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Number of results: 8
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Abstract

In this study, we present a new method for obtaining the parameters of the Johnson-Mehl-Avrami-Kolmogorov equation for dynamic recrystallization grain size. The method consists of finite-element analysis and optimization techniques. An optimization tool iteratively minimizes the error between experimental values and corresponding finite-element solutions. Isothermal backward extrusion of the AA6060 aluminum alloy was used to acquire the main parameters of the equation for predicting DRX grain size. We compared grain sizes predicted using optimized and reference parameters with experimental values from the literature and found better agreement when the optimized parameters were applied.

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Authors and Affiliations

Missam Irani
Mansoo Joun
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Abstract

Isothermal hot compression experiments were carried out using the Gleeble-1500D thermal mechanical simulator. The flow stress of the Cu-1%Zr and Cu-1%Zr-0.15%Y alloys was studied at hot deformation temperature of 550°C, 650°C, 750°C, 850°C, 900°C and the strain rate of 0.001 s–1, 0.01 s–1, 0.1 s–1, 1 s–1, 10 s–1. Hot deformation activation energy and constitutive equations for two kinds of alloys with and without yttrium addition were obtained by correlating the flow stress, strain rate and deformation temperature. The reasons for the change of hot deformation activation energy of the two alloys were analyzed. Dynamic recrystallization microstructure evolution for the two kinds of alloys during hot compression deformation was analyzed by optical and transmission electron microscopy. Cu-1%Zr and Cu-1%Zr-0.15%Y alloys exhibit similar behavior of hot compression deformation. Typical dynamic recovery occurs during the 550-750°C deformation temperature, while dynamic recrystallization (DRX) occurs during the 850-900°C deformation temperature. High Zr content and the addition of Y significantly improved Cu-1%Zr alloy hot deformation activation energy. Compared with hot deformation activation energy of pure copper, hot deformation activation energy of the Cu-1%Zr and Cu-1%Zr-0.15%Y alloys is increased by 54% and 81%, respectively. Compared with hot deformation activation energy of the Cu-1%Zr alloy, it increased by 18% with the addition of Y. The addition of yttrium refines grain, advances the dynamic recrystallization critical strain point and improves dynamic recrystallization.
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Authors and Affiliations

K. Tian
B. Tian
A.A. Volinsky
Y. Zhang
Y. Liu
Y. Du
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Abstract

In the current study, the hot deformation of medium carbon V-Ti micro-alloyed steel was surveyed in the temperature range of 950 to 1150°C and strain rate range of 0.001 to 1 s–1 after preheating up to 1200°C with a compression test. In all cases of hot deformation, dynamic recrystallization took place. The influence of strain rate and deformation temperature on flow stress was analyzed. An increase in the strain rate and decrease in the deformation temperature postponed the dynamic recrystallization and increased the flow stress. The material constants of micro-alloyed steel were calculated based on the constitutive equations and Zener-Hollomon parameters. The activation energy of hot deformation was determined to be 458.75 kJ/mol, which is higher than austenite lattice self-diffusion activation energy. To study the influence of precipitation on dynamic recrystallization, the stress relaxation test was carried out in a temperature range of 950 to 1150°C after preheating up to 1200°C. The results showed no a stress drop while representing the interaction of particles with dynamic recrystallization.

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Authors and Affiliations

K. Tavaei
A. Meysami
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Abstract

AISI 1045 steel has the characteristics of high strain rate, large strain, and sharp rise in temperature during high-speed deformation process, resulting in a concentrated deformation band and fine structure. In this work, the microstructure of submicron-sized grains in AISI 1045 steel material formed under 10 6 s –1 during a high speed cutting process was examined. To reveal the dynamic evolution mechanism of the AISI 1045 microstructure, the continuous dynamic recrystallization theory was introduced. The results show a high dislocation density which favor the formation of small angle grain boundaries during the high speed cutting process. Kinetics calculations that use continuous dynamic recrystallization mechanisms prove that the recrystallization size is constant when the strain rate ncreases from 10 3 s –1 to 10 6 s –1, and the transition time is reduced from 6×10 –5 s to 4×10 –8 s. The recrystallization grains were gradually formed during the deformation of the material, not generated after the deformation.
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Authors and Affiliations

Lingen Luo
1
Jianming Pang
1
Yaoxin Song
1
Shulan Liu
2
Guoliang Yin
3
Hao Peng
4
Chunlei Pu
5
Yinhe Lin
4
Jingwei Li
6
Xuefeng Shi
7

  1. Resource Application and Alloy Materials Division, China Iron and Steel Research Institute Group, Beijing, 100081, P.R. China
  2. Tangshan Normal University, School of Physical Science and Technology, Tangshan, 063000, P.R. China
  3. Yibin University, Depart ment of Materials and Chemical Engineering, Yibin, 644000, P.R. China
  4. Yangtze Normal University, Institute of Chemical Engineering, Chongqing, 408100, P.R. China
  5. MCC Huatian Engineering & Technology Corporation, Nanjing, 210019, P.R. China
  6. School of Materials Science and Engineering, Hefei University of Technology, Hefei, 230009, P.R. China
  7. North China University of Science and Technology, College of Metallurgy and Energy, Tangshan, 063210, P.R. China
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Abstract

The high-temperature deformation process and dynamic recrystallization (DRX) process of 21-4N were investigated under the conditions of the deformation temperature range of 1273~1453K, the strain rate range of 0.01~10s–1 and the deformation degree of 60% (the total deformation is 0.916) by using Gleeble-1500D thermal simulated test machine. The curves of stress-strain (σ – ε) were obtained, and the curves of work hardening rate (θ) and strain (ε) were obtained by taking derivative of σ – ε. The DRX critical strains under different conditions were determined by the curves of work hardening rate (θ – ε), and the DRX critical strain model was established. The peak strains of 21-4N were obtained by the curves of σ – ε, the relationship between peak stress (σp) and critical strain (εc) was determined, and the peak strain model was established. The DRX volume fraction models of 21-4N were established by using Avrami equation. The DRX grain size of 21-4N was calculated by Image Pro Plus 6.0, and its DRX grain size models were established.

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Authors and Affiliations

Yiming Li
Xiaomin Huang
Hongchao Ji
Yaogang Li
Baoyu Wang
Xuefeng Tang
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Abstract

A hot compression test was conducted on a Gleeble-3500 thermo-simulation machine to study the critical conditions and kinetics of dynamic recrystallization in a high-carbon tool steel. The critical conditions for the initiation of dynamic recrystallization were determined using the working-hardening theory. The quantitative relationship between the critical characteristics of dynamic recrystallization and the hot deformation parameters were elucidated based on two different methods:the apparent method and physically based method. It was found that the two methods both have high applicability for the investigated steel, but the physically-based method needs less parameters and makes it possible to study the effect of different factors. A dynamic recrystallization kinetics model was used to calculate the recrystallization volume fraction under different conditions. The calculation results matched well with the data obtained from the flow curves.

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Authors and Affiliations

Yong-Ji Zhang
Guang-Liang Wu
Shang-Wen Wu
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Abstract

This study investigated the effect of adding Al–5Ti–1B grain refiner on the solidification microstructure and hot deformation behavior of direct-chill (DC) cast Al–Zn–Mg–Cu alloys. The grain refiner significantly decreased the grain size and modified the morphology. Fine-grained (FG) alloys with grain refiners exhibit coarse secondary phases with a reduced number density compared to coarse-grained (CG) alloys without grain refiners. Dynamic recrystallization (DRX) was enhanced at higher compression temperatures and lower strain rates in the CG and FG alloys. Both particle stimulated nucleation (PSN) and continuous dynamic recrystallization (CDRX) are enhanced in the FG alloys, resulting in decreased peak stress values (indicating DRX onset) at 450°C. The peak stress of the FG alloys was higher at 300-400°C than that of the CG alloys because of grain refinement hardening over softening by enhanced DRX.
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Authors and Affiliations

Junho Lee
1
ORCID: ORCID
Namhyuk Seo
1
ORCID: ORCID
Sang-Hwa Lee
2
ORCID: ORCID
Kwangjun Euh
2
ORCID: ORCID
Singon Kang
3
ORCID: ORCID
Seung Bae Son
1 4
ORCID: ORCID
Seok-Jae Lee
1 4
ORCID: ORCID
Jae-Gil Jung
1 4
ORCID: ORCID

  1. Jeonbuk National University, Division of Advanced Materials Engineering, Jeonju 54896, Republic of Korea
  2. Korea Institute of Materials Science, Advanced Metals Division, Changwon 51508, Republic of Korea
  3. Dong-A University, Department of Materials Science And Engineering, Busan 49315, Republic of Korea
  4. Jeonbuk National University, Research Center for Advanced Materials Development, Jeonju 54896, Republic of Korea

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