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Abstract

The addition of hard ceramic particles of nc-(Ti,Mo)C in carbon network into Ti matrix has been proved to be an efficient way to enhance their properties. The purpose of this work was to analyze the corrosion, tribological, mechanical and morphological effects of combining nc-(Ti,Mo)C/C with titanium metal, to create a unique composite via selective laser melting technique (SLM). Composites with different weight percentage (5, 10 and 20 wt %) of ceramic phase were produced. The samples of pure Ti and Ti-6Al-4V alloy were also tested, as a reference. These composites were examined for corrosion resistance in body fluid (artificial saliva solution). Moreover, the properties of titanium composites reinforced with nc-TiC powders were compared. It was stated that mechanical properties were significantly improved with increasing amount of nc-(Ti,Mo)C/C in Ti matrix. In terms of corrosion resistance, the composites showed worse properties compared to pure titanium and Ti-6Al-4V alloy, but better than TiC-reinforced composites.

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Authors and Affiliations

P. Figiel
A. Biedunkiewicz
W. Biedunkiewicz
D. Grzesiak
M. Pawlyta
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Abstract

The article presents the technology of layered casting with the use of 3D printing to make a frame insert. The insert was made of powdered titanium and then filled with liquid cast iron. The paper presents the results of research, including structure observation and hardness measurements, as well as abrasion resistance tests. The results indicate the possibility of creating a local reinforcement using a frame insert. The resulting casting is characterized by a local increase in hardness and, in addition, an increase in abrasion resistance of the entire surface layer. The quality of the obtained connection depends strongly on the casting parameters.

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Authors and Affiliations

A. Dulska
ORCID: ORCID
J. Szajnar
ORCID: ORCID
M. Król
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Abstract

The article presents the results of a comparative analysis of the metal substructure for dental prosthesis made from a Co-Cr-Mo-W alloy by

two techniques, i.e. precision investment casting and selective laser melting (SLM). It was found that the roughness of the raw surface of

the SLM sinter is higher than the roughness of the cast surface, which is compensated by the process of blast cleaning during metal

preparation for the application of a layer of porcelain. Castings have a dendritic structure, while SLM sinters are characterized by a

compact, fine-grain microstructure of the hardness higher by about 100 HV units. High performance and high costs of implementation the

SLM technology are the cause to use it for the purpose of many dental manufacturers under outsourcing rules. The result is a reduction in

manufacturing costs of the product associated with dental work time necessary to scan, designing and treatment of sinter compared with

the time needed to develop a substructure in wax, absorption in the refractory mass, casting, sand blasting and finishing. As a result of

market competition and low cost of materials, sinter costs decrease which brings the total costs related to the construction unit making

using the traditional method of casting, at far less commitment of time and greater predictability and consistent sinter quality.

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Authors and Affiliations

D. Myszka
M. Skrodzki
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Abstract

Selective Laser Melting (SLM) is a modern manufacturing method with many applications in medicine, aerospace and automotive industries. SLM processed materials are characterized by good dimensional accuracy and properties comparable or superior to materials obtained by traditional processing methods. In this paper an SLM process was used to obtain 316L stainless steel parts. This paper presents the microstructure, chemical and phase composition, physicochemical and electrochemical properties of 12 groups of tested samples, differentiated by the SLM processing parameters. Based on the investigation, it can be inferred that the selection of the appropriate SLM parameters is very important to determined final material properties. The samples produced with the energy density E = 600 J/mm3 were observed to possess optimum properties – a homogeneous structure, density closest to the desired one, good wettability and pitting corrosion resistance.

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Authors and Affiliations

A. Woźniak
M. Adamiak
G. Chladek
J. Kasperski
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Abstract

The 17-4 PH Stainless Steel material is known for its higher strength and, therefore, extensively used to build structures for aerospace, automotive, biomedical, and energy applications. The parts must operate satisfactorily in different environmental conditions to widen the diverse application. The selective laser melting (SLM) technique build parts cost-effectively, ensuring near-net shape manufacturability. Laser power, scan speed, and hatch distance operating at different conditions were used to develop parts and optimize for higher density in printed parts. Laser power, scan speed, and hatch distance resulted in the percent contribution towards density equal to 73.74%, 24.48%, and 1.78%. The optimized conditions resulted in higher density and relative density equal to 7.76 g/cm 3 and 99.48%. Printed parts' corrosion rate and wear loss showed more stability in NaCl corrosive medium even at 75 °C than 1M of HCL corrosive medium. Less pitting corrosion was observed on the samples treated in NaCl solution at 25 °C and 75 °C at 72 Hrs than in HCL solution. Therefore, 17-4 PH SS parts are best suited even in marine applications.
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Authors and Affiliations

Priya Sahadevan
1
Chithirai Pon Selvan
2
ORCID: ORCID
G C Manjunath Patel
3
ORCID: ORCID
Amiya Bhaumik
1

  1. Lincoln University College Selangor, Malaysia
  2. Curtin University Dubai, United Arab Emirates
  3. PES Institute of Technology and Management, Shivamogga, Visvesvaraya Technological University, Belagavi, India
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Abstract

The aim of the paper is the residual stress analysis of AlSi10Mg material fabricated by selective laser melting (SLM). The SLM technique allows to product of complex geometries based on three-dimensional model, in which stiffness and porosity can be precisely designed for specific uses. As the studied material, there were chosen solid samples built in two different directions: parallel (P-L) and perpendicular (P-R) to the tested surface and cellular lattice built in perpendicular direction, as well. In the paper, for the complex characterization of obtained materials, the phase analysis, residual stress and texture studies were performed. The classical non-destructive sin2ψ method was used to measure the residual stress measurements.

The final products, both solid sample and cellular lattice, have a homogeneous phase composition and consist of solid solution Al(Si) (Fm-3m) type, Si (Fd-3m) and Mg2Si (Pnma). The obtained values of the crystallite size are in a range of 1000 Å for Al(Si), 130-180 Å for Si phase. For Mg2Si phase, the crystallite sizes depend on sintering process, they are 800 Å for solid samples and 107 Å for cellular lattice. The residual stress results have the compressive character and they are in a range from –5 to –15 MPa.

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Authors and Affiliations

M. Karolus
J. Maszybrocka
A. Stwora
G. Skrabalak
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Abstract

Industries that rely on additive manufacturing of metallic parts, especially biomedical companies, require material science-based knowledge of how process parameters and methods affect the properties of manufactured elements, but such phenomena are incompletely understood. In this study, we investigated the influence of selective laser melting (SLM) process parameters and additional heat treatment on mechanical properties. The research included structural analysis of residual stress, microstructure, and scleronomic hardness in low-depth measurements. Tensile tests with specimen deformation analysis using digital image correlation (DIC) were performed as well. Experiment results showed it was possible to observe the porosity growth mechanism and its influence on the material strength. Specimens manufactured with 20% lower energy density had almost half the elongation, which was directly connected with the porosity growth during energy density reduction. Hot isostatic pressing (HIP) treatment allowed for a significant reduction of porosity and helped achieve properties similar to specimens manufactured using different levels of energy density.

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Authors and Affiliations

J. Kluczyński
L. Śnieżek
ORCID: ORCID
K. Grzelak
ORCID: ORCID
A. Oziębło
K. Perkowski
J. Torzewski
I. Szachogłuchowicz
K. Gocman
M. Wachowski
ORCID: ORCID
B. Kania
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Abstract

Selective laser melting is one of the additive manufacturing technologies that is used to produce complex-shaped components for applications in the automotive industry. The purpose of the changes in the design, technology, and material tests was to make a steering gear housing using the SLM method. The steering gear housing was produced by the pressure casting method using an AlSi9Cu3(Fe) alloy. The construction of this housing is adapted to the specifics of left-hand traffic. The change in technology was related to the change of the position of the steering system from right-hand to left-hand and the demand for a limited number of gear housings. It was necessary to make a virtual model of the housing on the basis of the part that was removed from the vehicle. In SLM technology, the AlSi10Mg aluminum alloy was used as a raw material in the form of CL 32Al gas-atomized powder. After the SLM process was completed, the housings were subjected to heat treatment. The AlSi10Mg alloy fabricated by the SLM method after heat treatment is characterized by good plasticity and an average value of tensile strength. The last stage was to check the geometry of the SLM housing with a 3D scanner. As a result, a map of the dimensional deviations from the nominal values was obtained. This data was used to modify the CAD model before the next fabrication process.
The use of 3D printing technology allowed for the quick production of elements. The time to develop the technology and the production of the first two gear housings based on a 3D model was seven days.
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[18] Leary, M., Maconachie, T., Sarker, A. & Faruque, O. (2019). Mechanical and thermal characterisation of AlSi10Mg SLM block suport structures. Materials and Design. 183(5), 108-138. DOI: 10.1016/j.matdes.2019.108138.
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Authors and Affiliations

J. Piekło
1
ORCID: ORCID
A. Garbacz-Klempka
1
ORCID: ORCID

  1. AGH University of Science and Technology, Faculty of Foundry Engineering, Reymonta 23 Str., 30-059 Kraków, Poland
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Abstract

An investigation of the failure process of maraging steel grade X3NiCoTi18-9-5 produced by the SLM method that is subjected to various three-dimensional stress-states has been carried out. In this paper, deformations and damage evolution are analysed experimentally and numerically. Three microstructures of the SLM steel were obtained after the appropriate heat treatment. Tensile tests of smooth specimens and axisymmetric notched specimens have been performed. Numerical models of the samples with ring notches were made in order to determine the stress state and displacement field in the notch area at the moment of the sample’s breakage as well as to compare the experimentally determined effective strain in the notch after the sample’s breakage with the deformation being calculated on the basis of the numerical solution. As a result of the research, it was found that the type of fracture of samples obtained from X3NiCoTi18-9-5 steel powder by the SLM method depends on the size of the ring notch’s radius. Based on the performed numerical calculations and experimental tests, it was found that, for each of the analysed variants of heat treatment, it was possible to indicate the approximate limit value of triaxiality factor Tf, above which there is a scrap of brittle X3NiCoTi18-9-5 steel produced by the SLM method. This value is determined by the characteristic bending of the function that determines the relationship between triaxiality factor Tf and effective strain eeff.
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Authors and Affiliations

J. Piekło
1
ORCID: ORCID
A. Garbacz-Klempka
1
ORCID: ORCID

  1. AGH University of Science and Technology, Faculty of Foundry Engineering, Al. Mickiewicza 30, 30-059 Kraków, Poland
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Abstract

CM247LC alloy was manufactured by using selective laser melting (SLM) process, one of the laser powder bed fusion ­(L-PBF) methods. The hot isostatic pressing (HIP) process was additionally conducted on the SLM-built CM247LC to control its microstructures and defects. The high temperature oxidation property was investigated, and it was compared with conventional DS247LC sample (reference) prepared via the directional solidification process. The L-PBF HIP sample showed blocky-type MC carbides generated along the grain boundary with average size of about 200 nm. A semi-spherical primary γ' phase of size 0.4-1.0 μm was also observed inside the grains. Moreover, the DS247LC sample displayed a coarse eutectic γ' phase and many script-type MC carbides. Furthermore, cuboidal-type γ' with an average size of about 0.5 μm was detected. High-temperature oxidation tests were conducted at 1000°C and 1100°C for 24 hours. The results at 1100°C oxidation temperature showed that the measured oxidation weight gains for HIP and DS247LC were 1.96 mg/cm2 and 2.26 mg/cm2, respectively, indicating the superior high-temperature oxidation resistance of the L-PBF HIP sample. Based on the above results, a high-temperature oxidation mechanism of the CM247LC alloys manufactured by the SLM process and the directional solidification process has been proposed.
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Authors and Affiliations

Jung-Uk Lee
1
Young-Kyun Kim
2
ORCID: ORCID
Seong-Moon Seo
2
Kee-Ahn Lee
1
ORCID: ORCID

  1. Inha University, Department of Materials Science and Engineering, Incheon 22212, Republic of Korea
  2. Korea Institute of Materials Science, Changwon 51508, Republic of Korea
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Abstract

Microstructure and wear property of AlSi10Mg alloy manufactured by selective laser melting (SLM) were investigated. Also, the effect of post heat treatment on the mechanical and wear properties was examined. Two kinds of heat treatments (direct aging (DA) and T6) were separately conducted to SLM AlSi10Mg alloy. As-built alloy had a cellular structure formed inside the molten pool. Eutectic Si was also observed at the cellular boundary in as-built alloy. After DA heat treatment, the cellular structure still remained, and a large amount of nano-size Si particles were newly formed inside the cell structure. Both molten pool and cellular structure disappeared, and the size of Si increased in T6 alloy. The values of Vickers hardness measured as 139.4 HV (DA alloy), 128.0 HV (As-built alloy) and 85.1 HV (T6 alloy), respectively. However, concerning to wear property, T6 alloy showed better wear resistance than other alloys. The correlation between microstructure and wear mechanism of SLM AlSi10Mg alloy was also discussed.

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Authors and Affiliations

Tae-Hyun Park
Min-Seok Baek
Yongho Sohn
Kee-Ahn Lee
ORCID: ORCID
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Abstract

A powder-bed-based additive manufacturing process called electron beam melting (EBM) is defined by high temperature gradients during solidification, which produces an extremely fine microstructure compared to the traditional cast material. However, porosity and segregation defects are still present on a smaller scale which may lead to a reduction in mechanical properties. It is important to have a better knowledge of the influence of post-fabrication treatments on the microstructure and mechanical characteristics before the use of additive manufacturing parts in specific applications. In this study, the effects of solution heat treatment (SHT) and hot isostatic pressing (HIP) on the microstructure and mechanical properties of Ti-6Al-4V alloy fabricated by the EBM process have been investigated. The SHT and HIP treatments can significantly improve the ductility of EBM Ti-6Al-4V due to the coarsening of α laths and the formation of β grains.
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Authors and Affiliations

Dohoon Lee
1
ORCID: ORCID
Tae-Yeong So
1
ORCID: ORCID
Ha-Young Yu
1
ORCID: ORCID
Gyunsub Kim
2
ORCID: ORCID
Eushin Moon
2
ORCID: ORCID
Se-Hyun Ko
1
ORCID: ORCID

  1. Korea Institute of Industrial Technology (KITECH), Industrial Materials Processing R&D Department, 156, Gaetbeol-ro, Yeonsu-gu, Incheon 406-840, Republic of Korea
  2. Huneed Technologies, Incheon, Republic of Korea

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