The paper presents an investigation of mass transfer in gas-liquid annular flow in a microreactor. The microreactor had a meandered shape with a square cross-section of the channel (292×292 μm, hydraulic diameter 292 μm) and 250 mm in length. The rate of CO2 absorption from the CO2/N2 mixture in NaOH (0.1 M, 0.2 M, 0.7 M, 1.0 M and 1.5 M) water solutions was measured. Two velocities of gas flow and two velocities of liquid flow were used. In two cases a fully developed annular flow at the beginning of the channel was observed, whilst in two cases annular flow was formed only in about 2/3 of the microchannel length. Based on the measurements of CO2 absorption rate, the values of volumetric liquid - side mass transfer coefficients with the chemical reaction were determined. Then physical values of coefficients were found. Obtained results were discussed and their values were compared with the values predicted by literature correlations.

In the paper the experimental analysis of dryout in small diameter channels is presented. The investigations were carried out in vertical pipes of internal diameter equal to 1.15 mm and 2.3 mm. Low-boiling point fluids such as SES36 and R123 were examined. The modern experimental techniques were applied to record liquid film dryout on the wall, among the others the infrared camera. On the basis of experimental data an empirical correlation for predictions of critical heat flux was proposed. It shows a good agreement with experimental data within the error band of 30%. Additionally, a unique approach to liquid film dryout modeling in annular flow was presented. It led to the development of the three-equation model based on consideration of liquid mass balance in the film, a two-phase mixture in the core and gas. The results of experimental validation of the model exhibit improvement in comparison to other models from literature.