of the aggregates that represent the grain fraction 10-14 mm of the five varieties of basaltoids and the rock composites were determined according to the standards PN-EN 12620: 2008 and PN-EN 13043: 2004. Of the aggregates produced from the five major varieties, only those made of the nodular-porphyritic basaltoids have the properties of lower categories, whereas the remaining four are the materials of very high quality. Additionally, it has been shown that by combining various basaltoid types it is possible to produce composite aggregates with the variable qualities belonging to the categories LA and MDE (Tab. 3). The effect of rock petrography on the differentiation of the parameters of aggregates depending on the grain fraction of the products (Fig. 1, Tab. 4) is the lowest in the case of the aggregates produced from the homogenous and not weathered rock. In contrast, the range of variability of the parameters is higher if the starting material to produce aggregates is composed of several textural varieties and shows signs of weathering as well. The possibility of delineation of the areas occupied in the deposit by basaltoids with specific textural varieties creates the conditions of determining the rock zones, from which the aggregates of the predicted quality may be produced. This quality may be controlled and partly changed to the user needs by producing aggregates from the specially prepared rock mixtures (i.e. the charge to crushers) with specified proportions of the basaltoid varieties.

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Authors and Affiliations

Marek Rembiś
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Abstract

The research was aimed at examining the impact of the petrographic composition of coal from the Janina mine on the gasification process and petrographic composition of the resulting char. The coal was subjected to fluidized bed gasification at a temperature below 1000°C in oxygen and CO2 atmosphere. The rank of coal is borderline subbituminous to bituminous coal. The petrographic composition is as follows: macerals from the vitrinite (61.0% vol.); liptinite (4.8% vol.) and inertinite groups (29.0% vol.). The petrofactor in coal from the Janina deposit is 6.9. The high content of macerals of the inertinite group, which can be considered inert during the gasification, naturally affects the process. The content of non-reactive macerals is around 27% vol. The petrographic analysis of char was carried out based on the classification of International Committee for Coal and Organic Petrology.

Both inertoid (34.7% vol.) and crassinetwork (25.1% vol.) have a dominant share in chars resulting from the above-mentioned process. In addition, the examined char contained 3.1% vol. of mineroids and 4.3% vol. of fusinoids and solids. The calculated aromaticity factor increases from 0.75 in coal to 0.98 in char. The carbon conversion is 30.3%. Approximately 40% vol. of the low porosity components in the residues after the gasification process indicate a low degree of carbon conversion. The ash content in coal amounted to 13.8% and increased to 24.10% in char. Based on the petrographic composition of the starting coal and the degree of conversion of macerals in the char, it can be stated that the coal from the Janina deposit is moderately suitable for the gasification process.

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Authors and Affiliations

Barbara Bielowicz
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Abstract

The paper presents the results of a study of methane adsorption on coal samples with various degrees of metamorphism, coming from the Polish and Czech parts of the Upper Silesian Coal Basin (USCB). The range of coalification of the samples was from bituminous with vitrinite reflectance Ro equal to about 0.5% to para-anthracite coals with Ro equal to over 2%. The methane adsorption capacity was determined at the temperature 303 K for each of the studied coal seams. Methane adsorption isotherms were approximated using the Langmuir model. The relationship between the Langmuir isotherm parameters (am and PL) and the degree of coalification was presented. It was shown that the degree of coalification of the coal substance affects the adsorption ability of coal with respect to methane and determines the value of the Langmuir isotherm parameters. The study was conducted in order to present the distribution of adsorption capacity of Upper Silesian coals in relation to improving work safety in active mines as well as designing technologies that use coal bed methane (CBM) from balance and off-balance resources.
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Authors and Affiliations

Barbara Dutka
1
ORCID: ORCID
Katarzyna Godyń
1
ORCID: ORCID

  1. Strata Mechanics Research Institute of the Polish Academy of Sciences, 27 Reymonta Str.,30-059 Krakow, Poland
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Abstract

The article presents the analysis of the correlation between the self-ignition parameters and the ultimate and proximate analysis, as well as the petrographic properties of Polish lignite, sub-bituminous coal, bituminous coal and anthracite. The following coal properties were determined: the moisture, ash content, volatile matter and sulfur content, gross calorific value, net calorific value, C, O, N and H contents, total porosity, ash oxide composition, rates of spontaneous combustion in 237°C and 190°C, and activation energy. During the petrographic analysis, maceral composition and random reflectance were determined. To determine the linear correlation between the self-ignition parameters and the analyzed coal properties, the Pearson correlation coefficient was calculated. The results show that there is no strong linear correlation between the lignite tendency to self-ignition and its petrographic properties. However, a strong negative correlation between the rate of spontaneous combustion and moisture and volatile matter content was observed. In the case of bituminous coal, strong correlations between self-combustion parameters and various coal properties were confirmed. The most noteworthy are the correlations between self-ignition parameters and the maceral composition, that is, between the content of macerals of the inertinite group in coal and content of macerals of the huminite/vitrinite group. The obtained results suggest that the spontaneous combustion tendency of coal increases with the increasing content of semifusinite and liptinite.

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Authors and Affiliations

Barbara Bielowicz
ORCID: ORCID
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Abstract

The organic carbon (OC)-rich, black shale succession of the Middle Triassic Bravaisberget Formation in Spitsbergen contains scattered dolomite-ankerite cement in coarser-grained beds and intervals. This cement shows growth-related compositional trend from non-ferroan dolomite (0–5 mol % FeCO3) through ferroan dolomite (5–10 mol % FeCO3) to ankerite (10–20 mol % FeCO3, up to 1.7 mol % MnCO3) that is manifested by zoned nature of composite carbonate crystals. The d13C (-7.3‰ to -1.8‰ VPDB) and d18O (-9.4‰ to -6.0‰ VPDB) values are typical for burial cements originated from mixed inorganic and organic carbonate sources. The dolomite-ankerite cement formed over a range of diagenetic and burial environments, from early post-sulphidic to early catagenic. It reflects evolution of intraformational, compaction-derived marine fluids that was affected by dissolution of biogenic carbonate, clay mineral and iron oxide transformations, and thermal decomposition of organic carbon (decarboxylation of organic acids, kerogen breakdown). These processes operated during Late Triassic and post-Triassic burial history over a temperature range from approx. 40°C to more than 100°C, and contributed to the final stage of cementation of the primary pore space of siltstone and sandstone beds and intervals in the OC-rich succession.

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Authors and Affiliations

Krzysztof P. Krajewski
Ewa Woźny
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Abstract

The aim of the paper is the petrographic characterization of coal from the Wieczorek mine and the residues after its gasification. The coal was subjected to gasification in a fluidized bed reactor at a temperature of about 900°C and in an atmosphere of oxygen and CO2. The petrographic, proximate, and ultimate analysis of coal and char was performed. The petrographic composition of bituminous coal is dominated by macerals of the vitrinite group (55% by volume); macerals of inertinite and liptinite groups account for 23% and 16.0%, respectively. In the examined char, the dominant component is inertoid (41% vol.). Mixed dense and mixed porous account for 10.9% and 13.5% vol., respectively. In addition, the examined char also contained unreacted particles such as fusinoids, solids (11.3% vol.), and mineroids (5.1% vol.). The char contains around 65% vol. of low porosity components, which indicates a low degree of carbon conversion and is associated with a low gasification temperature. The char was burned and the resulting bottom and fly ashes were subjected to petrographic analysis. Their composition was compared with the composition of ashes from the combustion of bituminous coal from the Wieczorek mine. Bottom ashes resulting from the combustion of bituminous coal and char did not differ significantly in the petrographic composition. The dominant component was mineroid, which accounted for over 80% vol. When it comes to fly ash, a larger amount of particles with high porosity is observed in fly ash from bituminous coal combustion.

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Authors and Affiliations

Natalia Maciejończyk
Barbara Bielowicz
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Abstract

Palaeomagnetic−petrographic−structural analyses of Proterozoic–Lower Palaeozoic metamorphosed carbonates from 12 locations within Oscar II Land (Western Spitsbergen) have been carried out to determine their usefulness in palaeogeographic reconstructions for Caledonian time. Structural analyses confirm that metacarbonates record several stages of deformation: D1, D2 ductile phases related to Caledonian metamorphism and a D3 brittle phase related to Late Cretaceous–Paleogene evolution of the West Spitsbergen Fold Belt. The latter is represented by thrust faults, localized folds with strain slip cleavages and late extensional collapse. Petrographic investigations reveal that Caledonian greenschist facies metamorphism was characterized by the high activity of H 2 O−CO 2 −rich fluids which promoted extensive recrystallization and within−rock spatial reorganization of sampled meta carbonates. Microscopic, SEM and microprobe analyses exclude the existence of any primary pre−metamorphic ferromagnetic minerals (primary−related to sedimentation and or early diagenesis) and point to metamorphic 4C superstructure (Fe 7 S 8 ) pyrrhotite as the main ferromagnetic carrier in investigated rocks. This is confirmed by the three−component isothermal remanent magnetization (IRM) procedures and the results of thermal demagnetizations. In 12 sites a total number of 72 independently oriented palaeomagnetic samples were collected from which 181 specimens were drilled and thermally demagnetized. Sampled metacarbonates are weakly magnetized (NRM <0.2mA/m). The statistically significant palaeomagnetic results were achieved only from 1 of 12 investigated sites. In one site situated in the Western overturned limb of the Holmesletfjellet Syncline intermediate unblocking temperatures – “pyrrhotite related” component WTSJ5M superimposed on the S1 Caledonian schistosity was recognized (D = 100.7 ° , I = −21.4 °a 95% = 5.5 ° , k = 58.23). Coincidence of WTSJ5M with Silurian–Devonian sector of the Baltica reference path after unfolding of the syncline by the angle of 130 ° suggests synfolding origin of this direction. Further, this suggests that Holmesletfjellet Syncline originated as an open fold and has been transformed into an overturned syncline during the Late Caledonian shortening or in the Late Cretaceous–Palaeogene time.
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Authors and Affiliations

Krzysztof Michalski
Justyna Domańska-Siuda
Krzysztof Nejbert
Geoffrey Manby
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Abstract

The aim of this study was to establish the stratigraphic extent of a putative Tournaisian Stage within the Carboniferous succession in the Lublin Basin. The oldest part of the succession, known as the Huczwa Formation and comprising depositional sequences 1–4, was investigated based on lithofacies analysis, sequence stratigraphy and petrographic studies. The article provides descriptions of depositional sequences, parasequences (cyclothems) and lithofacies that were formed in a range of environments (elements of depositional architecture) and as a result of volcanic processes – lava and pyroclastic eruptions and chemical weathering of their products. Correlation of the sequence stratigraphy to the West European and global Carboniferous chronostratigraphic divisions, as well as to the Khoriv suite in the Lviv-Volyn Basin in adjacent Ukraine, indicates a putative late Tournaisian age for sequence 1, and a late Visean age for sequences 2–4. There is a stratigraphic gap between sequences 1 and 2, spanning probably the uppermost Tournaisian and the lower and middle Visean. The upper Tournaisian is represented by the FRST-LST deposits of sequence 1, comprising mainly volcaniclastic conglomerates and sandstones developed in braided-river channels and incised valleys with hyperconcentrated flow processes. These deposits are represented by polymictic paraconglomerate and lithic/sublithic/subarkose arenites or sublithic wackes, and contain predominantly grains of acidic and alkaline volcanic and igneous rocks. This material probably came from the Łuków-Wisznice Elevation and the Volynian Polesia region, located to the NE and E of the Lublin Basin. In the uppermost part of sequence 1, volcanic rocks and tuffs appear which developed during the activity of at least three volcanic cones in the Lublin Basin. The volcanoes were the source of alkaline lavas in the central and SW areas of the basin, and of acidic lavas in the SE area, previously undescribed. The Visean sequences 2–4 consist of the FRST-LST sediments deposited within incised valleys. The TST and HST deposits accumulated mainly in a shallow ramp-type carbonate shelf, shallow clayey shelf and deltaic environments.
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Authors and Affiliations

Maria I. Waksmundzka
1
Aleksandra Kozłowska
1
Magdalena Pańczyk
1

  1. Polish Geological Institute – National Research Institute, Rakowiecka 4, PL-00-975 Warsaw, Poland
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Abstract

Fennoscandinavian erratics found in the glacial deposits till and in the glaciofluvial sediments within the main limit of the Odra glacier lobe (NW Poland and NE Germany), have been examined in two fractions: of 4-10 mm and 2060 mm. The most numerous in the fraction of 4-10 mm are: crystalline rocks (Cr; 35-40%) originating in the Protero zoic Baltic Shield as well as Lower Palaeozoic limestones (LPL; 35-40%) - from the sedimentary sheet covering the Proterozoic Baltic Shield in the area of central Baltic Sea. Percentage of sandstones (S) amounts to 10-15%. The re maining rock types (several percent each) are: Palaeozoic shales (PS), the outcrops of which are localized in Scania (Skane) and on Bornholm, Cretaceous limestones (CL) and flintstones (F) originating from the western part of the southern Baltic Sea as well as quartz (Q), milk quartz (MQ) and isolated grains of Devonian dolomites (DD). From the analysis of indicator erratics, which was carried out in the 20-60 mm fraction, it appears that mainly the outcrops localized in Smaland (e.g. red and grey Viixjo granites, Paskallavik porphyries or Tessini and Kalmarsund sandstones) as well as in Scania (Hoor and Hardeberga sandstones) and Region Blekinge-Bornholm (e.g. Karlshamn and Halen granites as well as Nexo and Bavnodde sandstones) had been subjected to the glacial plucking. Theoretical boulder centres (TBC, German: TGZ das Theoretische Geschiebezentrum, Uittig 1958), which were calculated for 23 samples, are localized mostly in a small area in Smiiland, between 15°E-16°E and 56.5°N-58.5°N. Apart from indicator erratics the statistical ones are numerous, that are first of all grey and red Lower Palaeozoic limestones with their outcrops localized at the bottom of the central Baltic Sea. Taking into account the TBC values of indicator erratics as well as high percentage of statistical erratics it can be pronounced that the section of central and western Baltic Sea as well as the one of south-eastern Sweden had been subjected to the heaviest glacial plucking by that part of the Pleistocene ice-sheet which reached the studied area during the Pomeranian Phase.

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Authors and Affiliations

Maria Górska-Zabielska
Ryszard Zabielski

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