The magnetic properties of the U-type ferrite synthesized by a sol-gel process had studied by substituting cobalt with manganese or zinc in cobalt-based U-type ferrite. The substituted U-type ferrite showed a dominant crystal structure at a different substitution ratio of manganese and zinc. The change of the starting temperature of U-type ferrite formation according to substitutional elements was confirmed by TG-DTA analysis. In the case of manganese substitution, the starting temperature of U-type ferrite formation lowered, and on the contrary, when zinc was substituted, it became higher. The magnetic properties of the U-type ferrite substituted with manganese showed a tendency that the saturation magnetization was decreased and the coercivity was increased as the manganese ratio increased. The highest saturation magnetization was 57.9 emu/g in the specific composition (Ba4Co0.5Zn1.5Fe36O60) substituted with zinc.
Weld metal deposit (WMD) was carried out for standard MMA welding process. This welding method is still promising mainly due to the high amount of AF (acicular ferrite) and low amount of MAC (self-tempered martensite, retained austenite, carbide) phases in WMD. That structure corresponds with good impact toughness of welds at low temperature. Separate effect of these elements on the mechanical properties of welds is well known, but the combined effect of these alloy additions has not been analyzed so far. It was decided to check the total influence of nickel with a content between 1% to 3% and molybdenum with content from 0.1% up to 0.5%.
The U-type ferrite is a kind of hexagonal ferrite, and it is known as a microwave absorber in the X-band. The magnetic and dielectric loss of the U-type ferrite change to the composition and coating layer, etc. In this study, the silicon oxide layer was coated on the substituted U-type ferrites to improve microwave absorption characteristics. The complex permittivity and complex permeability were measured using toroidal specimens that were press-molded and the measured frequency range was set from 2-18 GHz. The improvement of the microwave absorption rate was different according to the type of the substituted U-type ferrites. Only in the substituted U-type ferrites with nickel and zinc, an improvement in the microwave absorption rate due to enhancement of magnetic loss was confirmed. The highest microwave absorption was 99.9% at 9.6 GHz, which was S_Z0.5U.
In this study, BaFe12-2xCoxTixO19 (X : 0 to 2.0, 0.2) powders were synthesized by sol-gel process. TG-DTA, XRD, SEM, VSM, and Network analyzer were measured in order to influence easy magnetization axis change on the wave absorption frequency range change. The easy magnetization axis change of the annealed powder at 900°C and 1200°C was confirmed by the coercive force decreased 4,800 and 3,870 Oe to 260 and 269 Oe, respectively, at the substitution ratio of 0.8 and 1.0. And it was confirmed that the change of the easy magnetization axis affected the change of the wave absorption frequency. The wave absorption frequency of substituted Barium Ferrite was less than 10 GHz range after the easy magnetization axis of Barium ferrite changed to a-b plan direction. It was confirmed the BaFe12-2xCoxTixO19(x = 0.8 to 1.6) was synthesized by the sol-gel process and it was annealed at 900°C and 1200°C, which could be used as a wave absorber in the X-band region of 10 GHz less.
A mathematical model of austenite - bainite transformation in austempered ductile cast iron has been presented. The model is based on a model developed by Bhadeshia [1, 2] for modelling the bainitic transformation in high-silicon steels with inhibited carbide precipitation. A computer program has been developed that calculates the incubation time, the transformation time at a preset temperature, the TTT diagram and carbon content in unreacted austenite as a function of temperature. Additionally, the program has been provided with a module calculating the free energy of austenite and ferrite as well as the maximum driving force of transformation. Model validation was based on the experimental research and literature data. Experimental studies included the determination of austenite grain size, plotting the TTT diagram and analysis of the effect of heat treatment parameters on the microstructure of ductile iron. The obtained results show a relatively good compatibility between the theoretical calculations and experimental studies. Using the developed program it was possible to examine the effect of austenite grain size on the rate of transformation.
The material selected for this investigation was low alloy steel weld metal deposit (WMD) after MAG welding with micro-jet cooling. The
present investigation was aimed as the following tasks: analyze impact toughness of WMD in terms of micro-jet cooling parameters. Weld
metal deposit (WMD) was first time carried out for MAG welding with micro-jet cooling of compressed air and gas mixture of argon and
air. Until that moment only argon, helium and nitrogen and its gas mixture were tested for micro-jet cooling
In paper is presented technology of bimetallic layered castings based on founding method of layer coating directly in cast proces so-called method of mould cavity preparation. Prepared castings consist two fundamental parts i.e. bearing part and working part (layer). The bearing part of bimetallic layered casting is typical foundry material i.e. ferritic-pearlitic unalloyed cast steel, whereas working part (layer) is plate of austenitic alloy steel sort X2CrNi 18-9. The ratio of thickness between bearing and working part is 8:1. The aim of paper was assessed the quality of the joint between bearing and working part in dependence of pouring temperature and carbon concentration in cast steel. The quality of the joint in bimetallic layered castings was evaluated on the basis of ultrasonic non-destructive testing, structure and microhardness researches.
In paper is presented technology of bimetallic layered castings based on founding method of layer coating directly in cast process so-called method of mould cavity preparation. Prepared castings consist two fundamental parts i.e. bearing part and working part (layer). The bearing part of bimetallic layered casting is typical foundry material i.e. unalloyed cast steel, whereas working part is plate of austenitic alloy steel sort X2CrNi 18-9. The ratio of thickness between bearing and working part is 8:1. The aim of paper was assessed the quality of the joint between bearing and working part in dependence of pouring temperature and carbon concentration in cast steel. The quality of the joint in bimetallic layered castings was evaluated on the basis of ultrasonic non-destructive testing, structure and microhardness researches.
U-type ferrite typified by Ba4Co2Fe36O60 is used as a RAM (Radar Absorbing Materials) in the X-band (8-12 GHz). Ba4Co2Fe36O60 is known to have a complex crystal structure, which makes it difficult to obtain single phase and have low reproducibility. Previously known U-type ferrites have been fabricated based on a ceramic process that mixing (by a ball mill), calcining, grinding, binder mixing, drying, sieving, pressing and sintering. In contrast, the process of preparing the powder by the sol-gel method and its heat-treating is advantageous in that it can reduce the process steps and the required time. In addition, the precise stoichiometric control by the sol-gel method can effectively evaluate the effect of added or substituted elements. In this study investigates the crystal structure of Ba4Co2Fe36O60 synthesized by the sol-gel method and the morphology of U-type ferrite nano-powders according to various heat treatment conditions. Analysis of the crystal structure is used for XRD. Morphology and size are observed by SEM. In addition, VSM is performed to confirm the change of magnetic properties according to various heat treatment conditions.
Repeated austenitisation and furnace cooling of homogenised 0.16 wt. % carbon steels result in ferrite grain sizes between 27 μm and 24 μm. Similarly, repeated austenitisation and normal-air cooling produces ferrite grain sizes between 17 μm and 12 μm; while repeated austenitisation and forced-air cooling produces a minimum grain size of 9.5 μm. Furnace cooling decomposes the austenite eutectoidally to lamellar pearlite; while normal-air cooling and forced-air cooling after austenitisation cause degeneration of pearlite regions producing grain boundary network as well as cluster of cementite and other carbides. Forced-air cooled samples provide the highest YS (364 MPa) and UTS (520 MPa); while furnace cooling provides the lowest (290 MPa and 464 MPa) leaving the normal-air cool performance in between. Hardness values depict the role of individual ferrite and pearlite content and the extent of pearlite degeneration occurring after each cyclic treatment.
In present work, two nuclear grade steel (P91, P92) are joined using the arc welding process. The welded joints were subjected to the heat treatment in order to restore the mechanical properties and overcome the heterogeneity across the joints. The weldments were studied for microstructure evolution and mechanical behavior under different condition of heat treatment. The variation in mechanical behavior obtained for the welded joints were tried to relate the microstructural evolution. After the normalizing based heat treatment, homogeneity with negligible δ ferrite across the welded joints was observed.
Pot-cored coils are commonly used as probes in eddy current testing. In this paper, an analytical model of such a coil placed over a three-layer plate with a hole has been presented. The proposed solution enables the modelling of both magnetic and non-magnetic conductive plates that contain different types of hole, i.e. a through, a surface, an inner or a subsurface hole. The problem was solved by using the truncated region eigenfunction expansion (TREE) method. The analysis was carried out in a cylindrical coordinate system in which the solution domain was radially limited. With the employment of the filamentary coil, the expressions for the magnetic vector potential, and subsequently for the impedance of the cylindrical coil were obtained. The final formulas were presented in a closed form and then implemented in Matlab. The resistance and reactance values were compared with the results obtained in the experiment and using the finite element method in the Comsol Multiphysics package. In each of the cases, good agreement was obtained.