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Number of results: 14
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Abstract

The temperature dependence of the particle size distribution (PSD) of the magnetic fluid with an additional biocompatible dextran layer was studied using a ultrasonic method. The measurements of the ultrasound velocity and attenuation were carried out as a function of the volume concentration of magnetite particles at temperatures ranging from 15°C to 40°C. In order to extract the PSD from ultrasonic measurements, the theoretical model of Vinogradov-Isakovich was used. The extraction of PSD from the ultrasonic data requires also the measurements the density and viscosity of the ferrofluid samples. The calculated PSD of the magnetic fluid with an additional biocompatible layer shows a greater thermal stability than that of a magnetic fluid with a single surfactant layer.
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Authors and Affiliations

Leszek Dąbek
Tomasz Hornowski
Arkadiusz Józefczak
Andrzej Skumiel
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Abstract

This paper presents the results of experimental drum granulation of silica flour with the use of wetting liquids with different values of surface tension. Additionally, different liquid jet breakup and different residual moisture of the bed were applied in the tests. The process was conducted periodically in two stages: wetting and proper granulation, during which no liquid was supplied to the bed. The condition of the granulated material after the period of wetting (particle size distribution and moisture of separate fractions) and a change in the particle size distribution during the further conduct of the process (granulation kinetics) were determined.

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Authors and Affiliations

Michał Błaszczyk
Andrzej Heim
Tomasz P. Olejnik
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Abstract

Accurate estimation of soil permeability is crucial in many geotechnical applications. Empirical and theoretical equations based on soil particle size distribution (PSD) offer a fast and cheap way for preliminary estimation of permeability in granular soils, however the results obtained from various formulas available in the literature often show significant discrepancies. While several comparative studies on this topic have been published, no definite conclusions can be drawn on the performance of the predictive equations in comparison with in-situ permeability measurements. Many formulas require porosity or void ratio as input parameter, which is difficult to obtain for granular soil in-situ. In this study we applied 30 predictive equations to estimate permeability of sandy soil in an outwash plain deposit. The equations were divided into 5 groups, based on their structure and the required input parameters. Empirical formulas were used to estimate the expected in-situ porosity range. The obtained permeability values were compared to the results of in-situ permeameter measurements and pumping tests. Significant differences in the results and in their sensitivity to porosity were found between the 5 groups of methods. In general, simple equations which do not include porosity were in better agreement with measurements than the other groups.
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Authors and Affiliations

Wioletta Gorczewska-Langner
1
ORCID: ORCID
Anna Gumuła-Kawecka
1
ORCID: ORCID
Beata Jaworska-Szulc
1
ORCID: ORCID
Rafael Angulo-Jaramillo
2
ORCID: ORCID
Adam Szymkiewicz
3
ORCID: ORCID

  1. Gdansk University of Technology, Faculty of Civil and Environmental Engineering, ul. Narutowicza11, 80-233 Gdansk, Poland
  2. Laboratoire LEHNA, 3, rue Maurice Audin, 69518 Vaulx-en-Velin, Franc
  3. Gdansk University of Technology, Faculty of Civil and Environmental Engineering, ul. Narutowicza 11, 80-233 Gdansk, Poland
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Abstract

This paper deals with the problem of determining the particle size distribution of selected organic soils from the vicinity of Rzeszów (Poland), using a laser diffractometer method, the knowledge of which will allow to determine the degree of differentiation or similarity of the tested organic soils in this aspect. The HELOS Laser Diffractometer manufactured by Sympatec GmbH was used for the tests. For proper analysis, the researches results in the form of graphs were grouped according to the content of organic substances in accordance with the standard classification. The conducted research was primarily aimed at presenting the grain differentiation and particle size distribution in terms of the applied method and comparing the test results of samples of selected, different organic soils, prepared using the same dispersion procedure and carried out in exactly the same test conditions, generated using capabilities of a diffractometer. Summing up, the laser diffractometer method presented in the article, although not fully verified in the case of organic soils, seems to be a the perspective method with capabilities allowing it to be nominated as an exceptionally useful method for the investigations of soft soils, including organic soils.
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Authors and Affiliations

Grzegorz Straż
1
ORCID: ORCID

  1. Rzeszow University of Technology, Faculty of Civil and Environmental Engineering and Architecture Civil Engineering, al. Powstanców Warszawy 12, 35-959 Rzeszow, Poland
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Abstract

The article presents the study results of electropulse grinding of amber in aqueous and alcoholic media at different amounts of supplied energy. Description of the electropulse grinding laboratory installation, the mechanism of the destruction process of amber particles and methods of statistical processing of experimental data are given. It was established that alcohol medium has a greater impact on the efficiency of crushing than water. Thus, under the same conditions of energy supply, in the aqueous medium the weighted average particle size of amber was 601:6±688:9 μm, and in an alcohol medium – 368:0±269:6 μm. In an aqueous medium, the particle size decreased to 1/13.6 of raw sample, and in an alcoholic medium to 1/22.3 of raw sample compared to the initial size of raw amber. We found that in the aqueous medium the ratio of large to small fractions is mainly the same with the coefficient of alignment of particles with a size of 1.09. In an alcoholic medium, this ratio significantly differs, with the coefficient of alignment of amber particles of a size of 1.67 with the amount of supplied energy of 125 kJ.
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Bibliography

[1] Y.M. Wang, M.X. Yang, and T. You. Latest progress of pressed amber. Journal of Gems & Gemmology, 14(1):38–45, 2012.
[2] N.V. Martynov, V.N. Dobromirov, and D.V. Avramov. Electro-hydraulic disintegration technology for diamond-bearing rocks. Ore Dressing, 2020(1):8–14. 2020. doi: 10.17580/or.2020.01.02 (in Russian).
[3] U. Andres. Development and prospects of mineral liberation by electrical pulses. International Journal of Mineral Processing, 97(1-4):31–38. 2010. doi: 10.1016/j.minpro.2010.07.004.
[4] D. Yan, D. Bian, J. Zhao, and S. Niu. Study of the electrical characteristics, shock-wave pressure characteristics, and attenuation law based on pulse discharge in water. Shock and Vibration, 2016:6412309, 2016. doi: 10.1155/2016/6412309.
[5] T. Krytska and T. Lytvynenko. Electropulse crushing of high-purity crystalline silicon in an aqueous medium. Metallurgy, 1(35):54–57, 2016. (in Ukrainian).
[6] N. Martynov, D.Avramov, G.Kozlov, and M. Pushkarev. Pulsed electric discharge in an aqueous medium for processing raw amber. Journal of Physics: Conference Series, 1614(1):012060, 2020. doi: 10.1088/1742-6596/1614/1/012060.
[7] X. Zhang, B. Lin, C. Zhu, Y. Wang, C. Guo, and J. Kong. Improvement of the electrical disintegration of coal sample with different concentrations of NaCl solution. Fuel, 222:695–704, 2018. doi: 10.1016/j.fuel.2018.02.151.
[8] A.P. Smirnov, V.G. Zhekul, E.I. Taftai, O.V. Khvoshchan, and I. S. Shvets. Effect of parameters of liquids on amplitudes of pressure waves generated by electric discharge. Surface Engineering and Applied Electrochemistry, 55(1):84–88, 2019. doi: 10.3103/S1068375519010149.
[9] V. Chornyi, T. Mysiura, N. Popova, and V. Zavialov. Solvent selection for extraction of target components from amber. Journal of Chemistry and Technologies, 29(1):92–99, 2020, doi: 10.15421/082106. (in Ukrainian).
[10] P.A. Kouzov. Fundamentals of disperse composition analysis of industrial dusts and ground materials. Chemistry, 1987. (in Russian).
[11] A.R. Demidov and S.E. Chirikov. Grinding methods and methods for evaluating their effectiveness. Report of Central Institute of Scientific and Technical Information and Technical and Economic Research of the Committee of Procurements of the USSR, Moscow, 1969. (in Russian).
[12] G.A. Egorov, V.T. Linnichenko, E.M. Melnikov, and T. P. Petrenko. Workshop on technology of flour, cereals and compound feed. Agropromizdat, Moscow, 1991. (in Russian).
[13] B.P. Demidovich and I.A. Maron. Fundamentals of Computational Mathematics. Science, Moscow, 1970. (in Russian).
[14] H. M. Bartenev. The statistical nature of strength and discrete levels of strength and durability of polymers. In: Strength and degradation mechanism of polymers, pages 243–261. Chemisty, 1984. (in Russian).
[15] W. Zuo, X. Li, F. Shi, R. Deng,W. Yin, B. Guo, and J. Ku. Effect of high voltage pulse treatment on the surface chemistry and floatability of chalcopyrite and pyrite. Minerals Engineering, 147:106170, 2020. doi: 10.1016/j.mineng.2019.106170.
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Authors and Affiliations

Valentyn Chornyi
1
ORCID: ORCID
Yevgen Kharchenko
1
ORCID: ORCID
Taras Mysiura
1
ORCID: ORCID
Nataliia Popova
1
ORCID: ORCID
Volodymyr Zavialov
1
ORCID: ORCID

  1. Institute of Food Technologies, National University of Food Technologies, Kyiv, Ukraine.
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Abstract

The analysis of particle size in suspensions carried out with use of the laser diffraction method enables us to obtain not only information about the size of particles, but also about their properties, shape and spatial structure, determined basing on fractal dimension. The fractal dimension permits the evaluation of the interior of aggregates, at the same time showing the degree of complexity of the matter. In literature, much attention is paid to the evaluation of the fractal dimension of flocs in activated sludge, in the aspect of control of single processes, i.e. sedimentation, dehydration, coagulation or flocculation. However, results of research concerning the size of particles and the structure of suspensions existing in raw and treated sewage are still lacking. The study presents optical fractal dimensions D3 and particle size distributions measured with use of laser granulometer in raw and treated sewage and activated sludge collected from six mechanical-biological wastewater treatment plants located in the Lower Silesian region. The obtained test results demonstrate that wastewater treatment plants that use both sequencing batch reactors and continuous flow reactors are more efficient at capturing suspension particles of a size up to 30 μm and are characterized by an increased removal of particles of a size ranging from 30 μm to 550 μm to the outflow. Additionally, in the case of samples of treated sewage and activated sludge collected at the same location, at short intervals, similar particle distributions were observed. As far as the analysis of fractal dimensions is concerned, particles contained in the raw sewage suspension were characterized by the lowest values of the fractal dimension (median equals 1.89), while the highest values occurred in particles of activated sludge (median equals 2.18). This proves that the spatial structure of suspension particles contained in raw sewage was similar to a linear structure, with a large amount of open spaces, while the structure of particles contained in the activated sludge suspension was significantly more complex in the spatial aspect.

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Authors and Affiliations

Magdalena Kuśnierz
Paweł Wiercik
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Abstract

This paper presents an effect of general dimensions of a reverse flow mini-cyclone with a tangential inlet on its separation efficiency. Several mini-cyclone design modifications are presented and evaluated for use in the air filtration systems of motor vehicles. Local design improvements of three components of a reverse flow mini-cyclone with a tangential inlet D-40 of an air filter fitted in an all-terrain vehicle engine were introduced. An asymmetric curvilinear shape of an outlet port was used instead of a symmetrical shape. An outlet vortex finder inlet port shape was streamlined, and a cylindrical outlet vortex finder of the cyclone was replaced with a conical one. Experimental evaluation of the effects of the design improvements of mini-cyclone on its separation efficiency and performance as well as flow resistance was carried out. Separation efficiency of the cyclone was determined using the mass method as a product of dust mass retained by the mini-cyclone and supplied to the mini-cyclone in a specified time. Separation performance of the cyclone was determined as the largest dust particle dz =dzmax in a specific test cycle in the cyclone outlet air stream. A polydisperse PTC-D test dust used in Poland, a substitute for AC-fine test dust was used. Dust concentration at the mini-cyclone inlet was kept at 1 g/m3. The size and total number of dust particles in the air stream at the outlet of the original mini-cyclone and at the outlet of the improved mini-cyclone was determined using a particle counter.
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Authors and Affiliations

Tadeusz Dziubak
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Abstract

The work presents results of solution combustion method utilization for yttria (Y2O3) nanopowder fabrication. Experiments were carried out with four different reducing agents: urea, glycine, citric acid and malonic acid added in stoichiometric ratio. The reactions were investigated using simultaneous DSC/DTA thermal analysis. After synthesis the reaction products were calcined at temperature range of 800-1100°C and analyzed in terms of particle size, specific surface area and morphology. Best results were obtained for nanoyttria powder produced from glycine. After calcination at temperature of 1100°C the powder exhibits in a form of nanometric, globular particles of diameter <100 nm, according to SEM analysis. The dBET for thus obtained powder is 104 nm, however the powder is agglomerated as the particle size measured by dynamic light scattering analysis is 1190 nm (dV50).
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Authors and Affiliations

M. Gizowska
I. Kobus
K. Perkowski
M. Piątek
G. Konopka
I. Witosławska
M. Osuchowski
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Abstract

Complex circuit of milling-classify systems are used in different branches of industry, because the required particle size distribution of product can seldom be reached in a single-stage grinding on the same device. The multistage processes of comminution and classification make possible suitable selection of parameters process for variables graining of fed material, mainly through sectioning of devices or change of their size and the types. Grinding material usually contains size fractions, which meet the requirements relating finished product. Then profitable is preliminary distributing material on a few size fractions, so to deal out with them demanded fraction of product, whereas remaining to direct alone or together with fed material to the same or different device. If the number of mills and classifiers in a circuit is large enough, building the model of particle size distribution transformation becomes rather complicated even for the circuit of a given structure. The situation becomes much more complicated, if we want to compare characteristics of all possible circuits, that can be constructed from these mills and classifiers, because the number of possible circuits increases greatly with the increase of number of devices being in the milling-classify system. The method creating matrix model for transformation of particle size distribution in a circuit of arbitrary structure of milling-classify system is presented in the article. The proposed model contains the mass population balance of particle equation, in which are block matrices: the matrix of circuit M, the matrix of inputs F and the matrix of feed F0. The matrix M contains blocks with the transition matrix P, the classification matrix C, the identity matrix I and the zero matrix 0 or elements describing the transformation of particle size distribution in the circuit. The matrix F is the block column matrix, which elements describing all particle size distributions at inputs to the circuit elements. The matrix F0 is the block column matrix, which elements describing particle size distributions in all feeds to the circuit. In paper was discussed this model in details, showed algorithm and three examples formatrix construction for the closed circuit ofmilling-classify systems. In conclusion was affirmed, that presented model makes possible to forecasting particle size distribution of grinding product, which leaving chosen the unit of system. The matrix model can be applied to improving modeling of mineral processing in the different grinding devices.

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Authors and Affiliations

Daniel Zbroński
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Abstract

The article provides an assessment of soil fertility indicators of agricultural lands in the northern foreststeppe of the Republic of Bashkortostan within the Iglinsky region (Russian Federation). The content of humus, mobile phosphorus, exchangeable potassium, the thickness of the humus horizon, granulometric composition, morphological properties and soil washout were studied. It was revealed that the soil-forming process occurs on rocks of different ages and genesis, such as diluvial carbonate and carbonate-free clays and heavy loams, limestone eluvium, sandstone eluvium and alluvial deposits, which determine the diversity of the soil cover. In the study area, water erosion processes are developing, influenced by anthropogenic and natural factors such as planar and linear washout on slopes with a steepness of more than 2–3° and high ploughing of agricultural land. In terms of humus content, low-humus and medium-humus soils are widespread, accounting for 45.5 and 40%, respectively. The soil map was corrected and digitised to identify the main types and subtypes of soils, indicating the varieties at a scale of 1: 25,000. Digitised maps, taking into account the current state of soil fertility, are used to develop projects for inter-farm and intra-farm land management of organisations of the agro-industrial complex, state cadastral valuation of agricultural land, determination of land tax and development of measures to improve soil fertility.
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Authors and Affiliations

Anna Kiseleva
1
Ilgiz Asylbaev
1
ORCID: ORCID
Ayrat Khasanov
1
ORCID: ORCID
Ramil Mirsayapov
1
ORCID: ORCID
Nadezhda Kurmashev
1

  1. Federal State Budgetary Educational Establishment of Higher Education “Bashkir State Agrarian University”, 50 Let Oktyabrya St, 34, Ufa, Republic of Bashkortostan, 450001, Russian Federation
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Abstract

The paper presents an experimental confirmation of the fact that if a three-dimensional volume does not contain spherical particles with particular size, the Probability Density Function (PDF1) of half-chord lengths has proportional ranges. This fact has been deduced in work [1] during the derivation process of the Probability Density Function (PDF3) that maps the particle radii on the basis of data (PDF1) collected from flat cross-sections. The experiment has been executed virtually by using a simple computer program written in the C++11 language. The computer generation of particles allowed imposing various kinds of known PDF3 and the ranges in which the particles could not be created. Next, the virtual nodules have been used to produce sets of chords that served as input data to create histograms that approximated the continuous PDF1. Having such histograms, it was possible to reveal proportional scopes of the PDF1. The proportional dependencies occurred in the same ranges where the nodules had not been generated.
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Bibliography

[1] Gurgul, D., Burbelko, A. & Wiktor T. (2021). Derivation of equation for a size distribution of spherical particles in non-transparent materials. Journal of Casting & Materials Engineering. 5(4), 53-60.
[2] Wicksell, S.D. (1925). The corpuscle problem: mathematical study of a biometric problem. Biometric. 17 (1/2), 84-89.
[3] Sheil, E. (1935). Statistische gefügeuntersuchungen I. Zeitschrift für Metallkunde. 27 (9), 199-208.
[4] Schwartz, H.A. (1934). The metallographic determination of the sze distribution of temper carbon nodules. Metals and Alloys. 5, 139-140.
[5] Saltykov, S.A. (1967). The determination of the size distribution of particles in an opaque material from the measurement of the size distribution of their section. in the second international congress for stereology, Chicago, 8-13 April 1967. Berlin–Heidelberg–New York, Springer Verlag.
[6] Cahn, J.W. & Fulmann, R.L. (1956) On the use of lineal analysis for obtaining particle size distributions in opaque samples. Transactions, American Institute of Mining, Metallurgical and Petroleum Engineers. 206, 177-187. [7] Lord, G.W. & Willis, T.F. (1951). Calculation of air bubble size distribution from results of a rosiwal traverse of aerated concrete. ASTM Bulletin. 177, 177-187.
[8] Spektor, A.G. (1950). Analysis of distribution of spherical particles in non-transparent structures. Zavodsk. Lab. 16, 173-177.
[9] https://www.cplusplus.com (date of access 06.06.2021).
[10] Burbelko, A., Gurgul, D., Guzik, E. & Kapturkiewicz, W. (2018). Stereological analysis of the statistical distribution of the size of graphite nodules in DI. Materials Science Forum. 925, 98-103.
[11] Fras, E., Burbelko, A.A. & Lopez, H.F. (1996). Secondary nucleation of eutectic graphite grains. Transactions of the American Foundrymen Society. 104, 1-4.

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Authors and Affiliations

D. Gurgul
1

  1. AGH University of Science and Technology, Kraków, Poland
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Abstract

The article discusses a new mathematical method for comparing the consistency of two particle size distribution curves. The proposed method was based on the concept of the distance between two graining curves. In order to investigate whether the distances between the particle size distribution curves are statistically significant, it was proposed to use the statistical test modulus-chi. As an example, the compliance of three sieve curves taken from the earth dam in Pieczyska on the Brda River in Poland was examined. In this way, it was established from which point of the dam the soil was washed away. However, it should be remembered that the size of the soil grains built into the dam does not have to be identical to the grain size of the washed out soil, because the fine fractions will be washed away first, while the larger ones may remain in the body of the earth structure.
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Bibliography

[1] J. Guevara, “Review of particle size distribution analysis methods”, 2018. University of Florida Soil and Water Sciences Department. [Online], Available: https://soils.ifas.ufl.edu/media/soilsifasufledu/sws-mainsite/pdf/technical-papers/Guevara_Jorge_One_Year_Embargo.pdf [Accessed: 28.04.2021].
[2] S. Blott, K. Pye, “GRADISTAT: A grain size distribution and statistics package for the analysis of unconsolidated sediments”, Earth Surface Processes and Landforms, 2001, vol. 26, pp. 1237–1248, DOI: 10.1002/esp.261.
[3] P. Guilherme, C. Borzone, M. Bueno, M. Lamour, “Análise granulométrica de sedimentos de praias arenosas através de imagens digitais. Descrição de um protocolo de mensuração de partículas no software ImageJ – Fiji”, Brazilian Journal of Aquatic Sciences and Technology, 2015, vol. 19 (2), pp. 1–10, DOI: 10.14210/ bjast.v19n2.6874.
[4] H. Alkhaldi, C. Ergenzinger, F. Fleißner, P. Eberhard, “Comparison between two different mesh descriptions used for simulation of sieving processes”, Granular Matter, 2008, vol. 10, pp. 223–229, DOI: 10.1007/s10035-008-0084-4.
[5] J. Fernlund, R. Zimmerman, D. Kragic, “Influence of volume/mass on grain-size curves and conversion of image-analysis size to sieve size”, Engineering Geology, 2007, vol. 90, pp. 124–137, DOI: 10.1016/j.enggeo.2006.12.007.
[6] W. Weipeng, L. Jianli, Z. Bingzi, Z. Jiabao, L. Xiaopeng, Y. Yifan, “Critical Evaluation of Particle Size Distribution Models Using Soil Data Obtained with a Laser Diffraction Method”, PLoS ONE, 2015, vol. 10(4): e0125048, DOI: 10.1371/journal.pone.0125048.
[7] G.L. Santana, C.T. Brasileiro, G.A. Azeredo, H.C. Ferreira, G.A. Neves, H.S. Ferreira, “A comparative study of particle size distribution using analysis of variance for sedimentation and laser diffraction methods”, Cerâmica, 2019, vol. 65(375), pp. 452–460, DOI: 10.1590/0366-69132019653752623.
[8] S. Brandt, Data Analysis. Statistical and Computational Methods for Scientists and Engineers. Cham: Springer, 2014, ISBN 978-3-319-03761-5, DOI: 10.1007/978-3-319-03762-2.
[9] L. Opyrchał, “Applying the chi-modulus distribution to test the consistency of measurements”, Metrology and Measurement Systems, 1999, vol. 6, no. 3, pp. 135–142.
[10] A. Bak, R. Chmielewski, “The influence of fine fractions content in non-cohesive soils on their compactibility and the CBR value”, Journal of Civil Engineering and Management, 2019, vol. 25, no. 4, DOI: 10.3846/jcem.2019.9687.
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Authors and Affiliations

Leszek Opyrchał
1
ORCID: ORCID
Ryszard Chmielewski
1
ORCID: ORCID
Aleksandra Bąk
1
ORCID: ORCID

  1. Military University of Technology, Faculty of Civil Engineering and Geodesy, ul. gen. Sylwestra Kaliskiego 2, 00–908 Warsaw, Poland
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Abstract

Petroleum products influence the engineering behaviour of the soil. Neogene clays and glacial tills from Central Poland were tested under laboratory conditions to evaluate the changes of selected physical and mechanical parameters: particle size distribution, particle density, swelling, shear strength and permeability. Four petroleum products were used in the experiments: diesel fuel, kerosene, jet fuel and mineral engine oil. The study revealed that even for the lowest degree of contamination the values of physical and mechanical properties of the soils changed significantly. Greater variation can be expected in soils contaminated with high-viscosity compounds. Also, higher relative changes were found for glacial tills than for Neogene clays. Consolidation tests revealed changes in soil permeability depending on the soil composition and the physical properties of the contaminant – considerable reduction of permeability was observed for glacial tills contaminated with light Jet fuel, while the reduction was lower for Neogene clays. The obtained results indicate the role of mesopores and the dimensionless pore pressure coefficient in changes of soil permeability. The methodological issues regarding testing and analysing the hydrocarbon-contaminated soils were also presented and discussed, which might be useful for researchers studying contaminated soils.
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Authors and Affiliations

Paweł Dobak
1
Dorota Izdebska-Mucha
1
Piotr Stajszczak
1
Emilia Wójcik
1
Kamil Kiełbasiński
1
Ireneusz Gawriuczenkow
1
Tomasz Szczepański
1
Piotr Zbigniew Zawrzykraj
ORCID: ORCID
Anna Bąkowska
1
ORCID: ORCID

  1. University of Warsaw, Faculty of Geology, Department of Engineering Geology and Geomechanics, Żwirki i Wigury 93, 02-089 Warszawa, Poland

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