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Abstract

The subject of the study concerns the enhancement of corrosion and wear resistance of nitrided 42CrMo4 steel by the formation of zinc phosphate top layer. The present work is aimed at the assessment of the effect of increasing thickness of nitrided layer from approximately 2 µm to 16 µm on the morphology and properties of zinc phosphate coating. XRD analysis showed that along with the increase in the thickness of the nitrides layer, a change in the phase composition was observed. SEM/EDS examination revealed that top layer consists of crystalline zinc phosphate coating. The shape and size of crystals does not significantly depend on a thickness of nitrides layer but corrosion resistance determined by potentiodynamic method in 0.5M NaCl increased with an increase of thickness of a “white layer”. Similarily the wear resistance determined by the 3-cone-roll test was also the highest for 16 µm nitride layer.

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Authors and Affiliations

A. Kapuściński
L. Kwiatkowski
P. Wach
A. Mazurek
R. Diduszko
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Abstract

Thermochemical treatment processes are used to produce a surface layer of the workpiece with improved mechanical properties. One of the important parameters during the gas nitriding processes is the temperature of the surface. In thermochemical treatment processes, there is a problem in precisely determining the surface temperature of heat-treated massive components with complex geometries. This paper presents a simulation of the heating process of a die used to extrude aluminium profiles. The maximum temperature differences calculated in the die volume, on the surface and at the most mechanically stressed edge during the extrusion of the aluminum profiles were analysed. The heating of the die was simulated using commercial transient thermal analysis software. The numerical calculations of the die assumed a boundary condition in the form of the heat transfer coefficient obtained from experimental studies in a thermochemical treatment furnace and the solution of the nonstationary and non-linear inverse problem for the heat conduction equation in the cylinder. The die heating analysis was performed for various heating rates and fan settings. Major differences in the surface temperature and in the volume of the heated die were obtained. Possible ways to improve the productivity and control of thermochemical treatment processes were identified. The paper investigates the heating of a die, which is a massive component with complex geometry. This paper indicates a new way to develop methods for the control of thermochemical processing of massive components with complex geometries.
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Authors and Affiliations

Damian Joachimiak
1
Wojciech Judt
1
Magda Joachmiak
1

  1. Poznan University of Technology, Institute of Thermal Engineering, Piotrowo 3a, 60-965, Poznan, Poland
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Abstract

Deep cryogenic treatment (DCT) is gaining popularity as a treatment used to modify structures obtained during heat or thermo-chemical treatment. The article presents the influence of DCT, carried out during heat treatment before and after gas nitriding processes, on the formation of gas nitrided layers on X153CrMoV12 steel. It was found that the use of DCT between quenching and tempering performed prior to gas nitriding processes, increases the hardness, thickness and wear resistance of the nitrided layers. At the same time, if we apply cryogenic treatment during post-heat treatment of nitrided layers, we also get very high wear resistance and increased thickness of nitrided layers, in comparison with conventional gas nitriding of X153CrMoV12 steel. In this case, DCT significantly increases also the hardness of the core by the transformation of retained austenite and the precipitation of fine carbides of alloying elements.

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Authors and Affiliations

P. Wach
A. Ciski
T. Babul
A. Kapuścińska
D. Oleszak

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