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Number of results: 31
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Abstract

Is dark matter real or just a convenient hypothesis? Although it was first proposed almost a century ago, physicists have yet to uncover its true nature. Scientists from the Nicolaus Copernicus University are investigating the phenomenon using atomic clocks.

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Authors and Affiliations

Beata Zjawin
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Abstract

In this study, the effect of gas pressure on the shape and size of the AZ91 alloy powder produced by using the gas atomization method was investigated experimentally. Experiments were carried out at 820°C constant temperature in 2-mm nozzle diameter and by applying 4 different gas pressures (0.5, 1.5, 2.5 and 3.5 MPa). Argon gas was used to atomize the melt. Scanning electron microscope (SEM) to determine the shape of produced AZ91 powders, XRD, XRF and SEM-EDX analysis to determine the phases forming in the internal structures of the produced powders and the percentages of these phases and a laser measuring device for powder size analysis were used. Hardness tests were carried out to determine the mechanical properties of the produced powders. The general appearances of AZ91 alloy powders produced had general appearances of ligament, acicular, droplet, flake and spherical shape, but depending on the increase in gas pressure, the shape of the powders is seen to change mostly towards flake and spherical. It is determined that the finest powder was obtained at 820°C with 2 mm nozzle diameter at 3.5 MPa gas pressure and the powders had complex shapes in general.

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Authors and Affiliations

M. Akkaş
T. Çetin
M. Boz
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Abstract

In this study, precisely controlled large scale gas atomization process was applied to produce spherical and uniform shaped high entropy alloy powder. The gas atomization process was carried out to fabricate CoCrFeNiMn alloy, which was studied for high ductility and mechanical properties at low temperatures. It was confirmed that the mass scale, single phase, equiatomic, and high purity spherical high entropy alloy powder was produced by gas atomization process. The powder was sintered by spark plasma sintering process with various sintering conditions, and mechanical properties were characterized. Through this research, we have developed a mass production process of high quality and spherical high entropy alloy powder, and it is expected to expand applications of this high entropy alloy into fields such as powder injection molding and 3D printing for complex shaped components.
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Authors and Affiliations

Tae Gyu Park
Sang Hyun Lee
Bin Lee
Hye Mi Cho
Won Jung Choi
Bum Sung Kim
Kwang Seon Shin
Taek-Soo Kim
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Abstract

Rare earth Nd-Fe-B, a widely used magnet composition, was synthesized in a shape of powders using gas atomization, a rapid solidification based process. The microstructure and properties were investigated in accordance with solidification rate and densification. Detailed microstructural characterization was performed by using scanning electron microscope (SEM) and the structural properties were measured by using X-ray diffraction. Iron in the form of α-Fe phase was observed in powder of about 30 μm. It was expected that fraction of Nd2Fe14B phase increased rapidly with decrease in powder size, on the other hand that of α-Fe phase was decreased. Nd-rich phase diffused from grain boundary to particle boundary after hot deformation due to capillary action. The coercivity of the alloy decreased with increase in powder size. After hot deformation, Nd2Fe14B phase tend to align to c-axis.

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Authors and Affiliations

Ju-Young Cho
Sardar Farhat Abbas
Yong-Ho Choa
Taek-Soo Kim
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Abstract

The presented article describes the method for determining one of the trace elements occurring in coalbismuth. The subjects of the analysis were coal type 34, 35 and their fly ashes derived from Jastrzębska Spółka Węglowa. The main reason for the research was the extensive use of bismuth in many industry sectors. Additionally, bismuth is on the list of deficit elements, therefore the possibility of obtaining an alternative for its recycling source of it is needed, is required. The research was carried out using atomic absorption spectrometry with electrothermal atomization in a graphite cuvette. The samples were incinerated at 800°C and microwave mineralization in a high-pressure closed system was performed until the spectrometric analysis was achieved. In order to achieve mineralization, a mixture of HF and HNO3 acids was used to turn the samples into acidic solutions. The preparation of the samples was based on available literature data and own observations. In the experiment, the effects of the additive modifier was modified by changing the temperature in further steps: drying, incineration, cooling, atomization and burning were described. In addition, the palladium modifier was used in order to limit secondary reactions and enable the evaporation of matrix components. The measurement conditions which are presented in this article allow for a linear calibration curve to be established. However, this is not clear and the definitive method for determining the bismuth in coal is carried out through the use of ET-AAS.

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Authors and Affiliations

Dorota Czarna
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Abstract

The aim of this work was to determine contents of cadmium, copper, lead, nickel and zinc in soils of 5 poviats in Łódzkie Voivodeship (Poviats: Łódź, Brzeziny, East Łódź, Pabianice and Zgierz). The objects of the investigation were over 500 samples of soils collected from cultivated fields, meadows, fallows and urban areas (lawns and city parks). The concentration of elements in all samples was analyzed by atomic absorption spectrometry after extraction with I rnol/drrr' HCl solution. The highest contents of heavy metals were detected in the City of Łódź area. The amounts of leachable metals in the samples under study were within the ranges: 0.3 - 48.4 ppm Cu, 1.7 - 162.9 ppm Pb; 0.9- 357.6 ppm Zn; below 2.1 ppm Cd and below 7.6 ppm Ni.
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Authors and Affiliations

Anna Turek
Jacek Krystek
Wojciech Wolf
J. Kubicki
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Abstract

Nozzle clogging seriously affects the continuity of spraying powder in vacuum induction melting gas atomization (VIGA) process and increases the consumption of gas and raw materials. However, there are few systematic studies on nozzle clogging. This paper reports the physics of nozzle clogging in gas atomization production. The influence of coupling-length of different melt delivery-tubes on nozzle clogging is studied numerically and experimentally. The interface tracking method of Volume of Fluid (VOF) and the large eddy simulation (LES) model are performed for visualizing the melt droplets flow traces in primary atomization and the associated simulation cloud images compared with experimental results. Four delivery-tube coupling-lengths (0 mm, 3 mm, 5 mm, and 7 mm) relative to nozzle position and two gas pressures (3 MPa and 4.5 MPa) are chosen for this study. The results indicated that the coupling-lengths of 0 mm and 3 mm increases the strength of the recirculation zone, the melt droplets backflow is obvious, and the nozzle is blocked. However, this phenomenon eliminated with increasing coupling-lengths, the atomization process is continuous, but the final fine powder yield decreases. This research is of guiding significance and reference for understanding the nozzle clogging of vacuum induction melting gas atomization (VIGA) technology.
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Authors and Affiliations

Junfeng Wang
1
ORCID: ORCID
Min Xia
1
ORCID: ORCID
Jialun Wu
1
ORCID: ORCID
Changchun Ge
2
ORCID: ORCID

  1. University of Science & Technology Beijing Institute of Special Ceramics and Powder Metallurgy, 30 Xueyuan Road, Haidian District, Beijing,100083, China
  2. University of Science & Technology Academician of CAS, Institute of Special Ceramics and Powder Metallurgy, Beijing, China
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Abstract

With the recent advancement in technology for titanium metal powder injection molding and additive manufacturing, high yield and good flowability powder production is needed. In this study, titanium powder was produced through vacuum induction melting gas atomization with a cold crucible, which can yield various alloy compositions without the need for material pretreatment. The gas behavior in the injection section was simulated according to the orifice protrusion length for effective powder production, and powder was prepared based on the simulation results. The gas distribution changes with the orifice protrusion length, which changes the location of the recirculation zone and production yield of the powder. The produced powders had a spherical morphology, and the content of impurities (N, O) changed with the injected-gas purity.

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Authors and Affiliations

Dae-Kyeom Kim
Young Il Kim
Hwaseon Lee
Young Do Kim
ORCID: ORCID
Dongju Lee
Bin Lee
Taek-Soo Kim
ORCID: ORCID
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Abstract

The paper presents the concept of new swirl inserts. An empty two-phase swirl flow atomizer, and three atomizers with inserts were designed, manufactured and tested. The tested atomizers did not differ in terms of their geometric dimensions, with the only variable being the type swirl chamber filling. Flow resistance and spray angle values were analysed for all the evaluated structures. It was shown that the presence of a swirl insert does not significantly increase flow resistance, but instead results in larger spray angles. Taking into account the values of flow resistance and spray angles, the best design solution turned out to be the set of inserts No. 2.
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Authors and Affiliations

Sylwia Włodarczak
1
Daniel Janecki
2
Bartosz Czajkowski
1
Adam Szmyt
1
Andżelika Krupińska
1
Magdalena Matuszak
1
Marek Ochowiak
1

  1. Department of Chemical Engineering and Equipment, Poznan University of Technology, M. Sklodowska-Curie 5, 60-965 Poznan, Poland
  2. Institute of Environmental Engineering and Biotechnology, University of Opole, 45-032 Opole, Poland
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Abstract

Physical mechanisms of gas recirculation and wake closure were investigated by modeling the gas field generated by High Pressure Gas Atomizer using computational fluid dynamics. A recirculation mechanism based on axial and radial gas pressure gradient was proposed to explain the gas recirculation. The occurrence of wake closure is regarded as a natural result when elongated wake is gradually squeezed by expansion waves of increasing intensity. An abrupt drop could be observed in the numerical aspiration pressure curve, which corresponds well with the experimental results. The axial gradient of gas density is considered as the reason that results in the sudden decrease in aspiration pressure when wake closure occurs. Lastly, it is found that a shorter protrusion length and a smaller melt tip diameter would lead to a smaller wake closure pressure, which could benefit the atomizer design to produce fine metal powder with less gas consumption.
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Authors and Affiliations

Mingxiang Liu
1
ORCID: ORCID
Shan Zhou
2

  1. Shanghai University, School of Materials Science and Engineering, Center for Advanced Solidification Technology, Shanghai 200444, China
  2. Shanghai Jiao Tong University, Institute of Forming Technology and Equipment, 1954 Huashan Road, Shanghai 200030, China
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Abstract

In this paper a new method of frequency jumps detection in data from atomic clock comparisons is proposed. The presented approach is based on histogram analysis for different time intervals averaging phasetime data recorded over a certain period of time. Our method allows identification of multiple frequency jumps for long data series as well to almost real-time jump detection in combination with advanced filtering. Several methods of preliminary data processing have been tested (simple averaging, moving average and Vondrak filtration), to achieve flexibility in adjusting the algorithm parameters for current needs which is the key to its use in determining ensemble time scale or to control systems of physical time scales, such as UTC(PL). The best results have been achieved with the Vondrak filter.
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Authors and Affiliations

Michał Marszalec
1
Marzenna Lusawa
1
Tomasz Osuch
1 2

  1. National Institute of Telecommunications, Szachowa 1, 94-894 Warsaw, Poland
  2. Warsaw University of Technology, Faculty of Electronics and Information Technology, Institute of Electronic Systems, Nowowiejska 15/19, 00-665 Warsaw, Poland
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Abstract

Tin dioxide (SnO2) is an n-type semiconductor and has useful characteristics of high transmittance, excellent electrical properties, and chemical stability. Accordingly, it is widely used in a variety of fields, such as a gas sensor, photocatalyst, optoelectronics, and solar cell. In this study, SnO2 films are deposited by thermal atomic layer deposition (ALD) at 180°C using Tetrakis(dimethylamino)tin and water. A couple of 5.9, 7.4 and 10.1nm-thick SnO2 films are grown on SiO2/Si substrate and then each film is annealed at 400°C in oxygen atmosphere. Current transport of SnO2 films are analyzed by measuring current – voltage characteristics from room temperature to 150°C. It is concluded that electrical property of SnO2 film is concurrently affected by its semiconducting nature and oxidative adsorption on the surface.

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Authors and Affiliations

Seong Yu Yoon
Byung Joon Choi
ORCID: ORCID
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Abstract

Electrode induction melting gas atomization (EIGA) is a newly developed method for preparing ultra-clean metal powders, and is a completely crucible-free melting and atomization process. Based on conducted several atomization experiments, we found that the fine powder yields obtained during the EIGA process were greatly affected by the status of metal melt flow. While, continuous metal melt flow was beneficial for the yield of fine powders, it was in conflict with the principle described for the vacuum induction melting inert gas atomization (VIGA) process. To understand the critical role of continuous metal melt flow in the EIGA process, a computational fluid dynamics (CFD) approach was developed to simulate the gas atomization process. The D50 particle size of powder prepared by atomization under continuous liquid metal flow was about 70 μm, while that obtained by atomization under non-continuous liquid metal flow was about 100 μm. The diameter distribution results of numerical simulations agreed well with the experimental measurements, which demonstrated the accuracy of our simulation method. This study provides theoretical support for understanding the critical role of continuous metal melt flow and improving fine powder yields in the EIGA process. PACS: 02.60.Cb; 43.28.Py; 41.20.Gz; 81.20.Ev
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Authors and Affiliations

Jialun Wu
1
ORCID: ORCID
Min Xia
1
ORCID: ORCID
Junfeng Wang
1
ORCID: ORCID
Changchun Ge
1
ORCID: ORCID

  1. University of Science & Technology Beijing, Institute of Powder Metallurgy and Advanced Ceramics, Beijing 100083, China
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Abstract

The technology of manufacturing silicon solar cells is complex and consists of several stages. The final steps in succession are the deposition of antireflection layer and discharge contacts. Metallic contacts are usually deposited by the screen printing method and then, fired at high temperature. Therefore, this article presents the results of a research on the effect of heat treatment on the properties of the Al2O3 thin film previously deposited by the atomic layer deposition method. It works well as both passivating and antireflection coating. Moreover, heat treatment affects the value of the cell short-circuit current and, thus, its efficiency. The surface morphology, optical and electrical properties were investigated, describing the influence of heat treatment on the properties of the deposited layers and the manufactured solar cells.
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Bibliography

  1. Marks-Bielska, R. et al. The importance of renewable energy sources in Poland’s energy Energies 13, 1–23 (2020). https://doi.org/10.3390/en13184624
  2. Asfar, Y. et al. Evaluating Photovoltaic Performance Indoors. in 2012 38th IEEE Photovoltaic Specialists Conference (PVSC). 1948–1951 (IEEE, Austin, USA 2012).
  3. Ranjan, S. et al. Silicon solar cell production. Comput. Chem. Eng. 35, 1439–1453 (2011). https://doi.org/10.1016/j.compchemeng.2011.04.017
  4. Drygala, A. et al. Influence of laser texturization surface and atomic layer deposition on optical properties of polycrystalline silicon. Int. J. Hydrog. Energy 41, 7563–7567 (2016). https://doi.org/10.1016/j.ijhydene.2015.12.180
  5. Hou, G., Garcia, I. & Rey-Stolle, I. High-low refractive index stacks for broadband antireflection coatings for multijunction solar cells. Sol. Energy 217, 29–39 (2021). https://doi.org/10.1016/j.solener.2021.01.060
  6. Dobrzański, L. A., Szindler, M., Drygała, A. & Szindler, M.M., Silicon solar cells with Al2O3 antireflection coating. Cen. Eur. J. Phys. 12, 666–670 (2014). https://doi.org/10.2478/s11534-014-0500-9
  7. Sarkar, S. & Pradhan, S. K. Silica-based antireflection coating by glancing angle deposition. Surf. Eng. 35, 982–985. (2019). https://doi.org/10.1080/02670844.2019.1596578
  8. Szindler, M. Szindler, M. M., Boryło, P. & Jung, T. Structure and optical properties of TiO2 thin films deposited by ALD Open Phys. 15, 1067–1071 (2017). https://doi.org/10.1515/phys-2017-0137
  9. Król, K. et al. Influence of atomic layer deposition temperature on the electrical properties of Al/ZrO2/SiO2/4H-SiC metal-oxide semiconductor structures. Phys. Status Solidi (A) 215, 1–7 (2018). https://doi.org/10.1002/pssa.201700882
  10. Boryło, P. et al. Structure and properties of Al2O3 thin films deposited by ALD proces. Vacuum 131, 319–326 (2016). https://doi.org/10.1016/j.vacuum.2016.07.013
  11. Drabczyk, K. et al. Comparison of diffused layer prepared using liquid dopant solutions and pastes for solar cell with screen printed electrodes. Microelectron. Int. 33, 167–171 (2016). https://doi.org/10.1108/MI-03-2016-0031
  12. Öğütman, K. et al. Spatial atomic layer deposition of aluminum oxide as a passivating hole contact for silicon solar Phys. Status Solidi (A) 217, 1–6 (2020). https://doi.org/10.1002/pssa.202000348
  13. Drabczyk, K. et al. Electroluminescence imaging for determining the influence of metallization parameters for solar cell metal contacts. Sol. Energy 126, 14–21 (2016). https://doi.org/10.1016/j.solener.2015.12.029
  14. Park, H. H. Inorganic materials by atomic layer deposition for perovskite solar cells. Nanomaterials 11, 1–22 (2021). https://doi.org/10.3390/nano11010088
  15. Hossain, A. et al. Atomic layer deposition enabling higher efficiency solar cells: A review. Nano Materials 2, 204–226 (2020). https://doi.org/10.1016/j.nanoms.2019.10.001
  16. Werner, F. et al. High-rate atomic layer deposition of Al2O3 for the surface passivation of Si solar cells. Energy Procedia 8, 301–306 (2011). https://doi.org/10.1016/j.egypro.2011.06.140
  17. Werner, F., Cosceev, A. & Schmidt, J. Silicon surface passivation by Al2O3: Recombination parameters and inversion layer solar cells. Energy Procedia 27, 319–324 (2012). https://doi.org/10.1016/j.egypro.2012.07.070
  18. Swatowska, B. Antireflective and passivation properties of the photovoltaic structure with Al2O3 layer of different thickness. Microelectron. Int. 35, 177–180 (2018). https://doi.org/10.1108/MI-04-2018-0020
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Authors and Affiliations

Marek Szindler
1
ORCID: ORCID
Magdalena M. Szindler
2
ORCID: ORCID

  1. Scientific and Didactic Laboratory of Nanotechnology and Material Technologies, Faculty of Mechanical Engineering, Silesian University of Technology, 7 Towarowa St., 44-100 Gliwice, Poland
  2. Department of Engineering Materials and Biomaterials, Faculty of Mechanical Engineering, Silesian University of Technology, 18a Konarskiego St., 44-100 Gliwice, Poland
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Abstract

The article describes the results of a research on the surface morphology and optical properties of Al 2O 3, ZnO, and TiO 2 thin films deposited by atomic layer deposition (ALD) for applications in silicon solar cells. The surface topography and elemental composition were characterised using a scanning electron microscope, and thickness was determined using an optical reflectometer. The samples were structurally examined using a Raman spectrometer. The structural variant was identified: for Al 2O 3 it is sapphire, for TiO 2 it is anatase, and for ZnO it is wurtzite. Possibilities of minimising light reflection using single and double thin film systems below 5% were presented. For the first time, the effectiveness of these thin films on the current-voltage characteristics and electrical parameters of manufactured silicon solar cells was examined and compared. The solar cell with the highest efficiency of converting solar radiation into electricity was obtained for Al 2O 3/TiO 2 and the efficiency of such a photovoltaic device was 18.74%.
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Authors and Affiliations

Marek Szindler
1
ORCID: ORCID
Magdalena M. Szindler
2
ORCID: ORCID

  1. Scientific and Didactic Laboratory of Nanotechnology and Material Technologies, Faculty of Mechanical Engineering, Silesian University of Technology, ul. Towarowa 7, 44-100 Gliwice, Poland
  2. Department of Engineering Materials and Biomaterials, Faculty of Mechanical Engineering, Silesian University of Technology, ul. Konarskiego 18a, 44-100 Gliwice, Poland
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Abstract

Al 2O 3/TiO 2 thin films were deposited onto monocrystalline silicon surfaces using an atomic layer deposition. Their surface morphology and optical properties were examined for their possible use in solar cells. The surface condition and chemical composition were characterized using a scanning electron microscope and the thickness was measured using a spectroscopic reflectometer. The refractive index and the reflection characteristics were determined. First, the optical properties of the Al 2O 3 thin film and its influence on recombination in the semiconductor were examined. In this way, it can fulfil a double role in a solar cell. Since reflection reduction was only achieved in a narrow range, it was decided to use the Al 2O 3/TiO 2 system. Thanks to this solution, the light reflection was reduced in a wide range (even below 0.2%).
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Authors and Affiliations

Marek Szindler
1
ORCID: ORCID
Magdalena M. Szindler
2
ORCID: ORCID
Justyna Orwat
3
ORCID: ORCID
Grażyna Kulesza-Matlak
4
ORCID: ORCID

  1. Scientific and Didactic Laboratory of Nanotechnology and Material Technologies, Faculty of Mechanical Engineering, Silesian University of Technology, 7 Towarowa St., 44-100 Gliwice, Poland
  2. Department of Engineering Materials and Biomaterials, Silesian University of Technology, 18a Konarskiego St., 44-100 Gliwice, Poland
  3. Department of Mining, Safety Engineering and Industrial Automation, Silesian University of Technology, 2 Akademicka St., 44-100 Gliwice, Poland
  4. Institute of Metallurgy and Materials Science of Polish Academy of Sciences, 25 Reymonta St., 30-059 Krakow, Poland
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Abstract

The methods arc described for determinations of Al, Fe, Ca, Mg, Ba, Cr, Mn, Ni, Cu, Zn, Pb, Cd, V and Sr in botanical, coal fly ash and soil samples by flame atomic absorption spectrometry (FAAS), and inductively coupled plasma atomic emission spectrometry (!CP-AES). Special attention has been paid to sample preparation, an important stage at which a sample is explored to contaminants. Results of the analysis of all samples arc discussed.
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Authors and Affiliations

Krystyna Srogi
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Abstract

Professor Łucjan Krause, a long-term head of the Department of Physics of the University of Windsor died on July 4, 2022 in Windsor, Ontario in Canada. He was an outstanding Polish-Canadian physicist, who made important contributions to the atomic, molecular and optical physics. Born in Poznań on January 8, 1928, as a scout and Home Army soldier (nickname “Leonidas”), he took part in the Warsaw Uprising and after its failure was sent to a POW camp in Bergen-Belsen, in Germany. In 1951 after graduating from King’s College University of London, he emigrated to Canada, where he began his studies of physics at the University of Toronto. In 1955 he obtained in Toronto the PhD degree in physics under the supervision of Professor Harry Welsh in Raman spectroscopy of gases. Then for three years he worked as an associate professor of physics at the Memorial University of Newfoundland in St. John’s. In 1958 he accepted an invitation from the University of Windsor and became a head of its Department of Physics. In Windsor, Krause created a vibrant scientific centre in which he developed research program in experimental studies of inelastic atomic collisions. The main attention was focused on the excitation energy transfer between colliding atoms, the quenching of fluorescence radiation by molecular gases and, more recently, on laser spectroscopy of metal excimers. In 1963 he initiated the cooperation with Professor Aleksander Jabłoński, head of the Chair of Experimental Physics of Nicolaus Copernicus University in Toruń. Thanks to this cooperation numerous physicists, first from Toruń and later from other Polish scientific centers – as postdoctoral fellows – participated in experiments with the use of advanced laser equipment, not available in Poland at that time. In this way, Łucjan Krause contributed significantly to the development of physics in Poland. In order to pay tribute to his effort and devotion, in 1983 the Senate of Nicolaus Copernicus University awarded Professor Łucjan Krause a doctor honoris causa degree.
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Authors and Affiliations

Józef Szudy
1

  1. Instytut FizykiUMK, Toruń
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Abstract

We describe Urukul, a frequency synthesizer based on direct digital synthesis (DDS), optimized for wave generate control in atomic, molecular and optical (AMO) physics experiments. The Urukul module is a part of the Sinara family of modular, open-source hardware designed for the ARTIQ quantum operating system. The Urukul has 4-channel, sub-Hz frequency resolution, controlled phase steps and accurate output amplitude control. The module is available in two population variants. This paper presents Urukul module construction and obtained characteristics.
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Authors and Affiliations

Grzegorz Kasprowicz
1
Thomas Harty
2
Sébastien Bourdeauducq
3
Robert Jördens
4
David Allcock
5
David Nadlinger
2
Joseph W. Britton
6 7
Ana Sotirova
2
Dorota Nowicka
1

  1. Warsaw University of Technology, Poland
  2. Oxford University, UK
  3. M-Labs, Hong Kong
  4. QUARTIQ, Germany
  5. Univeristy of Oregon, US
  6. University of Maryland, US
  7. Army Research Lab, US
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Abstract

This paper sets out to characterise and analyse logical atomism of Bertrand Russell. Main tenets of that theory are described by reference to Russell’s lecture Facts and Propositions (1918) and to other publications by that author. The essential claims of Russell’s position are discussed and confronted with tenets of ontology of situations developed by Bogusław Wolniewicz, a position inspired by logical atomism of Ludwig Wittgenstein. The author argues that several of Russell’s theses on logical atomism can be interpreted in the light of Wolniewicz’s ontology of situations. Finally, some minor concluding remarks are offered that can help to develop an ontology conceived in the spirit of the ontology of logical atomism. 366 Janusz Kaczmarek
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Authors and Affiliations

Janusz Kaczmarek
1
ORCID: ORCID

  1. Uniwersytet Łódzki, Instytut Filozofii, ul. Lindleya 3/5, 90-131 Łódź
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Abstract

The objective of this study was to deposit directly chromium with diamond nanoparticles (ND) on aluminum alloys and investigate the coating surface. The chromium coatings on aluminum alloys were obtained by electrochemical deposition. The coatings were doped with ND. The diamond nanoparticles were obtained by detonation synthesis. Chromium coatings were deposited on aluminum alloys with a silicon content of 7 % and 10 %. The ND concentration in the electrolyte was 25 g/l. The surface analysis was performed by means of Atomic force microscopy. The surface of the coating of chromium with ND on Al10Si is twice more even than that on Al7Si. The microstructure and microhardness were examined with a metallographic microscope and a microhardness tester. The microhardness of the coated samples is 9163 MPa compared to 893 MPa of uncoated aluminum samples. The thickness of the chromium coatings doped with diamond nanoparticles is between 45 – 55 μm. The coatings are dense, continuous and uniform with good adhesion to the substrate material.

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Authors and Affiliations

V. Petkov
R. Valov
S. Simeonova
M. Kandeva
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Abstract

An alternative fabrication method for metallic fuel in Gen-IV reactor was introduced with vibration packing of nuclear fuel particles to facilitate remote fabrication in a hot cell and reduce the generation of long-lived radioactive wastes. Vibration packing experiments on metallic particulate fuel using a surrogate 316L stainless steel powder were done to investigate the packing density and the uniformity of the simulated fuel according to the filling method and the vibration condition. Metallic particulate fuel filled with a pre-mixed power over all particles had the highest packing fraction and the most uniform distribution among the filling methods. The vibration packing method showed that it could fabricate the metallic particulate fuel having uniform distribution of spherical fuel particles through the adjustment of the filling method of the metallic powder and the vibration condition of the metallic particulate fuel.
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Authors and Affiliations

Ki-Hwan Kim
1
ORCID: ORCID
Seong-Jun Ha
1
Sang-Gyu Park
1
Seoung-Woo Kuk
1
Jeong-Yong Park
1

  1. Korea Atomic Energy Research Institute, Next-Generation Fuel Technology Development Division, 989-111, Daedeok-daero, Yuseong-gu, Daejeon, 34057, Republic of Korea
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Abstract

Gadolinium oxide (Gd2O3) is one of the lanthanide rare-earth oxides, which has been extensively studied due to its versatile functionalities, such as a high permittivity, reactivity with moisture, and ionic conductivity, etc. In this work, GdOx thin film was grown by atomic layer deposition using cyclopentadienyl (Cp)-based Gd precursor and water. As-grown GdOx film was amorphous and had a sub-stoichiometric (x ~ 1.2) composition with a uniform elemental depth profile. ~3 nm-thick GdOx thin film could modify the hydrophilic Si substrate into hydrophobic surface with water wetting angle of 70°. Wetting and electrical test revealed that the growth temperature affects the hydrophobicity and electrical strength of the as-grown GdOx film.
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Authors and Affiliations

Sung Yeon Ryu
1
Hee Ju Yun
1
Min Hwan Lee
2
Byung Joon Choi
1
ORCID: ORCID

  1. Seoul National University of Science and Technology, Department of Material Science and Engineering, Seoul 01811, Korea
  2. University of California Merced, Department of Mechanical Engineering, Merced, California, USA

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