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Abstrakt

The microstructures and mechanical properties of T92 martensitic steel/Super304 austenitic steel weld joints with three welding consumables were investigated. Three types of welding materials ERNiCr-3, ERNiCrCoMo-1and T-304H were utilized to obtain dissimilar welds by using gas tungsten arc weld (GTAW). The results show that heat affect zone (HAZ) of T92 steel consists of coarse-grained and fine-grained tempered martensites. The microstructures of joints produced from ERNiCrCoMo-1 consist of equiaxed dendrite and columnar dendrite grains, which are more complicated than that of ERNiCr-3. In the tensile tests, joints constructed from ERNiCrCoMo-1 and T-304H met the ASME standard. The highest fracture energy was observed in specimens with the welding material ERNiCrCoMo-1. Ni content in weld seam of ERNiCrCoMo-1 was highest, which was above 40%. In conclusion, the nickel alloy ERNiCrCoMo-1 was the most suitable welding material for joints produced from T92 martensitic steel/Super304 austenitic steel.

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Autorzy i Afiliacje

Z. Liang
Y. Gui
Q. Zhao

Abstrakt

Textural properties and microstructures are commonly used properties in the analysis of Pleistocene and older glacial deposits. However, contemporary glacial deposits are seldom studied, particularly in the context of post-depositional changes. This paper presents the results of a micromorphological study of recently deposited tills in the marginal zones of Hansbreen and Torellbreen, glaciers in southwestern Spitsbergen. The main objectives of this study were to compare modern tills deposited in subglacial and supraglacial conditions, as well as tills that were freshly released from ice with those laid down several decades ago. The investigated tills are primarily composed of large clasts of metamorphic rocks and represent coarse-grained, matrix-supported diamictons. The tills reveal several characteristic features for ductile (e.g. turbate structures) and brittle (e.g. lineations, microshears) deformations, which have been considered to be indicative of subglacial conditions. In supraglacial tills, the same structures are common as in the subglacial deposits, which points to the preservation of the primary features, though the sediment was transferred up to the glacier surface due to basal ice layer deformation and redeposited as slumps, or to formation of similar structures due to short-distance sediment re-deposition by mass flows. This study revealed that it might not be possible to distinguish subglacial and supraglacial tills on the basis of micromorphology if the latter are derived from a subglacial position. The only noted difference was the presence of iron oxide cementation zones and carbonate dissolution features in supraglacial tills. These features were found in tills that were deposited at least a few years ago and are interpreted to be induced by early post-depositional processes involving porewater/sediment interactions.
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Autorzy i Afiliacje

Grzegorz Rachlewicz
Katarzyna Skolasińska
Witold Szczuciński

Abstrakt

The results presented in this article are part of the research on fatigue life of various foundry alloys carried out in recent years in the Lukasiewicz Research Network – Institute of Precision Mechanics and AGH University of Science and Technology, Faculty of Foundry Engineering. The article discusses the test results obtained for the EN-GJS-600-3 cast iron in an original modified low-cycle fatigue test (MLCF), which seems to be a beneficial research tool allowing its users to evaluate the mechanical properties of materials with microstructural heterogeneities under both static and dynamic loads. For a comprehensive analysis of the mechanical behaviour with a focus on fatigue life of alloys, an original modified low cycle fatigue method (MLCF) adapted to the actually available test machine was used. The results of metallographic examinations carried out by light microscopy were also presented. From the analysis of the results of the conducted mechanical tests and structural examinations it follows that the MLCF method is fully applicable in a quick and economically justified assessment of the quality of ductile iron after normalizing treatment.

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Autorzy i Afiliacje

M. Maj
K. Pietrzak
A. Klasik

Abstrakt

In this study, Strontium Bismuth Niobate (SrBi2-xTmxNb2O9 with 0 ≤ x ≤ 0.1) doped by Tm was synthesized using by the hydrothermal method. The microstructure and electrical properties were mainly investigated. XRD analysis showed a single-phase orthorhombic structure for Tm-doped SrBi2Nb2O9 samples. The crystallite size is anisotropic and the strain is apparently independent of Tm amount. Dielectric properties for doped SrBi2Nb2O9 with Tm3+ ion have the same trend discussed for the pure sample. FTIR resulats showed that NbO6 octahedral is formed, on one hand, and on the other hand, it shows that spectras for doped and undoped samples are nearly the same. The Cross-section of ceramics showed the plate-like morphology, also the distribution of the pore in ceramics are observed for all samples. Tm dopants produce only minor changes in the impendence parameter values at room temperature. The luminescent (PL) properties of Tm-doped SrBi2Nb2O9 ceramic powders were investigated. The optimum Tm3+ concentration for the maximum PL intensity was found to be at x = 0.075.
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Autorzy i Afiliacje

Mohamed Afqir
1
ORCID: ORCID
Stevan Stojadinović
2
ORCID: ORCID
Mohamed Elaatmani
1
ORCID: ORCID
Abdelouahad Zegzouti
1
ORCID: ORCID
Nabiha Tahiri
1
Mohamed Daoud
1
ORCID: ORCID

  1. Université Cadi Ayyad, Faculté des Sciences Semlalia, Laboratoire des Sciences des Matériaux et Optimisation des Procédés, Marrakech, Morocco
  2. University of Belgrade, Faculty of Physics, Studentskitrg 12-16, Belgrade, Serbia

Abstrakt

The phase transformation dynamic and electrical conductivity equations of the aged Cu-2.7Ti-2.5Ni-0.8V alloy were established in this work. The microstructure evolution and precipitated phases were characterized by scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The mechanical properties were tested using a hardness testing machine and universal test machine, and the electrical conductivity was measured by the eddy conductivity gauge. The results show that NiTi intermetallic compounds are formed during the solidification, and these phases such as Ni3Ti and NiV3 are precipitated after aging treatment. The fracture morphology displays that a large number of shallow and equiaxed dimples occur on the tensile fracture, indicating a typical ductile fracture. After aging treatment at 450°C for 240 min, the hardness, tensile strength, elongation and electrical conductivity of the Cu-2.7Ti-2.5Ni-0.8V alloy are 184 HV, 459 MPa, 6.3% and 28.72% IACS, respectively.
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Autorzy i Afiliacje

Jia Liu
1 2
ORCID: ORCID
Jituo Liu
3
ORCID: ORCID
Xianhui Wang
3
ORCID: ORCID

  1. Xi’an Polytechnic University, School of Materials Science and Engineering, Xi’an 710048, P.R. China
  2. Xi’an University of Technology, School of Mechanical and Precision Instrument Engineering, Xi’an 710048, P. R. China
  3. Xi’an University of Technology, School of Materials Science and Engineering, Xi’an 710048, P. R. China

Abstrakt

The paper presents research results on the selection of parameters for the asymmetric rolling process of bimetallic plates 10CrMo9-10 + X2CrNiMo17-12-2. They consisted in determining the optimum parameters of the process, which would be ensured to obtain straight bands. Such deformation method introduces in the band the deformations resulting from shear stress, which affect changes in the microstructure. But their effect on the structure is more complicated than in the case of homogeneous materials. It has been shown that the introduction of asymmetric conditions into the rolling process results in greater grain refinement in the so-called hard layer. There was no negative effect on the structural changes in the soft layer observed.

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Autorzy i Afiliacje

D. Rydz
ORCID: ORCID
B. Koczurkiewicz
G. Stradomski
T. Garstka
J. Wypart

Abstrakt

The paper deals with the possibilities of influencing the final microstructure of aluminium alloy castings by changing the external conditions of crystallization and solidification. Aluminum alloys, especially Al-Si alloys, are nowadays one of the most used non-ferrous metal alloys, especially due to their mass application in the automotive field. It is in this industry that extreme emphasis is placed on the quality of cast parts with regard to safety. For this reason, a key production parameter is the mastery of the control of the resulting microstructure of the castings and the associated internal quality, which is subject to high demands defined by international standards. The aim of the experiment of this paper is to evaluate the effect of different preheating of the metal mould on the resulting structure and hardness of test castings made of AlSi7Mg0.3 material. The hardness measurement will be evaluated on a hardness tester. The parameter SDAS, Microporosity, Content of excluded eutectic will be evaluated. Dependencies will be found and plotted.
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Autorzy i Afiliacje

F. Radkovský
1
ORCID: ORCID
M. Gawronová
1
ORCID: ORCID
I. Kroupová
1
ORCID: ORCID

  1. VSB - Technical University of Ostrava, Czech Republic
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Abstrakt

Iron aluminides are iron-aluminum alloys that have excellent resistance to oxidation at high temperatures with low density, high resistance/weight ratio and a low manufacturing cost. Due to its characteristics, these alloys are presented as an option to replace stainless steels in certain applications. This works intends report the casting process and subsequent analyses involving microstructure, mechanical properties, and corrosion resistance of two Fe-Al-C alloys (Fe-11wt%Al and Fe-25wt%Al, containing 0.31-0.37%C), which were prepared in an induction furnace and poured in a permanent mold. Samples of these alloys were characterized and presented elevated hardness values of 37 HRC (alloy Fe-11wt%Al) and 49.6HRC (alloy Fe-25wt%Al) and microstructure with aluminides type Fe3Al and FeAl and also carbides type K. The Fe-11wt%Al alloy exhibited superior resistance to uniform corrosion, although both Fe-Al-C alloys exhibited significantly higher corrosion rates compared to a binary iron aluminide in 0.5M H2SO4 containing naturally dissolved oxygen.
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Bibliografia

[1] Zamanzade, M., Barnoush, A. & Motz, C. (2016). A review on the properties of iron aluminide intermetallics. Crystals. 6(10), 1-29. DOI: 10.3390/cryst6010010.
[2] Stoloff, N.S. (1998). Iron aluminides: present status and future prospects. Materials Science and Engineering: A. 258(1-2), 1-14. DOI: 10.1016/S0921-5093(98)00909-5.
[3] Cinca, N., Lima, C.R.C. & Guilemany, J.M. (2013). An overview of intermetallics research and application: Status of thermal spray coatings. Journal of Materials Research and Technology. 2(1), 75-86. DOI: 10.1016/j.jmrt.2013.03.013.
[4] Palm, M., Stein, F. & Dehm, G. (2019). Iron Aluminides. Annual Review of Materials Research. 49, 297-326. DOI: 10.1146/annurev-matsci-070218-125911.
[5] Deevi, S.C. & Sikka, V.K. (1996). Nickel and iron aluminides: an overview on properties, processing, and applications. Intermetallics. 4(5) 357-375. DOI: 10.1016/0966-9795(95)00056-9.
[6] Shankar Rao, V., Baligidad, R. G. & Raja, V. S. (2002). Effect of carbon on corrosion behaviour of Fe3Al intermetallics in 0.5N sulphuric acid. Corrosion Science. 44, 521-533. DOI: 10.1016/S0010-938X(01)00084-1.
[7] Shankar Rao, V. (2005). Repassivation behaviour and surface analysis of Fe3Al based iron aluminide in 0.25M H2SO4. Corrosion Science. 47, 183-194. DOI: 10.1016/j.corsci.2004.05.014.
[8] Nigam, A.K., Balasubramaniam, R., Bhargava, S. & Baligidad, R.G. (2006). Electrochemical impedance spectroscopy and cyclic voltammetry study of carbon-alloyed iron aluminides in sulfuric acid. Corrosion Science. 48(7), 1666-1678. DOI: 10.1016/j.corsci.2010.05.006.
[9] Schneider, A., Falat, L., Sauthoff, G. & Frommeyer, G. (2005). Microstructures and mechanical properties of Fe3Al-based Fe-Al-C alloys. Intermetallics. 13(12), 1322-1331. DOI: 10.1016/j.intermet.2005.01.0.
[10] Brito, P., Pinto, H., Klaus, M., Genzel, C. & Kaysser-Pyzalla, A. (2010). Internal stresses and textures of nanostructured alumina scales growing on polycrystalline Fe3Al alloy. Powder Diffraction. 25(2), 114-118. DOI: 10.1154/1.3402764
[11] Brito, P., Schuller, E., Silva, J., Campos, T.R., Araújo, C.R. & Carneiro, J.R. (2017). Electrochemical corrosion behaviour of (100), (110) and (111) Fe3Al single crystals in sulphuric acid. Corrosion Science. 126, 366-373. DOI: 10.1016/j.corsci.2017.05.029.
[12] Brito, P.P., Carvalho Filho, C.T. & Oliveira, G.A. (2020). Electrochemical corrosion behavior of iron aluminides in sulfuric acid. Materials Science Forum. 1012, 395-400. DOI: 10.4028/www.scientific.net/MSF.1012.395.
[13] Hernández-Hernández, M., Liu, H. B., Alvarez-Ramirez, J. & Espinosa-Medina, M. A. (2017). Corrosion behavior of Fe-40at.%Al-Based intermetallic in 0.25M H2SO4 solution. Journal of Materials Engineering and Performance. 26, 5983-5996. DOI: 10.1007/s11665-017-3036-5.

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Autorzy i Afiliacje

A.P. Silva
1
ORCID: ORCID
P.P. Brito
1
N. Martins
1

  1. PUC Minas, Brazil

Abstrakt

The study presented in this paper concerned the possibility to apply a heat treatment process to ductile cast-iron thin-walled castings in order to remove excessive quantities of pearlite and eutectic cementite precipitates and thus meet the customer’s requirements. After determining the rates of heating a casting up to and cooling down from 900°C feasible in the used production heat treatment furnace (vh = 300°C/h and vc = 200°C/h, respectively), dilatometric tests were carried out to evaluate temperatures Tgr, TAc1start, TAc1end, TAr1start, and TAr1end. The newly acquired knowledge was the base on which conditions for a single-step ferritizing heat treatment securing disintegration of pearlite were developed as well as those of a two-step ferritization process guaranteeing complete disintegration of cementite and arriving at the required ferrite and pearlite content. A purely ferritic matrix and hardness of 119 HB was secured by the treatment scheme: 920°C for 2 hours / vc = 60°C/h / 720°C for 4 hours. A matrix containing 20–45% of pearlite and hardness of 180–182 HB was obtained by applying: 920°C for 2 hours or 4 hours / vc = 200°C/h to 650°C / ambient air.

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Autorzy i Afiliacje

Marek Mróz
ORCID: ORCID
A.W. Orłowicz
ORCID: ORCID
M. Tupaj
ORCID: ORCID
B. Kupiec
M. Kawiński

Abstrakt

The paper presents the results of microstructural and mechanical investigation of long-term aged TP347HFG austenitic stainless steel. Ageing was performed at a time of up to 30 000 hours and the temperature of 600 and 650◦C. Ageing was proved to lead to the precipitation of secondary phase particles not only inside grains but also on the boundaries of grains and twins. The MX precipitates were observed inside the grains. However, M23C6 carbides and sigma phase precipitates were observed on grain boundaries. The changes in the microstructure of the examined steel translated into the mechanical properties, i.e. initially observed growth and then the decrease of yield strength and a gradual decrease in impact energy. The overageing process – a decrease in strength properties – was associated with the growth of the size of M23C6 carbides and the precipitation of the sigma phase. The reduction of impact energy in TP347HFG austenitic stainless steel was found to be associated with the precipitation of M23C6 carbides in the case of the 600◦C temperature, and the M23C6 carbides and sigma phase in the case of the 650◦C temperature. The rate of changes in the microstructure and mechanical properties depended on the ageing temperature.
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Autorzy i Afiliacje

Grzegorz Golański
1
ORCID: ORCID
Hanna Purzyńska
2

  1. Czestochowa University of Technology, Department of Materials Science, Armii Krajowej 19, 42-200 Częstochowa, Poland
  2. Łukasiewicz Research Network – Institute for Ferrous Metallurgy, K. Miarki 12-14, 44-100 Gliwice, Poland
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Abstrakt

This research investigates the microstructural evolution and mechanical properties of LM25 (Al-Si-Mg) alloy and Cr-modified LM25-Cr (Al-Si-Mg-Cr) alloy. Microstructural analysis reveals distinctive ε-Si phase morphologies, with Cr addition refining dendritic structures and reducing secondary dendrite arm spacing in the as-cast condition. Cr modification results in smaller-sized grains and a modified ε-Si phase, enhancing nucleation sites and reducing ε-Si size. Microhardness studies demonstrate significant increases in hardness for both alloys after solutionising and aging treatments. Cr-enriched alloy exhibits superior hardness due to solid solution strengthening, and prolonged aging further influences ε-Si particle size and distribution. The concurrent rise in microhardness, attributed to refined dendritic structures and unique ε-Si morphology, underscores the crucial role of Cr modification in tailoring the mechanical properties of aluminium alloys for specific applications.
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Bibliografia

[1] Gustafsson, G., Thorvaldsson, T. & Dunlop, G. L. (1986). The influence of Fe and Cr on the microstructure of cast Al-Si-Mg alloys. Metallurgical Transactions A. 17(1), 45-52. https://doi.org/10.1007/bf02644441.

[2] Liang, C., Zhao, J. F., Chang, J. & Wang, H. P. (2020). Microstructure evolution and nano-hardness modulation of rapidly solidified Ti–Al–Nb alloy. Journal of Alloys and Compounds. 836, 155538, 1-11. https://doi.org/10.1016/j.jallcom.2020.155538.

[3] Tsepeleva, A., Novák, P., Vlášek, J. & Simoniakin, A. (2023). Use of rapid solidification in processing of aluminum alloys with reduced deep-sea nodules. Journal of Alloys and Compounds. 968, 171790, 1-9. https://doi.org/10.1016/j.jallcom.2023.171790.

[4] Ahmad, R. (2018). The effect of chromium addition on fluidity, microstructure and mechanical properties of aluminium LM6 cast alloy. International Journal of Material Science and Research. 1(1), 32-35. https://doi.org/10.18689/ijmsr-1000105.

[5] Zhang, G.-H., Zhang, J.-X., Li, B.-C. & Cai, W. (2011). Characterization of tensile fracture in heavily alloyed Al-Si piston alloy. Progress in Natural Science: Materials International. 21(5), 380-385. https://doi.org/10.1016/s1002-0071(12)60073-2.

[6] Barnes, S.J. & Lades, K. (2002). The evolution of aluminium based piston alloys for direct injection diesel engines. SAE Technical Paper Series.

[7] Cole, G.S. & Sherman, A.M. (1995). Light weight materials for automotive applications. Materials Characterization. 35(1), 3-9. https://doi.org/10.1016/1044-5803(95)00063-1.

[8] Strobel, K., Easton, M.A., Sweet, L., Couper, M.J., & Nie, J.-F. (2011). Relating quench sensitivity to microstructure in 6000 series aluminium alloys. Materials Transactions. 52(5), 914-919. https://doi.org/10.2320/matertrans.l-mz201111.

[9] Yang, Y., Zhong, S.-Y., Chen, Z., Wang, M., Ma, N. & Wang, H. (2015). Effect of Cr content and heat-treatment on the high temperature strength of eutectic Al–Si alloys. Journal of Alloys and Compounds. 647, 63-69. https://doi.org/10.1016/j.jallcom.2015.05.167.

[10] Lodgaard, L. & Ryum, N. (2000). Precipitation of dispersoids containing Mn and/or Cr in Al–Mg–Si alloys. Materials Science & Engineering. A. 283(1-2), 144-152. https://doi.org/10.1016/s0921-5093(00)00734-6.

[11] Tocci, M., Pola, A., Angella, G., Donnini, R. & Vecchia, G. M.L. (2019). Dispersion hardening of an AlSi3Mg alloy with Cr and Mn addition. Materials Today: Proceedings. 10, 319-326. https://doi.org/10.1016/j.matpr.2018.10.412.

[12] Kim, H.Y., Han, S.W. & Lee, H.M. (2006). The influence of Mn and Cr on the tensile properties of A356–0.20Fe alloy. Materials Letters. 60(15), 1880-1883. https://doi.org/10.1016/j.matlet.2005.12.042.

[13] Fu, Y., Wang, G.G., Hu, A., Li, Y., Thacker, K.B., Weiler, J.P. & Hu, H. (2022). Formation, characteristics and control of sludge in Al-containing magnesium alloys: An overview. Journal of Magnesium and Alloys. 10(3), 599-613. https://doi.org/10.1016/j.jma.2021.11.031.

[14] Yamamoto, K., Takahashi, M., Kamikubo, Y., Sugiura, Y., Iwasawa, S., Nakata, T. & Kamado, S. (2020). Influence of process conditions on microstructures and mechanical properties of T5-treated 357 aluminum alloys. Journal of Alloys and Compounds. 834, 155133, 1-13. https://doi.org/10.1016/j.jallcom.2020.155133.

[15] Callegari, B., Lima, T.N. & Coelho, R.S. (2023). The influence of alloying elements on the microstructure and properties of Al-Si-based casting alloys: A review. Metals, 13(7), 1174, 1-36. https://doi.org/10.3390/met13071174.

[16] Silva, M.S., Barbosa, C., Acselrad, O. et al. (2004). Effect of chemical composition variation on microstructure and mechanical properties of a 6060 aluminum alloy. Journal of Materials Engineering and Performance. 13, 129-134. https://doi.org/10.1361/10599490418307.

[17] Xiao, L., Yu, H., Qin, Y., Liu, G., Peng, Z., Tu, X., Su, H., Xiao, Y., Zhong, Q., Wang, S., Cai, Z. & Zhao, X. (2023). Microstructure and mechanical properties of cast Al-Si-Cu-Mg-Ni-Cr alloys: Effects of time and temperature on two-stage solution treatment and ageing. Materials. 16(7), 2675, 1-16. https://doi.org/10.3390/ma16072675.

[18] Li, Y., Yang, Y., Wu, Y., Wei, Z. & Liu, X. (2011). Supportive strengthening role of Cr-rich phase on Al–Si multicomponent piston alloy at elevated temperature. Materials Science & Engineering. A. 528(13-14), 4427-4430. https://doi.org/10.1016/j.msea.2011.02.047.

[19] Tocci, M., Donnini, R., Angella, G. & Pola, A. (2017). Effect of Cr and Mn addition and heat treatment on AlSi3Mg casting alloy. Materials Characterization. 123, 75-82. https://doi.org/10.1016/j.matchar.2016.11.022.

[20] Engler, O. & Miller-Jupp, S. (2016). Control of second-phase particles in the Al-Mg-Mn alloy AA 5083. Journal of Alloys and Compounds. 689, 998-1010. https://doi.org/10.1016/j.jallcom.2016.08.070.

[21] Liu, F.-Z., Qin, J., Li, Z., Yu, C.-B., Zhu, X., Nagaumi, H. & Zhang, B. (2021). Precipitation of dispersoids in Al–Mg–Si alloys with Cu addition. Journal of Materials Research and Technology. 14, 3134-3139. https://doi.org/10.1016/j.jmrt.2021.08.123.

[22] Cui, J., Chen, J., Li, Y. & Luo, T. (2023). Enhancing the strength and toughness of A356.2-0.15Fe aluminum alloy by trace Mn and Mg Co-addition. Metals. 13(8), 1451, 1-12. https://doi.org/10.3390/met13081451.

[23] Zhan, H. & Hu, B. (2018). Analyzing the microstructural evolution and hardening response of an Al-Si-Mg casting alloy with Cr addition. Materials Characterization. 142, 602-612. https://doi.org/10.1016/j.matchar.2018.06.026.

[24] Tocci, M., Donnini, R., Angella, G. et al. (2019). Tensile Properties of a Cast Al-Si-Mg Alloy with Reduced Si Content and Cr Addition at High Temperature. Journal of Materials Engineering and Performance. 28, 7097-7108. https://doi.org/10.1007/s11665-019-04438-9.

[25] Kumar, A., Sharma, G., Sasikumar, C., Shamim, S. & Singh, H. (2015). Effect of Cr on grain refinement and mechanical properties of Al-Si-Mg alloys. Applied Mechanics and Materials. 789-790, 95-99. https://doi.org/10.4028/www.scientific.net/amm.789-790.95.

[26] Möller, H., Stumpf, W.E. & Pistorius, P.C. (2010). Influence of elevated Fe, Ni and Cr levels on tensile properties of SSM-HPDC Al-Si-Mg alloy F357. Transactions of the Nonferrous Metals Society of China. 20, 842-846. https://doi.org/10.1016/s1003-6326(10)60592-4.

[27] Raj, A.N. & Sellamuthu, R. (2016). Determination of hardness, mechanical and wear properties of cast Al–Mg–Si alloy with varying Ni addition. ARPN Journaol of Engineering and Applied Science. 11(9), 5946-5952.

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Autorzy i Afiliacje

V.V. Ramalingam
1
K.V. Shankar
2
B. Shankar
2
R. Abhinandan
3
A. Dineshkumar
3
P.A. Adhithyan
3
K. Velusamy
3
A. Kapilan
3
N. Sudheer
3

  1. Department of Mechanical Engineering, Amrita School of Engineering, Amrita Vishwa Vidyapeetham, Coimbatore, 64112, India
  2. Department of Mechanical Engineering, Amrita Vishwa Vidyapeetham, Amritapuri, India; Centre for Flexible Electronics and Advanced Marerials, Amrita Vishwa Vidyapeetham, Amritapuri, India
  3. Department of Mechanical Engineering, Amrita Vishwa Vidyapeetham, Amritapuri, India

Abstrakt

In this study, the effect of calcium treatment on the mechanical properties and fatigue behavior of low carbon steel material is investigated. By applying calcium treatment after aluminum deoxidation for steel cleanliness, the aim is to transform the inclusions into harmless structures and produce cleaner liquid steel. As a result of the study, calcium treated material’s tensile strength slightly increases while fatigue life decreases. SEM studies were conducted to evaluate the results and it was observed that while elongated inclusions were observed as well as spherical shapes in the untreated sample, the inclusions generally had a spherical shape in the calcium treated sample. After the steel cleanliness process, the mechanical properties of the samples were improved. The tensile strength of the calcium treated sample increased slightly. However, a significant decrease in fatigue strength was observed depending on brittle inclusions that occur as a result of the calcium treatment process.
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Autorzy i Afiliacje

Barış Karabayrak
1
ORCID: ORCID
Sinem Baskut
2
ORCID: ORCID
Dilek Turan
1
ORCID: ORCID

  1. Eskisehir Technical University, Faculty of Aeronautics and Astronautics, Department of Airframe and Power Plant Maintenance, Eskisehir, Turkey
  2. Eskisehir Technical University, Faculty of Engineering, Department of Materials Science and Engineering, Eskisehir, Turkey

Abstrakt

In this study, the effects of heat-treatment conditions of Fe powder compacts on densification, microstructure, strength and magnetic properties were investigated. The prepared Fe powder was compressed in a mold of diameter 20 mm at a pressure of 800 MPa for 30 sec. This Fe powder compact was heat-treated under different atmospheres (air and 90% Ar + 10% H2 and heat-treatment temperatures (300 and 700℃). The Fe powder compacts heat-treated in an Ar+H2 mixed gas atmosphere showed a denser microstructure and higher density than the Fe powder compacts heat-treated in an air atmosphere. Oxygen content in the heat-treatment conditions played a significant role in the improvement of the densification and magnetic properties.
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Autorzy i Afiliacje

Hyo-Sang Yoo
1
ORCID: ORCID
Yong-Ho Kim
1
ORCID: ORCID
Cheol-Woo Kim
1
ORCID: ORCID
Hyeon-Taek Son
1
ORCID: ORCID

  1. Korea Institute of Industrial Technology, Automotive Materials & Components R&D Group, 1110-9 Oryong-dong, Buk-gu, Gwangju 61012, Republic of Korea

Abstrakt

Effect of annealing treatment on deep drawing behavior of hot-rolled Q235 carbon steel/410/304 stainless steel three-layer composite plate was investigated. Deep drawability of the unannealed composite plates exhibits a sharp difference for various contact surfaces with the die. The limit drawing ratio (LDR) of the composite plate with the carbon steel contacting the die is 1.75, while it is 1.83 with the stainless steel contacting the die due to the different mechanical responses to the tensile stress at the corner of the die. After annealing at 900°C for 2 h, however, the deep drawabilities of the composite plates both for various contact surfaces with the die are significantly improved and becomes almost identical, which are attributed to the stress relief, the enhanced ductility and the improved interface bonding strength of the hot-rolled component plates during annealing.
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Autorzy i Afiliacje

Zehua Lv
1 2 3
Zhixiong Zhang
1 2 3
Jianchao Han
1 2 3
Tao Wang
1 2 3
ORCID: ORCID

  1. Taiyuan University of Technology, College of Mechanical and Vehicle Engineering, Taiyuan 030024, PR China
  2. Taiyuan University of Technology, Engineering Research Center of Advanced Metal Composites Forming Technology and Equipment, Ministry of Education, Taiyuan 030024, PR China
  3. Taiyuan University of Technology, Tyut-Uow Joint Research Centre, Taiyuan 030024, PR China

Abstrakt

The purpose of the research was to examine the influence of boron on the selected properties of low-alloy cast steels. The chemical compositions of the cast steels were designed especially for this study to contain different alloy elements. The first composition lacked significant alloying elements. The subsequent grades of cast steels had the addition of chrome, chrome with vanadium, and chrome with titanium. It was decided to investigate the influence of boron in the presence of such alloying additives on the temperature of phase transformations. On the basis of dilatometric curves, the characteristic temperatures of the phase transformations were determined. Additionally, to assess the influence of the cooling rate on the structure of cast steels, an analysis of their microstructure, after full annealing and quenching, was carried out.
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Autorzy i Afiliacje

B. Białobrzeska
1
ORCID: ORCID
R. Dziurka
2
ORCID: ORCID

  1. Wroclaw University of Science and Technology, Department of Vehicle Engineering, Smoluchowskiego Str. 25, 50-370 Wroclaw, Poland
  2. University of Science and Technology, Faculty of Metals Engineering and Industrial Computer Sciences, Al. A. Mickiewicza 30, 30-059 Krakow, Poland

Abstrakt

The surfacing layer of cobalt-based alloy is prepared using the tungsten inert gas welding (TIG) process and employing the UMCo50, ST1 and ST6 filler materials. The metallographic testing, hardness, wear and corrosion testing of different surfacing layers have been carried out. Each area of the surfacing layer is characterized using the optical and scanning electron microscope (SEM). Cellular and a few columnar dendrites have been observed near the fusion line of the UMCo50 surfacing layer, and cellular structure is observed in the central region. Dendrites and cellular crystals have been observed in the ST1 and ST6 surfacing layers. The average hardness of UMCo50, ST1 and ST6 surfacing layers are 320 HV, 672.3 HV and 497.5 HV, respectively. The wear loss of the ST1, ST6 and UMCo50 surfacing layer is 2.71 mg, 4.35 mg, and 14.57 mg, respectively. The corrosion weight loss of the ST1, ST6 and UMCo50 surfacing layers are 0.0388 g, 0.0477 g and 0.0833 g, respectively.
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Autorzy i Afiliacje

Haitao Xue
1
ORCID: ORCID
Xiaoping Luan
1
ORCID: ORCID
Weibing Guo
1
ORCID: ORCID
Dong Zhou
1
ORCID: ORCID

  1. Hebei University of Technology, School of Materials Science and Engineering, No. 5340, Xipingdao Road, Beichen District, Tianjin, 300401, PR China

Abstrakt

In this study, we have developed Sn-Ag alloy by a simple high energy ball milling technique. We have ball-milled the eutectic mixture of Sn and Ag powders for a period of 45 h. The milled powder for 45 h was characterized for particle size and morphology. Microstructural investigations were carried out by scanning electron microscopy and X-ray diffraction studies. The melting behavior of 45 h milled powder was studied by differential scanning calorimetry. The resultant crystallite size of the Sn(Ag) solid solution was found to be 85 nm. The melting point of the powder was 213.6oC after 45 h of milling showing depression of ≈6oC in melting point as compared to the existing Sn-3.5Ag alloys. It was also reported that the wettability of the Sn-3.5Ag powder was significantly improved with an increase in milling time up to 45 h due to the nanocrystalline structure of the milled powder.

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Autorzy i Afiliacje

Ashutosh Sharma
ORCID: ORCID
Byungmin Ahn
ORCID: ORCID

Abstrakt

In this paper, we have studied the evolution of morphology and brazing behavior of Ag-28Cu alloy filler processed by high energy ball milling. The milling of the powder mixture was carried out for 40 h. The structural and morphological analyses were performed by the X-ray diffraction and scanning electron microscopy. The melting temperature of the braze filler was determined by differential thermal analysis. The filler wetting properties were assessed from the spread area ratio measurements on various Ti substrates. The results indicate that the ball milling can effectively depress the filler melting point and enhance the brazeability. The milled powder mixture showed Ag(Cu) solid solution with a crystallite size of 174-68 nm after 40 h. It was shown that the high energy ball milling can be a potential method to develop low temperature brazing fillers for advanced microjoining applications.

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Autorzy i Afiliacje

Ashutosh Sharma
ORCID: ORCID
Myoung Jin Chae
Byungmin Ahn
ORCID: ORCID

Abstrakt

The presented access the influence of Mn content (0-0.94 wt.%) on the course of the cooling curves, phase transformation, macrostructure, and microstructure of Al-Cu alloys for three series: initial (Series I), with the addition of an AlTi master (Series II), and modified with AlTi5B1 (Series III). The maximum degree of undercooling ΔT was determined based on the cooling curves. The surface density of the grains (NA) was determined and associated with the inverse of solidification interval 1/ΔTk. Titanium (contained in the charge materials as well as the modifier) has a significant effect on the grinding of the primary grains in the tested alloys. A DSC thermal analysis allowed for the determination of phase transition temperatures under conditions close to equilibrium. For series II and III, the number of grains decreases above 0.2 wt.% Mn with a simultaneous increase in solidification interval 1/ΔTk. The presence of Al2Cu eutectics as well as the Cu-, Fe-, and Mn-containing phases in the examined samples was demonstrated using scanning electron microscopy.

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Autorzy i Afiliacje

S. Stąpór
M. Górny
M. Kawalec
B. Gracz

Abstrakt

The corrosion behaviour of a thermo-mechanically treated Beta C titanium alloy in a 3.5 wt% NaCl solution was investigated in this study. Thermomechanical processing prejudges titanium alloys to improve corrosion properties. Scanning electron microscopy and electron-backscattered diffractions were used to investigate the microstructural evolution and grain orientation after thermo-mechanical processing. The electrochemical characteristics of Beta C titanium alloy were examined using electrochemical impedance spectroscopy (EIS), corrosion potential, and corrosion current density measurements. The 45 percent deformed specimen experiences significant plastic deformation with increased dislocation density, resulting in strong ND //<111> orientation. However, the annealing after deformation exhibits a strong g-fiber texture with the lowest in-grain misorientation, which contributes to improving the corrosion resistance of the titanium alloy.
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Autorzy i Afiliacje

Unissa Nichul
1
ORCID: ORCID
Pankaj Tambe
2
ORCID: ORCID
Vijay Hiwarkar
1
ORCID: ORCID

  1. Defence Institute of Advanced Technology, Department of Metallurgical and Materials Engineering, Pune, Maharashtra, India
  2. VIT-AP University, School of Mechanical Engineering, Amaravati, Andhra Pradesh, India

Abstrakt

In the present time, advanced high strength steel (AHSS) has secured a dominant place in the automobile sector due to its high strength and good toughness along with the reduced weight of car body which results in increased fuel efficiency, controlled emission of greenhouse gases and increased passengers’ safety. In the present study, four new advanced high strength steels (AHSS) have been developed using three different processing routes, i.e., thermomechanical controlled processing (TMCP), quenching treatment (QT), and quenching & tempering (Q&T) processes, respectively. The current steels have achieved a better combination of the high level of strength with reasonable ductility in case of TMCP as compared to the other processing conditions. The achievable ultrahigh strength is primarily attributed to mixed microstructure comprising lower bainite and lath martensite as well as grain refinement and precipitation hardening.

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Autorzy i Afiliacje

G. Mandal
S.K. Ghosh
S. Chatterjee

Abstrakt

Laser-generated surface patterns provide the means for local mechanical interlocking between the joined materials, tunes the wettability of surfaces that come in contact, and generally are the main factor for bonding strength enhancement, especially between dissimilar materials. This paper presents the influence of different patterning overlays generated with a pulsed laser on the surface of stainless-steel sheets. For all experiments, an overlapping degree of 90% has been chosen between three different patterns, while the engraving speed, pulse frequency and number of passes have varied. The textured surfaces’ morphology was assessed through optical microscopy, and the roughness of the surfaces was correlated with the corresponding experimental parameters. The results have indicated promising insights for joining stainless steel to plastic materials, which is otherwise difficult to assess through usual welding techniques.
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Autorzy i Afiliacje

E.R. Moldovan
1
ORCID: ORCID
C. Concheso Doria
2
ORCID: ORCID
J.L. Ocaña Moreno
3
ORCID: ORCID
L.S. Baltes
1
ORCID: ORCID
E.M. Stanciu
1
ORCID: ORCID
C. Croitoru
1
ORCID: ORCID
A. Pascu
1
ORCID: ORCID
M.H. Tierean
1
ORCID: ORCID

  1. Transilvania University of Brasov, Brasov, Romania
  2. BSH Electrodomésticos España S.A., Zaragoza, Spain
  3. Universidad Politecnica de Madrid, Madrid, Spain

Abstrakt

The influence of the hold time of the austempering heat treatment at 280°C on the microstructure and corrosion resistance in NaCl-based media of austempered ductile iron was investigated using X-ray diffraction, micro-hardness measurements, corrosion tests and surface observations. Martensite was only found in the sample which was heat treated for a short period (10 minutes). Corrosion tests revealed that this phase does not play any role in the anodic processes. Numerous small pits were observed in the α-phase which is the precursor sites in all samples (whatever the value of the hold time of the austempering heat treatment).

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Autorzy i Afiliacje

H. Krawiec
V. Vignal
J. Lelito
A. Krystianiak
E. Tyrała

Abstrakt

The effect of heat treatment on the corrosion resistance of Ti-6Al-4V alloy was investigated in the artificial saliva solution (MAS). It has been revealed that the thermal annealing treatment temperature favors the cathodic reactions and reduce the protective properties of passive film. The heat treatment causes the enrichment of β phase in vanadium. The lowest corrosion resistance in the artificial saliva revealed the Ti-6Al-4V alloy heated for 2 hours at 950°C. Heterogeneous distribution of vanadium within the β phase decreases the corrosion resistance of the Ti-6Al-4V.

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Autorzy i Afiliacje

J. Ryba
M. Kawalec
E. Tyrała
H. Krawiec

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