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Abstract

The present paper is a presentation of results of a study on morphology, chemical composition, material properties (HVIT, HIT, EIT), and nanoindentation elastic and plastic work for carbide precipitates in chromium cast iron containing 24% Cr. It has been found that the carbides differ in chemical composition, as well as in morphology and values characterizing their material properties. The carbides containing the most chromium which had the shape of thick and long needles were characterized with highest values of the analyzed material properties.

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Authors and Affiliations

A.W. Orłowicz
M. Mróz
M. Tupaj
A. Trytek
M. Jacek
M. Radoń
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Abstract

The work presents a computer simulation realized with the ADINA program concerning nanoindendation test. A shape of nanoindenter was proposed to be similar to the real surgical tools. The theoretical model was used to predict phenomena which would appear in practice. The contribution of the TiN coating thickness to the implant rigid properties was simulated. Three types of extortion conditions could be considered, i.e., short contact with surgery tool (i); long continuous contact with natural tissue (ii); long cyclic contact with natural tissue (iii). In the first part of the work, the authors focused on the first type of extortion (i). The second part of the work is dedicated to the calculations of temperature impact to layer behaviour. Two layer thicknesses are considered i.e., 250 nm and 50 nm. The examined coatings find serious practical applications as a blood-contacting material in medicine. The coatings were subjected to transmission electron microscopy investigations. Columnar mechanism of film growth controlled by kinetic process is stated to operate for the considered range of layer thickness. Plasma temperature is observed to influence the substrate behaviour. Examinations of thinner layers, i.e. under 100nm, revealed higher degree of smoothness and uniformity, which could be related to the operation of the surface diffusion mechanism at the early stage of deposition. The physical explanation of TEM images was based on the finite element calculations of the temperature distribution using the ADINA program .

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Authors and Affiliations

R. Major
P. Lacki
J.M. Lackner
B. Major
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Abstract

This study investigates the effects of grain boundary structures on mechanical properties of nanocrystalline Al-0.7Mg-1.0Cu alloy using nanoindentation system. Grain boundary structure transforms to high angle grain boundaries from low angle ones with increase of heat treatment temperature and the transformation temperature is about 400℃. Young’s modulus and hardness are higher in sample with low angle grain boundaries, while creep length is larger in sample with high angle ones. These results indicate that progress of plastic deformation at room temperature is more difficult in sample with low angle ones. During compression test at 200℃, strain softening occurs in all samples. However, yield strength in sample with low angle grain boundaries is higher twice than that with high angle ones due to higher activation energy for grain boundary sliding.
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Bibliography

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Authors and Affiliations

Jin Man Jang
1 2
ORCID: ORCID
Wonsik Lee
1
ORCID: ORCID
Se-Hyun Ko
1
ORCID: ORCID

  1. Korea Institute of Industrial Technology, Incheon, 21999, Republic of Korea
  2. Inha University, Department of Materials Science and Engineering, Incheon, 22212, Republic of Korea
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Abstract

Thermal spraying methods are commonly used to regenerate damaged surface or change materials surface properties. One of the newest methods is cold spraying, where coating is deposited of material in the solid state. Therefore shape and size of the powder particles are very important parameters. The article presents the influence of copper powder morphology on mechanical properties of the coatings (adhesion, hardness, Young’s modulus) deposited with the Low Pressure Cold Spraying method on the AA1350 aluminium alloy substrate. The coatings were deposited using two commercially available copper powders with spherical and dendritic morphology and granulation of –40+10 µm. The bond strength of coatings was determined with the pull off method, the hardness with the Vickers method at load of 2.94 N, while the Young’s modulus through measurement of nanoindentation. Microstructure of the coatings was analysed using the light and scanning electron microscopy (SEM). Shape of the powder influences mechanical properties of the coating significantly. The coatings deposited with dendritic powder had low mechanical properties, hardness of the 81 HV0.3 order and adhesion of about 4 MPa. However changing powder morphology to spherical increased hardness of the coating to 180 HV0.3 and adhesion to 38.5 MPa.
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Authors and Affiliations

D. Grygier
1
ORCID: ORCID
M. Rutkowska-Gorczyca
1
ORCID: ORCID
M.G. Winnicki
2
ORCID: ORCID
T. Wojdat
2
ORCID: ORCID

  1. Wroclaw University of Science and Technology, Faculty of Mechanical Engineering, Department of Vehicle Engineering, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland
  2. Wroclaw University of Science and Technology, Faculty of Mechanical Engineering, Department of Metal Forming, Welding and Metrology, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland

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