@ARTICLE{Izairi_N._Microhardness_2018, author={Izairi, N. and Ajredini, F. and Vevecka-Pfiftaj, A. and Makreski, P. and Ristova, M.M.}, volume={vol. 63}, number={No 3}, journal={Archives of Metallurgy and Materials}, pages={1101-1108}, howpublished={online}, year={2018}, publisher={Institute of Metallurgy and Materials Science of Polish Academy of Sciences}, publisher={Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences}, abstract={Equal-channel angular pressing (ECAP) was used as a technique for severe plastic deformation (SPD) on Al alloy AA3004. This technique produced fully dense materials of refined grain structure to sub-micrometer dimensions and advanced mechanical properties. The ECAP processing of samples was conducted as 1 to 4 passes through the die at room temperature. We present the results of the studied homogeneity evolution with the ECAP treatment. Furthermore, a Scanning Electron Microscope (SEM) was used for examination of the microstructure changes in samples undergone from 1 to 4 passes. The microhardness-HV increased upon each ECAP pass. The resulting micro-hardness evolution was attributed to crystalline microstructure modifications, such as the d-spacing (studied by X-ray Diffraction-XRD) depending on the number of ECAP pressings. The microcrystalline changes (grain refining evaluated from the Scanning Electron Microscopy – SEM images) were found to be related to the HV, following the Hall-Petch equation.}, type={Artykuły / Articles}, title={Microhardness Evolution in Relation to the Crystalline Microstructure of Aluminum Alloy AA3004}, URL={http://journals.pan.pl/Content/107985/AMM-2018-3-05-Izairi.pdf}, doi={10.24425/123782}, keywords={Al alloys, AA3004, Equal-channel angular pressing (ECAP), microhardness, SEM, grain size, XRD}, }