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Abstract

This study was carried out to evaluate the aspect of microstructure and mechanical property development on additive manufactured pure Ti at elevated heat-input. For this work, pure Ti powder (commercial purity, grade 1) was selected, and selective laser melting was conducted from 0.5 to 1.4 J/mm. As a result, increase in heat-input led to the significant grain growth form 4 μm to 12 μm, accompanying with the change of grain shape, correctly widmanstätten structured grains. In addition, Vickers microhardness was notably increased from 228 Hv to 358 Hv in accordance with elevated heat-input, which was attributed to the increased concentration of oxygen and nitrogen mainly occurred during selected laser melting process.

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Authors and Affiliations

Dong-Jin Kim
Hyung-Giun Kim
Ji-Sun Kim
Kuk-Hyun Song
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Abstract

Industries that rely on additive manufacturing of metallic parts, especially biomedical companies, require material science-based knowledge of how process parameters and methods affect the properties of manufactured elements, but such phenomena are incompletely understood. In this study, we investigated the influence of selective laser melting (SLM) process parameters and additional heat treatment on mechanical properties. The research included structural analysis of residual stress, microstructure, and scleronomic hardness in low-depth measurements. Tensile tests with specimen deformation analysis using digital image correlation (DIC) were performed as well. Experiment results showed it was possible to observe the porosity growth mechanism and its influence on the material strength. Specimens manufactured with 20% lower energy density had almost half the elongation, which was directly connected with the porosity growth during energy density reduction. Hot isostatic pressing (HIP) treatment allowed for a significant reduction of porosity and helped achieve properties similar to specimens manufactured using different levels of energy density.

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Authors and Affiliations

J. Kluczyński
L. Śnieżek
ORCID: ORCID
K. Grzelak
ORCID: ORCID
A. Oziębło
K. Perkowski
J. Torzewski
I. Szachogłuchowicz
K. Gocman
M. Wachowski
ORCID: ORCID
B. Kania
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Abstract

Selective laser melting is one of the additive manufacturing technologies that is used to produce complex-shaped components for applications in the automotive industry. The purpose of the changes in the design, technology, and material tests was to make a steering gear housing using the SLM method. The steering gear housing was produced by the pressure casting method using an AlSi9Cu3(Fe) alloy. The construction of this housing is adapted to the specifics of left-hand traffic. The change in technology was related to the change of the position of the steering system from right-hand to left-hand and the demand for a limited number of gear housings. It was necessary to make a virtual model of the housing on the basis of the part that was removed from the vehicle. In SLM technology, the AlSi10Mg aluminum alloy was used as a raw material in the form of CL 32Al gas-atomized powder. After the SLM process was completed, the housings were subjected to heat treatment. The AlSi10Mg alloy fabricated by the SLM method after heat treatment is characterized by good plasticity and an average value of tensile strength. The last stage was to check the geometry of the SLM housing with a 3D scanner. As a result, a map of the dimensional deviations from the nominal values was obtained. This data was used to modify the CAD model before the next fabrication process.
The use of 3D printing technology allowed for the quick production of elements. The time to develop the technology and the production of the first two gear housings based on a 3D model was seven days.
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Bibliography

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[2] Frazier, W.E. (2014). Metal additive manufacturing: A review. Journal of Materials Engineering and Performance. 23, 1917-1928. DOI: 10.1007/s11665-014-0958-z.
[3] Sercombe, T.B. & Li, X. (2016). Selective laser melting of aluminum and aluminum metal matrix composites. Review. Materials Technology. 31(2), 77-85. DOI: 10.1179/1753555715Y.0000000078.
[4] Yadroitsev, I., Yadroitsava, I., Bertrand, P. & Smurov, I. (2012). Factor analysis of selective laser melting process parameters and geometrical characteristics of synthesized single tracks. Rapid Prototyping Journal. 18(3), 201-208. DOI: 10.1108/13552541211218117.
[5] Olakanmi, E.O. (2013). Selective laser sintering/melting (SLS/SLM) of pure Al, Al-Mg, and Al-Si powders: Effect of processing conditions and powder properties. Journal of Materials Processing Technology. 213(8), 1387-1405. DOI: 10.1016/j.jmatprotec.2013.03.009.
[6] Gibson, I., Rosen, D.W. & Stucker, B. (2010). Additive Manufacturing Technologies, Rapid Prototyping to Direct Digital Manufacturing. Springer New York Heidelberg Dordrecht London. DOI: 10.1007/978-1-4419-1120-9.
[7] Kempen, K., Thijs, L., Van Humbeeck, J. & Kruth, J.P. (2015). Processing AlSi10Mg by selective laser melting: parameter optimisation and material characterization. Materials Science and Technology. 31(8), 917-923, DOI: 10.1179/1743284714Y.0000000702.
[8] Aboulkhair, N.T., Everitt, N.M., Ashcroft, I. & Tuck, C.N. (2014). Reducing porosity in AlSi10Mg parts processed by selective laser melting. Additive Manufacturing. 1-4, 77-86. DOI: 10.1016/j.addma.2014.08.001.9.
[9] Read, N., Wang, W. & Essa, K. & Attallah, M. (2015). Selective laser melting of AlSi10Mg alloy: Process optimisation and mechanical properties development. Materials & Design. 65, 417-424. DOI: 10.1016/J.MATDES.2014.09.044.
[10] Lam, L.P., Zhang, D.Q., Liu, Z.H. & Chua, C.K. (2015). Phase analysis and microstructure characterisation of AlSi10Mg parts produced by Selective Laser Melting. Virtual and Physical Prototyping. 10 (4), 207-215. DOI: 10.1080/17452759.2015.1110868.
[11] EOS Material data sheet, EOS Aluminium AlSi10Mg. www.eos.info/03_system-related-assets/material-related-contents/metal-materials-and-examples/metal-material- datasheet/aluminium/alsi10mg-9011-0024-m400_flexline_material_data_sheet_03-18_en.pdf.
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[13] Li, W., Li, S., Liu, J., Zhang, Y., Wei, Q., Yan, C. & Shi, Y. (2016). Effect of heat treatment on AlSi10Mg alloy fabricated by selective laser melting: Microstructure evolution, mechanical properties and fracture mechanism. Materials Science and Engineering A. 663, 116-125. DOI: 10.1016/j.msea.2016.03.088.
[14] Thijs, L., Kempen, K., Kurth, J.P. & Van Humbeeck, J. (2013). Fine-structured aluminium products with controllable texture by selective laser melting of pre-alloyed AlSi10Mg powder. Acta Materialia. 61(5), 1809-1819. DOI: 10.1016/j.actamat.2012.11.052.
[15] Brandl, E., Heckenberger, U., Holzinger, V. & Buchbinder, D. (2012). Additive manufactured AlSi10Mg samples using Selective Laser Melting (SLM): Microstructure, high cycle fatigue, and fracture behavior. Materials & Design. 34, 159-169. DOI: 10.1016/j.matdes.2011.07.067.
[16] Piekło, J., Garbacz-Klempka, A., Żuczek, R. & Małysza, M. (2019). Computational modeling of fracture toughness of Al-Si, and Al-Zn-Mg-Cu alloys with detected porosity. Journal of Materials Engineering and Performance. 28, 1373-1381. DOI: 10.1007/s11665-019-03899-2.
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Authors and Affiliations

J. Piekło
1
ORCID: ORCID
A. Garbacz-Klempka
1
ORCID: ORCID

  1. AGH University of Science and Technology, Faculty of Foundry Engineering, Reymonta 23 Str., 30-059 Kraków, Poland
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Abstract

An investigation of the failure process of maraging steel grade X3NiCoTi18-9-5 produced by the SLM method that is subjected to various three-dimensional stress-states has been carried out. In this paper, deformations and damage evolution are analysed experimentally and numerically. Three microstructures of the SLM steel were obtained after the appropriate heat treatment. Tensile tests of smooth specimens and axisymmetric notched specimens have been performed. Numerical models of the samples with ring notches were made in order to determine the stress state and displacement field in the notch area at the moment of the sample’s breakage as well as to compare the experimentally determined effective strain in the notch after the sample’s breakage with the deformation being calculated on the basis of the numerical solution. As a result of the research, it was found that the type of fracture of samples obtained from X3NiCoTi18-9-5 steel powder by the SLM method depends on the size of the ring notch’s radius. Based on the performed numerical calculations and experimental tests, it was found that, for each of the analysed variants of heat treatment, it was possible to indicate the approximate limit value of triaxiality factor Tf, above which there is a scrap of brittle X3NiCoTi18-9-5 steel produced by the SLM method. This value is determined by the characteristic bending of the function that determines the relationship between triaxiality factor Tf and effective strain eeff.
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Authors and Affiliations

J. Piekło
1
ORCID: ORCID
A. Garbacz-Klempka
1
ORCID: ORCID

  1. AGH University of Science and Technology, Faculty of Foundry Engineering, Al. Mickiewicza 30, 30-059 Kraków, Poland
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Abstract

CM247LC alloy was manufactured by using selective laser melting (SLM) process, one of the laser powder bed fusion ­(L-PBF) methods. The hot isostatic pressing (HIP) process was additionally conducted on the SLM-built CM247LC to control its microstructures and defects. The high temperature oxidation property was investigated, and it was compared with conventional DS247LC sample (reference) prepared via the directional solidification process. The L-PBF HIP sample showed blocky-type MC carbides generated along the grain boundary with average size of about 200 nm. A semi-spherical primary γ' phase of size 0.4-1.0 μm was also observed inside the grains. Moreover, the DS247LC sample displayed a coarse eutectic γ' phase and many script-type MC carbides. Furthermore, cuboidal-type γ' with an average size of about 0.5 μm was detected. High-temperature oxidation tests were conducted at 1000°C and 1100°C for 24 hours. The results at 1100°C oxidation temperature showed that the measured oxidation weight gains for HIP and DS247LC were 1.96 mg/cm2 and 2.26 mg/cm2, respectively, indicating the superior high-temperature oxidation resistance of the L-PBF HIP sample. Based on the above results, a high-temperature oxidation mechanism of the CM247LC alloys manufactured by the SLM process and the directional solidification process has been proposed.
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Authors and Affiliations

Jung-Uk Lee
1
Young-Kyun Kim
2
ORCID: ORCID
Seong-Moon Seo
2
Kee-Ahn Lee
1
ORCID: ORCID

  1. Inha University, Department of Materials Science and Engineering, Incheon 22212, Republic of Korea
  2. Korea Institute of Materials Science, Changwon 51508, Republic of Korea
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Abstract

Microstructure and wear property of AlSi10Mg alloy manufactured by selective laser melting (SLM) were investigated. Also, the effect of post heat treatment on the mechanical and wear properties was examined. Two kinds of heat treatments (direct aging (DA) and T6) were separately conducted to SLM AlSi10Mg alloy. As-built alloy had a cellular structure formed inside the molten pool. Eutectic Si was also observed at the cellular boundary in as-built alloy. After DA heat treatment, the cellular structure still remained, and a large amount of nano-size Si particles were newly formed inside the cell structure. Both molten pool and cellular structure disappeared, and the size of Si increased in T6 alloy. The values of Vickers hardness measured as 139.4 HV (DA alloy), 128.0 HV (As-built alloy) and 85.1 HV (T6 alloy), respectively. However, concerning to wear property, T6 alloy showed better wear resistance than other alloys. The correlation between microstructure and wear mechanism of SLM AlSi10Mg alloy was also discussed.

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Authors and Affiliations

Tae-Hyun Park
Min-Seok Baek
Yongho Sohn
Kee-Ahn Lee
ORCID: ORCID
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Abstract

A powder-bed-based additive manufacturing process called electron beam melting (EBM) is defined by high temperature gradients during solidification, which produces an extremely fine microstructure compared to the traditional cast material. However, porosity and segregation defects are still present on a smaller scale which may lead to a reduction in mechanical properties. It is important to have a better knowledge of the influence of post-fabrication treatments on the microstructure and mechanical characteristics before the use of additive manufacturing parts in specific applications. In this study, the effects of solution heat treatment (SHT) and hot isostatic pressing (HIP) on the microstructure and mechanical properties of Ti-6Al-4V alloy fabricated by the EBM process have been investigated. The SHT and HIP treatments can significantly improve the ductility of EBM Ti-6Al-4V due to the coarsening of α laths and the formation of β grains.
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Authors and Affiliations

Dohoon Lee
1
ORCID: ORCID
Tae-Yeong So
1
ORCID: ORCID
Ha-Young Yu
1
ORCID: ORCID
Gyunsub Kim
2
ORCID: ORCID
Eushin Moon
2
ORCID: ORCID
Se-Hyun Ko
1
ORCID: ORCID

  1. Korea Institute of Industrial Technology (KITECH), Industrial Materials Processing R&D Department, 156, Gaetbeol-ro, Yeonsu-gu, Incheon 406-840, Republic of Korea
  2. Huneed Technologies, Incheon, Republic of Korea

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