This paper presents the results of experimental drum granulation of silica flour with the use of wetting liquids with different values of surface tension. Additionally, different liquid jet breakup and different residual moisture of the bed were applied in the tests. The process was conducted periodically in two stages: wetting and proper granulation, during which no liquid was supplied to the bed. The condition of the granulated material after the period of wetting (particle size distribution and moisture of separate fractions) and a change in the particle size distribution during the further conduct of the process (granulation kinetics) were determined.
The analysis of particle size in suspensions carried out with use of the laser diffraction method enables us to obtain not only information about the size of particles, but also about their properties, shape and spatial structure, determined basing on fractal dimension. The fractal dimension permits the evaluation of the interior of aggregates, at the same time showing the degree of complexity of the matter. In literature, much attention is paid to the evaluation of the fractal dimension of flocs in activated sludge, in the aspect of control of single processes, i.e. sedimentation, dehydration, coagulation or flocculation. However, results of research concerning the size of particles and the structure of suspensions existing in raw and treated sewage are still lacking. The study presents optical fractal dimensions D3 and particle size distributions measured with use of laser granulometer in raw and treated sewage and activated sludge collected from six mechanical-biological wastewater treatment plants located in the Lower Silesian region. The obtained test results demonstrate that wastewater treatment plants that use both sequencing batch reactors and continuous flow reactors are more efficient at capturing suspension particles of a size up to 30 μm and are characterized by an increased removal of particles of a size ranging from 30 μm to 550 μm to the outflow. Additionally, in the case of samples of treated sewage and activated sludge collected at the same location, at short intervals, similar particle distributions were observed. As far as the analysis of fractal dimensions is concerned, particles contained in the raw sewage suspension were characterized by the lowest values of the fractal dimension (median equals 1.89), while the highest values occurred in particles of activated sludge (median equals 2.18). This proves that the spatial structure of suspension particles contained in raw sewage was similar to a linear structure, with a large amount of open spaces, while the structure of particles contained in the activated sludge suspension was significantly more complex in the spatial aspect.
Complex circuit of milling-classify systems are used in different branches of industry, because the required particle size distribution of product can seldom be reached in a single-stage grinding on the same device. The multistage processes of comminution and classification make possible suitable selection of parameters process for variables graining of fed material, mainly through sectioning of devices or change of their size and the types. Grinding material usually contains size fractions, which meet the requirements relating finished product. Then profitable is preliminary distributing material on a few size fractions, so to deal out with them demanded fraction of product, whereas remaining to direct alone or together with fed material to the same or different device. If the number of mills and classifiers in a circuit is large enough, building the model of particle size distribution transformation becomes rather complicated even for the circuit of a given structure. The situation becomes much more complicated, if we want to compare characteristics of all possible circuits, that can be constructed from these mills and classifiers, because the number of possible circuits increases greatly with the increase of number of devices being in the milling-classify system. The method creating matrix model for transformation of particle size distribution in a circuit of arbitrary structure of milling-classify system is presented in the article. The proposed model contains the mass population balance of particle equation, in which are block matrices: the matrix of circuit M, the matrix of inputs F and the matrix of feed F0. The matrix M contains blocks with the transition matrix P, the classification matrix C, the identity matrix I and the zero matrix 0 or elements describing the transformation of particle size distribution in the circuit. The matrix F is the block column matrix, which elements describing all particle size distributions at inputs to the circuit elements. The matrix F0 is the block column matrix, which elements describing particle size distributions in all feeds to the circuit. In paper was discussed this model in details, showed algorithm and three examples formatrix construction for the closed circuit ofmilling-classify systems. In conclusion was affirmed, that presented model makes possible to forecasting particle size distribution of grinding product, which leaving chosen the unit of system. The matrix model can be applied to improving modeling of mineral processing in the different grinding devices.