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Number of results: 10
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Abstract

In the article, the characterization of the microstructure, phase composition and distribution of elements in the Eu2O3-ZrO2 sintered materials obtained by four different ways of powders’ homogenization (mixing) process and different temperature of sintering process is shown. The feedstock powders with an average mole ratio of ZrO2 to Eu2O3 equal 74% to 26% were used as an initial material. The principal aim of the investigation was characterization of differences in the microstructure of the same type of ceramics, however, prepared via different mixing and manufacturing processes. The range of the investigation covered a characterization of these materials via phase identification of all samples by XRD (X-ray diffraction) and characterization of internal morphology of the specimens with detailed analysis of elements distributions by SEM (scanning electron microscopy) and EDS (energy dispersive spectrometry). The aim of the following investigation is to characterize the possibilities of the solid state synthesis of the europium zirconate based materials, dedicated for TBC applications.

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Authors and Affiliations

M. Mikuśkiewicz
G. Moskal
ORCID: ORCID
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Abstract

Worldwide commercial interest in the production of cerium doped yttrium aluminium garnet (YAG:Ce) phosphors is reflected in the widespread use of white light emitting devices. Despite of the fact that YAG:Ce is considered a “cool phosphor” it is the most important in white LED technology. This article reviews the developed techniques for producing phosphors with superior photoluminescence efficiency, including solid-state reaction, sol-gel and (co)precipitation methods. Also, by co-doping with rare earth elements, a red/blue shift is reached in the spectrum. The characteristics of YAG:Ce phosphors are investigated because the properties of the phosphors are strongly influenced by the synthesis routes and the sintering temperature treatment. After the phase analysis, morphology and emission studies of the phosphors there may be seen the conditions when the transition from the amorphous phase to the crystalline phase appears, when luminescent properties are influenced by the crystalline form, purity, average size of the particles, co-doping and so on.

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Authors and Affiliations

V. Tucureanu
A. Matei
A.M. Avram
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Abstract

The aim of these studies was to obtain single phase cubic modification of Li7La3Zr2O12 by mechanical milling and annealing of La(OH)3, Li2CO3 and ZrO2 powder mixture. Fritsch P5 planetary ball mill, Rigaku MiniFlex II X-ray diffractometer, Setaram TG-DSC 1500 analyser and FEI Titan 80-300 transmission electron microscope were used for sample preparation and investigations. The applied milling and annealing parameters allowed to obtain the significant contribution of c-Li7La3Zr2O12 in the sample structure, reaching 90%. Thermal measurements revealed more complex reactions requiring further studies.

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Authors and Affiliations

D. Oleszak
B. Kurowski
T. Pikula
M. Pawlyta
M. Senna
H. Suzuki
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Abstract

Al and Nb-doped Li7La3Zr2O12 (LLZO) and W-doped LLZO lithium ion conducting electrolyte samples were prepared and their H2O stability was investigated. The LLZO samples were exposed to 50% humidified air for 48 h. After H2O exposure, a cubic to tetragonal transformation occurred and acquired SEM images exhibited the presence of reaction phases at the grain boundaries of Al and Nb-LLZO. As a result, the lithium ion conductivity significantly decreased after H2O exposure. On the contrary, W-LLZO showed good stability against H2O. Although the cubic to tetragonal transformation was also observed in H2O-exposed W-LLZO, the decrease in lithium ion conductivity was found to be modest. No morphological changes of the W-LLZO samples were confirmed in the H2O-exposed W-LLZO samples.

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Authors and Affiliations

Eun-Jeong Yi
Keun-Young Yoon
Hyun-Ah Jung
Haejin Hwang
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Abstract

In this paper, explain the preparation of CaTiO3 ceramics synthesized by the solid-state reaction method. Calcium carbonate and titanium dioxide were high energy mixed in stoichiometric amounts, and the obtained mixture was calcined at different temperatures (800, 900, 1000 and 1300ºC) for 2 h. The obtained samples were characterized by measurement of particle size, Energy Dispersive X-Ray (EDX) Analysis; differential thermal analysis, X-ray diffraction and SEM images. XRD patterns indicated that CaTiO3 ceramics with the structure of perovskite is obtained from calcined powders at 1,300°C for 2 h. SEM images show the formation of a very fine and homogeneous morphology. The measured values of electrical resistivity were within the typical range of insulating materials and approach values corresponding to insulating ceramics.

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Authors and Affiliations

E. Rocha-Rangel
J. López-Hernández
J.A. Castillo-Martínez
J.J. Osorio-Ramos
C.A. Calles-Arriaga
I. Estrada-Guel
R. Martínez-Sánchez
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Abstract

An efficient operation of a Ho:YLF laser pumped by a Tm-doped fibre laser is reported. The research in a continuous-wave (CW) operation was done for two crystals of the same 0.5 at.%Ho dopant concentration and with different lengths (3×3×30 mm3 and 3×3×50 mm3). For an output coupling transmission of 20% and a crystal length of 50 mm, the maximum CWoutput power of 38.9 W for 81.4 W of incident pump power, corresponding to the slope efficiency of 52.3% and optical-to-optical conversion efficiency of 47.8% (determined with respect to the incident pump power) was achieved. The highest opti- cal-to-optical conversion efficiency of 70.2% with respect to the absorbed pump power was obtained. The influence of a heat-sink cooling water temperature on theCWlaser performance was studied. For a Q-switched operation the pulse repe- tition frequency (PRF) was changed from 2 to 10 kHz. The maximum average output power of 34.1 W at the PRF of 10 kHz was obtained for a 50 mm holmium crystal length. For 2 kHz PRF and 71.9 W of incident pump power, pulse energies of 13.7 mJ with a 21 ns FWHM pulse width corresponding to 652 kW peak power were recorded.

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Authors and Affiliations

J. Kwiatkowski
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Abstract

Replacing mathematical models with artificial intelligence tools can play an important role in numerical models. This paper analyses the modeling of the hardening process in terms of temperature, phase transformations in the solid state and stresses in the elastic-plastic range. Currently, the use of artificial intelligence tools is increasing, both to make greater generalizations and to reduce possible errors in the numerical simulation process. It is possible to replace the mathematical model of phase transformations in the solid state with an artificial neural network (ANN). Such a substitution requires an ANN network that converts time series (temperature curves) into shares of phase transformations with a small training error. With an insufficient training level of the network, significant differences in stress values will occur due to the existing couplings. Long-Short-Term Memory (LSTM) networks were chosen for the analysis. The paper compares the differences in stress levels with two coupled models using a macroscopic model based on CCT diagram analysis and using the Johnson-Mehl-Avrami-Kolmogorov (JMAK) and Koistinen-Marburger (KM) equations, against the model memorized by the LSTM network. In addition, two levels of network training accuracy were also compared. Considering the results obtained from the model based on LSTM networks, it can be concluded that it is possible to effectively replace the classical model in modeling the phenomena of the heat treatment process.
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Authors and Affiliations

Joanna Wróbel
1
Adam Kulawik
1
ORCID: ORCID

  1. Department of Computer Science, Czestochowa University of Technology, Dabrowskiego 73, 42-201 Czestochowa, Poland
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Abstract

Roman Micnas was a distinguished Polish physicist, well known for his works in the field of condensed matter theory and statistical physics. One of his best known achievements is development of theory of superconductivity with local electron pairing. He also published a number of important contributions to the theory of magnetism, theory of phase transitions, and theory of ultracold atoms on optical lattices. His more than 140 publications were cited over 3200 times by other authors. He graduated at the Faculty of Mathematics, Physics and Chemistry of Adam Mickiewicz University (AMU) in 1970, where he hold a position until his passing away on 13 January 2022. He received PhD in 1978, habilitation in 1988, and became Professor in 1990. In the Faculty of Physics of AMU he was the head of Solid State Theory Division in years 1998–2018. For his development of theory of superconductivity with local electron pairing he was awarded, together with Stanisław Robaszkiewicz, the Marie Skłodowska-Curie Scientific Prize of the Polish Academy of Sciences (PAS) in 1989. In 1994 he became Corresponding Member of PAS, and in 2016 – Ordinary Member. He served a number of important functions in PAS, among others he was a member of Committee for Physics of PAS, and since 2015 a Dean of Division III of Exact Sciences and Earth Sciences of PAS. He was a member of several scientific societies: Polish Physical Society, European Physical Society, American Physical Society and American Association for Advancement of Science. He co-organized 35 home and international conferences, among others the cycle of the European Conferences „Physics of Magnetism”, which he co-chaired since 1993.
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Authors and Affiliations

Tomasz Kostyrko
1
Marek Thomas
1

  1. Wydział Fizyki, Instytut Spintroniki i Informacji Kwantowej, Zakład Teorii Materii Skondensowanej, Uniwersytet im.Adama Mickiewicza
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Abstract

49th Winter School on Wave and Quantum Acoustics constituted platforms for sharing the results and achievements obtained in different branches of physical acoustics, as molecular acoustics, quantum acoustics, acousto-optics, magnetoacoustics, photoacoustics, acoustics of solid state, acoustic emission, and others. Moreover, researches in some selected topics related to those mentioned above (e.g. optoelectronics, relaxation processes) were presented during the school.

The conference consisted of the 16th Workshop on Acoustoelectronics and the 16th Workshop on Molecular Acoustics, Relaxation and Calorimetric Methods. However, the organizers are opened to organizing workshops on other subjects in future. We would like to invite scientific centers and other professional groups to cooperate in organizing workshops on the subjects of their interests.

XLVIIIth Winter School on Environmental Acoustics and Vibroacoustics was a forum for all environmental and vibroacoustics fields. Particularly it was concerned with traffic noise, vibroacoustics of machines, room acoustics, building acoustics, noise protection and similar problems. During the Conference, seminars on “Measurement of noise and vibration at the workplace” and Environmental noise monitoring”, combined with measurement workshops, were organised in association with SVANTEK.

The Conferences began with the special, joined session dedicated to celebration of the 15th Jubilee Conference Integrated Optics – Sensors, Sensing Structures and Methods. In summary, 48 people participated in Conferences and seminars, presenting 37 lectures, reports and posters. In this issue one can find abstracts of some lectures and posters, which were presented during the Conferences.

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Authors and Affiliations

Winter Schools on Acoustics

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