This study is the first comparison of the morphology of pollen grains in ten cultivars of three species of the Taxus,

Torreya nucifera and Cephalotaxus harringtonia var. drupacea genera. The material came from the Botanical

Garden of Adam Mickiewicz University in Poznań, Poland. Each measurement sample consisted of 50 pollen

grains. In total, 750 pollen grains were analyzed. Light and electron scanning microscopy was used for the morphometric

observation and analysis of pollen grains. The pollen grains were inaperturate and classified as small

and medium-sized. They were prolate-spheroidal, subprolate to prolate in shape. The surface of the exine was

microverrucate-orbiculate, perforate in Cephalotaxus harringtonia var. drupacea, granulate-orbiculate, perforate

in all Taxus taxa and granulate-microverrucate-orbiculate, perforate in Torreya. The orbicules were rounded to

oval in surface view, and the size was considerably diversified. The pollen features were insufficient to distinguish

between individual Taxus members – only groups were identified. The values of the coefficient of variability of

three features (LA, SA and LA/SA) were significantly lower than the orbicule diameter. The pollen surface of all

Taxus specimens was similar, so it was not a good identification criterion. The pollen grains of the Taxus taxa

were smaller and had more orbicules than Cephalotaxus and Torreya. Palynological studies provided taxonomic

support for recognition of two different genera of the Cephalotaxaceae and Taxaceae families, which are closely

related.

Silver coatings have a very high reflection ability. To avoid their darkening from the hydrogen sulphide in the air, a thin layer of heat-resistant colorless lacquer is applied to the coatings. Silver plating is mainly used in jewelery, optics, electronics and electrical engineering. Depending on their application the thickness of the layer may vary from 2 to 24 μm. It can be done in several ways: chemical, electrochemical, contact, etc. The most common way of silver plating is the electrochemical deposition using cyanide and non-cyanide electrolytes. The cyanide electrolytes produce light, fine crystalline, dense and plastic coatings upon silver-plating. Usually silver coatings are applied with copper or nickel intermediate layer. In order to improve the de-oxidation of the aluminum surface new chemical treatment in acid – alkaline solution was applied. Our previous research shows that the presence of diamond nanoparticles in the electrolyte increase the metal deposition. Samples were prepared from electrolyte containing 10 g/l diamond nanoparticles. Their properties were compared to the properties of reference samples. The diamonds were obtained by detonation synthesis. The aim of this study is to obtain electrochemically deposited silver layer with high density, adhesion and electric conductivity on aluminum alloys substrate. The coatingwas directly plated without intermediate layer. Non-cyanide electrolyte composition and electrochemical parameters were determined in order to produce Ag coatings on Al alloy substrate without intermediate layer. The coating is with good adhesion, density and thickness of 14-23 μm.

La0,7Ca0,3MnO3 polycrystalline were synthesized from La2O3, CaO and MnO2 powder mixture using a solid state reaction technique. The compound powders were obtained through the free sintering method at different temperatures and sintering times in order to study the influence of technological conditions on Ca doped La manganites. The most important physical features as structure, microstructure and morphology were described after X-ray diffraction investigation. Photographs of the specimen fractures were taken with SEM (scanning electron microscope) and they revealed high porosity of the tested material and great tendency for its grains to create agglomerates. Influence of doping and technological conditions on lattice parameters were studied by means of Rietvield analysis. The XRD measurements reveal that La0,7Ca0,3MnO3 has orthorhombic symmetry with Pnma space group.

The results of structure observations of Ni base superalloy subjected to long-term influence of high pressure hydrogen atmosphere at 750K

and 850K are presented. The structure investigation were carried out using conventional light-, scanning- (SEM) and transmission electron

microscopy (TEM). The results presented here are supplementary to the mechanical studies given in part I of this investigations. The

results of study concerning mechanical properties degradation and structure observations show that the differences in mechanical

properties of alloy subjected different temperature are caused by more advanced processes of structure degradation during long-term aging

at 850K, compare to that at 750K. Higher service temperature leads to formation of large precipitates of δ phase. The nucleation and

growth of needle- and/or plate-like, relative large delta precipitates proceed probably at expense strengthening γ" phases. Moreover, it can't

be excluded that the least stable γ" phase is replaced with more stable γ' precipitates. TEM observations have disclosed differences in

dislocation structure of alloy aged at 750K and 850K. The dislocation observed in alloy subjected to 750K are were seldom observed only,

while in that serviced at high stress and 850K dislocation array and dislocation cell structure was typical.

Background: a humidity sensor is used to sense and measure the relative humidity of air. A new composite system has been fabricated using environmental pollutants such as carbon black and low-cost zinc oxide, and it acts as a humidity sensor. Residual life of the sensor is calculated and an expert system is modelled. For properties and nature confirmation, characterization is performed, and a sensing material is fabricated. Methodology: characterization is performed on the fabricated material. Complex impedance spectroscopy (CIS), Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD) and scanning electron microscopy (SEM) are all used to confirm the surface roughness, its composite nature as well as the morphology of the composite. The residual lifetime of the fabricated humidity sensor is calculated by means of accelerated life testing. An intelligent model is designed using artificial intelligence techniques, including the artificial neural network (ANN), fuzzy inference system (FIS) and adaptive neuro-fuzzy inference system (ANFIS). Results: maximum conductivity obtained is 6.4×10⁻³ S/cm when zinc oxide is doped with 80% of carbon black. Conclusion: the solid composite obtained possesses good humidity-sensing capability in the range of 30–95%. ANFIS exhibits the maximum prediction accuracy, with an error rate of just 1.1%.

The paper presents the results and provides an analyse of the geometric structure of Fe-Al protective coatings, gas-treated under specified GDS conditions. The analysis of the surface topography was conducted on the basis of the results obtained from the SEM data. Topographic images were converted to three-dimensional maps, scaling the registered amplitude coordinates of specific gray levels to the relative range of 0÷1. This allowed us to assess the degree of surface development by determining the fractal dimension. At the same time, the generated three-dimensional spectra of the autocorrelation function enabled the researchers to determine the autocorrelation length (Sal) and the degree of anisotropy (Str) of the surfaces, in accordance with ISO 25178. Furthermore, the reconstructed three-dimensional images of the topography allowed us to evaluate the functional properties o the studied surfaces based on the Abbott-Firestone curve (A-F), also known as the bearing area curve. The ordinate describing the height of the profile was replaced by the percentage of surface amplitude in this method, so in effect the shares of the height of the three-dimensional topographic map profiles of various load-bearing properties were determined. In this way, both the relative height of peaks, core and recesses as well as their percentages were subsequently established.

In the work five ceramic compounds based on the (K0.44Na0.52Li0.04)NbO3 (KNLN) material modified with oxides: Cr2O3, ZnO, Sb2O3 or Fe2O3 (in an amount of 0.5 mol.%) were obtained. The KNLN-type composition powder was prepared by solid phase synthesis from a mixture of simple oxides and carbonates, while compacted of the ceramic samples was conducted by free sintering methods. In the work the effect of the used admixture on the electrophysical properties of the KNLN ceramics was presented. The XRD, EDS tests, the SEM measurements of the morphology ceramic samples, dielectric properties and DC electric conductivity were conducted. The research showed that the used admixtures introduced into the base of KNLN-type composition improve the microstructure of the ceramic samples and improve their sinterability. In the case of the dielectric measurements, it was observed a decrease in the maximum dielectric permittivity at the TC for dopred KNLN-type samples. The addition of an admixture of chromium, zinc, antimony or iron in an amount of 0.5 mol.% to the base composition (K0.44Na0.52Li0.04)NbO3 practically does not change the phase transition temperature. The diminution in the density value of doped KNLN ceramics was attributed to the alkali elements volatilization.

ZnO thin layers were deposited on p-type silicon substrates by the sol-gel spin-coating method and, then, annealed at various temperatures in the range of 573–873 K. Photoluminescence was carried out in the temperature range of 20–300 K. All samples showed two dominant peaks that have UV emissions from 300 nm to 400 nm and visible emissions from 400 nm to 800 nm. Influence of temperature on morphology and chemical composition of fabricated thin layers was examined by XRD, SEM, FTIR, and Raman spectroscopy. These measurements indicate that ZnO structure is obtained for samples annealed at temperatures above 573 K. It means that below this temperature, the obtained thin films are not pure zinc oxide. Thus, annealing temperature significantly affected crystallinity of the thin films.

In this paper, study the preparation of Y-Fe alloy by reduction-diffusion process, which is novel technique for producing an alloy from its ores directly at different temperatures. From this work, investigates the particles size and morphology structure of alloy by X-Ray Diffraction (XRD), Energy dispersive-X-ray analyzer (EDAX) and Scanning Electron Microscope (SEM) respectively. Here study the thermodynamics of property of system such as Gibbs free energy and reaction kinetics of system respectively. The Vibrating Sample magnetometer (VSM) is used to study the magnetic properties of alloy such as cocerviety, saturation magnetization and retentivity.