Determination of the physico-chemical interactions between liquid and solid substances is a key technological factor in many industrial processes in metallurgy, electronics or the aviation industry, where technological processes are based on soldering/brazing technologies. Understanding of the bonding process, reactions between materials and their dynamics enables to make research on new materials and joining technologies, as well as to optimise and compare the existing ones. The paper focuses on a wetting force measurement method and its practical implementation in a laboratory stand – an integrated platform for automatic wetting force measurement at high temperatures. As an example of using the laboratory stand, an analysis of Ag addition to Cu-based brazes, including measurement of the wetting force and the wetting angle, is presented.

This paper presents a method for quantitative assessment of the mechanisms of nucleation and granules growth by layering in the process of bed wetting during periodic disc granulation. This study included two initial, consecutive stages of a process with defined time courses. The first phase was a time period, in which only formation of new nuclei took place, while in the second stage simultaneous nucleation and growth of granules as a result of sticking raw material grains to pre-existing nuclei occurred. Different kinds of binding liquid were used for bed wetting in each phase. In the first phase, an aqueous solution of dye was used, and pure distilled water in the second stage. The contribution of particular mechanisms to the formation of agglomerates at different time points within the second phase of the process was determined in this study. To do that the results of bed granulometric analysis, mass balance of size fractions and the analysis of contents of a marker (dye) delivered to the bed with the binding liquid during the first phase in agglomerates were used. To assess the concentration of the dye in different size fractions of the batch, spectrophotometric analysis was utilised. The study was performed using UV-VIS JASCO V-630 spectrophotometer equipped with an integrating sphere. The sieve analysis, spectrophotometric studies and mass balance were used to determine changes in the weight of the dye containing nuclei and of the nuclei containing no dye. The aforementioned analyses were also used to assess changes in the weight of formed granules and of raw material particles attached to nuclei during simultaneous nucleation and growth of granules.

In the paper, an attempt was made to evaluate the effect of preliminary wetting of high-silica base during preparation of moulding sands

containing a selected grade of sodium water-glass, designed for hardening by traditional drying or by electromagnetic microwaves at 2.45

GHz. In the research, some water was dosed during stirring the sandmix before adding 1.5 wt% of the binder that was unmodified sodium

water-glass grade 137, characterised by high molar module within 3.2 to 3.4. Scope of the examinations included determining the effect of

wetting the base on mechanical parameters like compression, bending and tensile strength, as well as on technological parameters like

permeability, abrasion resistance and apparent density. The research revealed a significant positive effect of adding water to wet surfaces

of high-silica base grains on mechanical properties and quality of moulding sands hardened by physical methods, in particular by

microwave heating

The work presents investigation on the water droplet impingement at a substrate with three different surface coating. The experiments are carried out for two temperatures of the surface: 23ºC (room temperature) and -10ºC. The water droplet contact is recorded via ultra-fast camera and simultaneously via fast thermographic camera. The wetting properties are changing for subzero temperatures of substrates.

The grain boundary wetting phase transition in an industrial EZ33A cast alloy is studied. 12% of the grain boundaries are completely wetted at the temperature slightly higher than the eutectic transformation temperature (530°C). The fraction of wetted grain boundaries increases with temperature, reaches a maximum of 85% at 570°C, and does not change further until the alloy melts. In the as-cast state, the alloy has low ductile properties at the ambient temperature. The microstructure in the as-cast state corresponds to the wetting state at about 560°C, which indicates that the cooling rate in casting is almost equal to that in quenching. The volume and the surface fraction of the second phase and the hardness measured at the least wetted state of samples point to its good machinability. The wetting data are used to suggest a sequence of heat treatment and machining for processing EZ33A alloy parts.

Some materials-related microstructural problems calculated using the phase-field method are presented. It is well known that the phase field method requires mesh resolution of a diffuse interface. This makes the use of mesh adaptivity essential especially for fast evolving interfaces and other transient problems. Complex problems in 3D are also computationally challenging so that parallel computations are considered necessary. In this paper, a parallel adaptive finite element scheme is proposed. The scheme keeps the level of node and edge for 2D and level of node and face for 3D instead of the complete history of refinements to facilitate derefinement. The information is local and exchange of information is minimized and also less memory is used. The parallel adaptive algorithms that run on distributed memory machines are implemented in the numerical simulation of dendritic growth and capillary-driven flows.

One of the parameters which enables the evaluation of carbonaceous material is the thermal effect of wetting. The value of the heat of wetting provides information about the surface energy and the texture of the materials immersed in the wetting liquid. Knowledge of the heat of wetting of the carbonaceous materials is used to research their sorption properties, to characterize the structure and to determine the surface area. A method of me asuring the wetting of the carbonaceous materials as one of the methods to evaluate the carbonaceous materials was proposed. On the basis of research which was conducted, one determined the heat of wetting black coal from the Brzeszcze mine by methyl alcohol and lignites from the Turów and Bełchatów mine. One of activated carbons furnished by the Gryfskand company (WD-extra) was selected for the purpose of the comparison. The enthalpy of immersion was calculated on the basis of the results, the surface of the carbonaceous materials that were studied. It was revealed that the energetic effects of wetting depend both upon the microporous structure and the chemical nature of the adsorbent. The greatest heat of wetting calculated per 1g of the carbonaceous material, which has the most developed surface area and micropore volume, was obtained for the activated carbon. However, the heat of wetting does not increase proportionally to the surface area. The study revealed that the thermal effects of wetting for fossil coal decreases with the increasing of the surface area. The linear relationship was obtained for the three samples which were studied. The highest thermal effects (ΔT) and heat of wetting (Q) among the fossil coals was determined for the lignite from the Bełchatów mine, even though this coal had the least-developed porous structure. One may discern a clear influence of the swelling process upon the measured thermal effects on the basis of this sample.

In this work we report on fabrication of quantum wires and quantum point contacts from the modulation doped CdMgTe/Cd(Mn)Te structures, with the application of a high-resolution electron-beam lithography. We emphasize on methods which were not yet utilized for these substrate materials. In particular, we describe the so-called shallow-etching approach, which allows for the fabrication of quantum constrictions of a physical width down to 100 nm, which are characterized by the smoother confining potential as compared to the deep-etched devices. For that purpose, a single-line exposure mode of electron-beam lithography has been used. We demonstrate also, how to combine the etching of separating grooves with the thermal evaporation of metal side-gates into a single post-processing stage of a quantum point contact fabrication.

This article is an expanded version of the scientific reports presented at the International Conference on Semiconductor Nanostructures for Optoelectronics and Biosensors 2016 ICSeNOB2016, May 22–25, 2016, Rzeszow, Poland.

Wet shotcrete technology is being gradually used in roadway support in frigid mining areas. Thus, problems such as low strength, fragility, and high repair rate have also emerged. This study focuses on low strength, cracking, and other problems in the wet shotcrete support of a mine. It introduced the fishbone diagram to investigate the effects of temperature, cement content, and water-cement ratio (W/C) on the strength of the shotcrete layer. The microscopic morphology of wet shotcrete based on scanning electron microscopy (SEM) is observed. Results demonstrated that temperature was the main influencing factor of wet shotcrete in frigid mining areas. When the curing temperature was lower than 10°C, the early strength of wet shotcrete dropped significantly. Temperatures above 15°C were favorable for later gain in strength. W/C was of a complementary relationship with strength development at different ages. Temperature was the essential factor that influenced the microscopic morphology of wet shotcrete. Furthermore, internal initial porosity and aggregate interface bonding strength had a direct effect on macro-mechanical properties of wet shotcrete.

Recently, significant progress has been made in experimental studies on the flow of wet steam, measuring techniques based on recording the phenomenon of extinction of light and ultrasound have been elaborated or improved. The basic value experimentally determined in the final stage was the content of the liquid phase defined as the wetness fraction. The methodology of tests and experimental investigations was presented, as well as the applied and developed measurement systems. Next, some developed designs of new ultrasonic and light extinction measuring probe and their modifications are described. The article presents also some examples of applications of the developed measurement techniques in application to experimental research conducted on wet steam. Examples of comparison between experimental and numerical tests for the extinction method are also provided.

In the present paper, elemental Fe, Cr and Ni powders were used to fabricate nano-structured duplex and ferritic stainless steel powders by using high energy planetary ball milling. We have studied the effect of milling atmosphere like wet (toluene) and dry (argon) milling of elemental Fe-18Cr-13Ni (duplex) and Fe-17Cr-1Ni (ferritic) powders for 10 h in a dual drive planetary mill. Stearic acid of 1wt. % was added during milling to avoid agglomeration. The dry and wet milled duplex and ferritic stainless steel powders were characterized by XRD, SEM and particle size analysis techniques. We have found that both the milling atmospheres have great influence in controlling the final particle morphology, size and phase evolution during milling. It was reported that dry milling is more effective in reducing particle size than the wet milling. The Nelson-Riley method of extrapolation was used to calculate the precise lattice parameter and Williamson-Hall method was used to calculate the crystallite size and lattice strain of both the stainless steel milled in argon atmosphere. Dry milled duplex and ferritic stainless steel were then consolidated by conventional sintering method at 1100, 1200 and 1300°C temperatures under argon atmosphere for 1 hour.

104 algal taxa (31 blue-green algae, 48 diatoms and 25 green algae) were identified from 18 stands of tundra soils in the Kaffiöyra Plain (Oscar II Land, NW Spitsbergen). Basing on numerical analysis by the reciprocal averaging method and on hierarchic classification based on ."distinguishing species", two groups of stands were distinguished: moist and wet ones characterized by diatoms, and dry and drying ones characterized by blue-green algae.

The runoff coefficient is one of the fundamental hydrological characteristics of a catchment. It indicates a share of the precipitation water that runs off from the catchment.

The results of the runoff coefficient calculation based on measurements carried out continuously in the Cerhovický Stream catchment over a considerable period of time, i.e. from 1988 up to 2006 are presented. The precipitation and runoff data in the catchment were used. Mean value of the runoff coefficient and the runoff coefficients for the agricultural and forest parts of the catchment are presented. The total mean runoff coefficient for the Cerhovický Stream is 0.19 with the standard deviation of 0.06. Mean runoff coefficient for the forest part is 0.13 and for the agricultural part – 0.24.

Differences between the years with a higher and a lower precipitation were followed as well. We also statistically evaluated possible hydrological changes caused by the construction of the highway and the market centre. For another possible explanation of quite high standard deviation of the mean annual runoff coefficient we followed the monthly runoff coefficient dependence on water temperature and of ground water table depth.